EP1829059A1 - Procede de production d'un conducteur d'enroulement pour appareils electriques et conducteur d'enroulement produit par ce procede - Google Patents
Procede de production d'un conducteur d'enroulement pour appareils electriques et conducteur d'enroulement produit par ce procedeInfo
- Publication number
- EP1829059A1 EP1829059A1 EP05850434A EP05850434A EP1829059A1 EP 1829059 A1 EP1829059 A1 EP 1829059A1 EP 05850434 A EP05850434 A EP 05850434A EP 05850434 A EP05850434 A EP 05850434A EP 1829059 A1 EP1829059 A1 EP 1829059A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- insulation
- thermoplastic
- temperature
- layer
- layers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
- H01B3/18—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
- H01B3/30—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F41/00—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties
- H01F41/02—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for manufacturing cores, coils, or magnets
- H01F41/04—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for manufacturing cores, coils, or magnets for manufacturing coils
- H01F41/12—Insulating of windings
- H01F41/122—Insulating between turns or between winding layers
-
- H—ELECTRICITY
- H02—GENERATION; CONVERSION OR DISTRIBUTION OF ELECTRIC POWER
- H02K—DYNAMO-ELECTRIC MACHINES
- H02K3/00—Details of windings
- H02K3/30—Windings characterised by the insulating material
Definitions
- the invention relates to a method for producing a winding conductor for electrical devices, in particular for electrical machines and transformers.
- the invention also relates to a winding conductor produced by this process.
- a winding conductor for magnetic coils in which the metallic core conductor with a paint insulation (basic insulation) on the basis of polyurethane PU, polyester imide PEI or THEIC polyester imide THEIC-PEI ver ⁇ see. On this paint insulation a baked enamel layer is placed on ⁇ , with which the winding conductors are fused in a winding block.
- an enamel insulation conductor core is generally carried out by loading ⁇ layers of the bare metal wire with a dissolved in a solvent polymer, for example by spraying or in a dipping method, and then drying.
- a suitable method for producing such a single-layer or multi-layer enameled wire is explained in more detail, for example, in DE 195 38 189 A1.
- thermoplastic materials used are not suitable for continuous use temperatures above 15O 0 C.
- a copper wire is usually used as a winding conductor, which is provided with a simple paint insulation.
- This paint insulation is also referred to as functional insulation and has only a low dielectric strength.
- winding conductors suitable for this purpose must have a significantly improved dielectric strength compared to conventional paint insulation.
- Wickellei ⁇ ter are known in which at least three thermoplastic Iso ⁇ lations slaughteren are applied to a wire without paint insulation in the extrusion process.
- plastics mixtures are used, which on the one hand to each other reaches a separability of the individual layers and on the other hand, the solderability ver ⁇ is improved, since the insulation layers in the solder bath easily detached from the wire.
- An advantage of the separability is that, for a damage to the outermost insulating layer crack propagation takes place only up to the surface of the second insulation layer, and this as well as all further inward lie ⁇ constricting layers remain intact.
- these known winding conductors are only suitable for use up to thermal class B (130 0 C).
- an embodiment of an insulated wire in which a PU polyurethane coated wire with three further insulating layers of a fluoropolymer is extrusion-coated.
- Such an insulated wire is, however, for use as a winding conductor only suitable, since the adhesion between the poly-urethane layer and the innermost thermoplastic insulating layer and layers between the thermoplastic insulation ⁇ is insufficient itself, so that it at exerting a tensile stress in peeling of the insulating layers can lead from the painted wire.
- Winding conductors are known from EP 0 825 623 A2, in which a plurality of insulation layers are likewise applied by extrusion to a wire, which may be a bare metal wire or a wire provided with functional insulation. These known winding conductors are only suitable for use up to thermal class B.
- thermoplastic insulation layer having one or more insulation layers from a high temperature thermoplastic and is suitable for higher thermal classes ge ⁇ . These high-temperature thermoplastics are applied to the bare metal wire in an extrusion process. In practice, however, it has been found that the adhesion of the thermoplastic insulation layer to the bare metal wire is unsatisfactory.
- the invention is based on the object of providing a method for the production of a winding conductor for electrical devices, in particular for transformers, which is also suitable for use in a higher thermal class than the thermal class B.
- the invention has the object of providing a Herge by this method ⁇ presented winding conductor indicated.
- thermoplastic insulation layers ie, one or more thermoplastic insulation layers, each applied by an extrusion process to an insulated with a functional insulation enameled wire
- each of these thermoplastic insulation layers consists exclusively of a high-temperature thermoplastic.
- the enameled wire is surrounded by at least one insulating layer consisting of a high-temperature thermoplastic.
- Resistant to high peraturthermoplasten the purposes of the present invention are all suitable for thermoplastic processing ⁇ art materials which have continuous service temperatures in excess of 150 °, with the exception of the group of melt-processable fluoropolymers.
- Plastics such as polyethersulfone (PES), polyphenylsulfone (PPSU), polyetherimide (PEI), syndiotactic polystyrene (s-PS), polyphenylene sulfide (PPS), polyaryl ether ketones (PAEK), polyether ether ketone (PEEK ), thermoplastic polyimide (t-PI), liquid crystalline polymers (LCP) as well as some special polyarylates (PAR) and partially aromatic polyamides (PPA).
- PES polyethersulfone
- PPSU polyphenylsulfone
- PEI polyetherimide
- s-PS syndiotactic polystyrene
- PPS polyphenylene sulfide
- PAEK polyaryl ether ketones
- PEEK polyether ether ketone
- thermoplastic polyimide t-PI
- LCP liquid crystalline polymers
- PAR partially aromatic polyamides
- thermoplastics consisting be understood in the context of the present invention is such that, if added for processing reasons copolymers which by itself no Hochtem ⁇ peraturthermoplaste would, if necessary in a peripheral ⁇ EXISTING the are that the resulting polymer mixture still the group attributable to high-temperature thermoplastics. Representation beyond the high-temperature thermoplastics, customary processing aids or additives for modification or improvement of material properties, for example plasticizers, fillers or dyes may be added ⁇ mixes.
- the enameled wire can be a commercially available enameled wire, ie one with a single-layer or multi-layered enameled wire. onsisoltechnik for the corresponding thermal class verse ⁇ henen metal wire act.
- the invention is based on the finding that the thermoplastic insulation layer or the thermoplastic insulation layers adhere significantly better on a paint wire than on a bare metal wire.
- thermal class F of the magnet wire is in particular a copper wire whose coating layer has a degree of 1 entspre ⁇ sponding thickness with a single coat of modified polyurethane, the thickness of theforensicsisolati- ons slaughter a function of the conductor diameter in the standard DIN EN 60 317- 0- 1 and DIN EN 60 317-20.
- thermal class H is as enameled wire, preferably a copper wire grade 1 having a two layer coating of modified polyester-amide-imide THEIC and Overcoat vorgese ⁇ hen, specified according to DIN EN 60 317-0-1 and DIN EN 60317-13.
- Winding conductors in which an enameled wire is provided with only one thermoplastic insulation layer, are referred to as wound conductors with basic insulation.
- wound conductors with basic insulation In the case of two thermoplastic insulation layers, one speaks of winding conductors with additional insulation, in the case of three or more thermoplastic insulation layers of wound conductors with reinforced insulation.
- one or more insulation layers, each consisting of high-temperature thermoplastics, to an enameled wire can be extremely thin, non-porous and stress-resistant winding conductor with basic, ⁇ additional and reinforced insulation produce that the claims for use in the thermal classes F and H suffice.
- the total insulation layer thickness (functional insulation + three thermoplastic insulation layers) layers) are still well below 100 microns and the dielectric strength is greater than 18 kV.
- the extrusion coating is carried out preferably in the so-called tubular stretching method, wherein the high temperature thermoplastic emerges in tubular form from a surrounding annular die and the wire only at a distance from the annular die, the upper surface of the wire touches ⁇ .
- the high temperature thermoplastic emerges in tubular form from a surrounding annular die and the wire only at a distance from the annular die, the upper surface of the wire touches ⁇ .
- which is characterized by moving through the annular nozzle toward ⁇ wire takes the high-temperature thermoplastics and claimed it due to this relative motion to train, wherein the thickness of the applied insulation layer is controlled by the speed of the wire. Since the total insulation is applied regardless of the number of insulation layers in a single operation, a cost-effective production of the winding conductor is possible due to the high production speeds possible in the extrusion coating and the low material usage due to the thin insulating layers.
- the winding conductors according to the invention make it possible to produce grid connection transformers, control transformers and isolating transformers for the thermal classes F and H in smaller and more compact sizes.
- two or more insulation layers are applied from a high-temperature thermoplastic, they can be applied to the wire in a single operation in a tandem or / and coextrusion process, which is particularly cost-effective.
- each individual thermoplastic insulation layer depends on the wire diameter, between 10-40 ⁇ m. Preferably, thicknesses ⁇ 25 microns, in particular between 15-25 ⁇ m. Winding conductors with such layer thicknesses allow, with sufficient dielectric strength, particularly space- saving windings.
- thermoplastic insulation layer On the functional insulation of the enameled wire be as well, in case a plurality of thermoplastic insulating layers, good adhesion of the thermoplastic insulating layers together ensured.
- the good adhesion is a prerequisite for the fact that it does not come in the later winding production to detachment or to a wrinkling and cavitation between individual insulation layers.
- glowing and partial discharge processes can quickly occur in such cavities, destroying the insulation layers and leading to early failures.
- a good adhesion of the functional insulation and the first thermoplastic insulation layer can be achieved if the wire is preheated accordingly in the extrusion coating.
- this preheating temperature is 150 0 C - 250 0 C, be ⁇ vorzugt at 180 0 C - 220 0 C.
- thermoplastics and the extrusion process can be constructed with sufficient adhesion adhesion between the layers, a completely separable insulation layer system, or optionally an insulation layer system in which only a defined partial separation of individual insulation layers is possible.
- a paint a first wire and a second thermoplastic insulation ⁇ layer from the same high temperature thermoplastics applied by co-extrusion so these two are Iso ⁇ lations slaughteren later in the cooled state is no longer detachable from each other.
- two different, mutually compatible thermoplastics are applied in Koextrusions ⁇ method.
- the coating is carried out with the same insulating materials in a tandem process, wherein the first thermoplastic insulation layer undergoes a certain cooling - about 50-100 0 C below the processing temperature - and solidifies before the second thermoplastic insulation layer is applied, then these two layers in the later , cooled state separated from each other, but the above-mentioned necessary adhesion adhesion is maintained.
- thermoplastics As with all thermoplastics, high-temperature thermoplastics also have to distinguish between amorphous and semi-crystalline thermoplastics.
- amorphous high-temperature thermoplastics are PES, PPSU, PEI and PAR. These have a glass transition temperature Tg (softening temperature) of about 22O 0 C.
- Tg glass transition temperature
- PPS, s-PS, PAEK, PEEK, LCP and PPA are partially crystalline, with a melting point> 270 0 C. This distinction is of Be ⁇ importance for use in the Thermal class F or H, as standard EN 60317-20 prescribes a thermal shock test at elevated temperature.
- this is the La ⁇ delay a, around a mandrel, the diameter of which depends on the wire diameter, wound sample which is (also depending on the wire diameter) at a defined winding tension, at least 175 0 C for 30 minutes with subsequent ⁇ the Testing the dielectric strength.
- the softening temperature of the amorphous high-temperature thermoplastics is on par with the prescribed minimum storage temperature of 220 0 C.
- thermoplastic insulating layer preferably made of a semi-crystalline high ⁇ temperature thermoplastic with a melting point> 270 0 C.
- the thermoplastic insulating layer preferably made of a semi-crystalline high ⁇ temperature thermoplastic with a melting point> 270 0 C. in a multi-layer structure of the thermoplastic insulation can also amorphous high-temperature thermoplastics are used for internal insulation layers, as long as the La ⁇ delay temperature does not exceed the required minimum temperature of 220 0 C.
- Significantly higher Lagerungstemperatu ⁇ called ren, only the semi-crystalline high-temperature thermostat should also in a multi-layer structure preferably plastering apply.
- thermoplastic insulating layers are PPS, PAEK, PEEK, LCP, s-PS, t-PI and PPA.
- the outer insulating layer is preferably made of one of the mentioned semi-crystalline high-temperature layers. thermo-thermoplastic. Such a winding conductor is then suitable for casting with all impregnating resins.
- the object according to the invention is achieved by a winding conductor having the features of patent claim 13, the advantages of which as well as the pre ⁇ parts of the winding conductor according to the claim 13 subordinate claims mutatis mutandis result from the respective zugeord ⁇ Neten method claims.
- Fig. 1-7 each an extruder arrangement according to the invention for the preparation as well as a respectively with this Extruderanord ⁇ winding conductor voltage produced in each schematic representations principle.
- a pre-insulated enameled wire 2 is passed through an extruder 4 at a predetermined speed v and coated in a tubular stretching process with a thermoplastic insulation layer 60 made of a high-temperature plastic.
- the enameled wire 2 is preheated to a predetermined temperature prior to the extrusion coating. This preheating he ⁇ preferably follows immediately before the extrusion coating within the extruder.
- a so- ⁇ -called base-isolated winding conductor 6a occurs with only a thermoplastic insulating layer 60 from the extruder. 4
- the enameled wire 2 consists of a bare metal wire 20, which is coated with a single or multi-layer functional insulation 22 made of a lacquer. On this enameled wire 2, a single ther ⁇ moplastic insulating layer 60 is applied.
- Fig. 2 illustrates an extrusion process in which the enameled wire 2 with the aid of two in tandem arrangement operated extruder 4 with two thermoplastic insulation layers is provided.
- End product is a winding conductor 6b with additional insulation.
- a second insulating layer 62 is applied on a first insulating layer 60.
- the enameled wire 2 is coated in a coextrusion process with two insulation layers 60, 62.
- the first insulation layer 60 and the second insulation layer 62 can not be more separated from each other.
- the extrusion process of the enameled wire 2 by means of three is in tandem Betrie ⁇ surrounded extruders 4 with three insulating layers 60,62,64 provided.
- a winding conductor 6d with reinforced insulation which has a first, second and third ther ⁇ moplastic insulating layers 60, 62 and 64, respectively.
- FIG. 5 shows an arrangement of three extruders 4 operated by the coextrusion process, with which the enamelled wire 2 is likewise provided with three insulation layers 60, 62, 64.
- Darge ⁇ represents, in which the enameled wire 2 is also provided with three Isolati ⁇ ons slaughteren 60,62,64, wherein the two inner insulation layers 60,62 applied in the coextrusion process and the outer insulation layer 64 with the help a downstream extruder 4 is applied.
- the first and second insulating layers can be 60 or 62 are not separated from each other. While a separability between the second and third insulating layer 62 and 64 is achieved.
- Diameter copper conductor 0.8 mm
- Preheating temperature 200 ° C
- Diameter winding wire with insulation layer 0, 889 mm
- Diameter winding wire with insulation layer 0, 891 mm
- Insulation layer and PPS (second insulation layer)
- Tandem extrusion coating with PSU first insulation layer
- PPSU second insulation layer
- PEEK third insulation layer
- Diameter winding wire with insulation layers 0, 981 mm
- Diameter winding wire with insulation layers 0, 985 mm
- Diameter winding wire with insulation layers 0, 979 mm
- Tandem extrusion coating with PSU (first insulation layer), coextrusion process PPSU (second insulation layer) and PEEK (third insulation layer) Preheating temperature: 210 0 C
- Diameter winding wire with insulation layers 0, 973 mm
- Diameter winding wire with insulation layers 0, 981 mm
- FIG. 1 2.1 winding wire with a single insulation layer
- Diameter copper conductor 0, 8 mm
- Diameter enamelled copper wire grade 1 (functionalis, polyester-THEIC and amidimide, double-layered, 845 mm):
- Diameter winding wire with functional insulation 0, 895 mm
- Diameter winding wire with insulation layers 0, 981 mm
Landscapes
- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Processes Specially Adapted For Manufacturing Cables (AREA)
- Insulated Conductors (AREA)
- Insulation, Fastening Of Motor, Generator Windings (AREA)
Abstract
L'invention concerne un procédé de production d'un conducteur d'enroulement (6a) destiné à des appareils électriques. Selon ce procédé, une ou plusieurs couches d'isolation thermoplastiques (60) sont appliquées par un procédé d'extrusion sur un fil laqué (2) préisolé au moyen d'une isolation fonctionnelle (22), chacune de ces couches d'isolation thermoplastiques (60) étant constituée exclusivement d'un thermoplastique haute température. L'invention concerne en outre un conducteur d'enroulement produit par ce procédé. L'utilisation d'un thermoplastique haute température comme couche d'isolation permet de produire à moindre coût par un procédé d'extrusion des conducteurs d'enroulement adaptés aux classes thermiques H et F.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102004058755 | 2004-12-06 | ||
PCT/EP2005/056456 WO2006061360A1 (fr) | 2004-12-06 | 2005-12-05 | Procede de production d'un conducteur d'enroulement pour appareils electriques et conducteur d'enroulement produit par ce procede |
Publications (1)
Publication Number | Publication Date |
---|---|
EP1829059A1 true EP1829059A1 (fr) | 2007-09-05 |
Family
ID=35840294
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP05850434A Withdrawn EP1829059A1 (fr) | 2004-12-06 | 2005-12-05 | Procede de production d'un conducteur d'enroulement pour appareils electriques et conducteur d'enroulement produit par ce procede |
Country Status (5)
Country | Link |
---|---|
US (1) | US20080128154A1 (fr) |
EP (1) | EP1829059A1 (fr) |
JP (1) | JP2008523544A (fr) |
CN (1) | CN101073127A (fr) |
WO (1) | WO2006061360A1 (fr) |
Families Citing this family (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2008126375A1 (fr) * | 2007-03-30 | 2008-10-23 | The Furukawa Electric Co., Ltd. | Procédé et appareil de production de fil isolé |
CN101246766B (zh) * | 2008-03-06 | 2010-06-16 | 上海弘杰电工器材成套有限公司 | 一种绕组线的制造工艺 |
JP5306742B2 (ja) * | 2008-08-28 | 2013-10-02 | 古河電気工業株式会社 | 絶縁ワイヤ |
US20100219555A1 (en) * | 2009-02-27 | 2010-09-02 | Tyco Electronics Corporation | Method for extrusion of multi-layer coated elongate member |
US20140216340A1 (en) * | 2010-04-08 | 2014-08-07 | Furukawa Electric Co., Ltd. | Method and apparatus for producing insulated wire |
DE102011052518A1 (de) * | 2011-08-09 | 2013-02-14 | Elantas Gmbh | Lösemittelfreie Drahtlackzusammensetzung |
US20140336326A1 (en) * | 2011-11-24 | 2014-11-13 | Kaneka Corporation | Electric/electronic component using flame-retardant polyester-based resin composition |
CN102568665A (zh) * | 2012-03-07 | 2012-07-11 | 大同电线电缆科技(吴江)有限公司 | 复合绝缘电线、其制备方法及用于该方法的装置 |
EP2885856B1 (fr) * | 2012-10-12 | 2020-04-08 | Siemens Aktiengesellschaft | Procédé de fabrication d'isolation de conducteur |
US20140152155A1 (en) * | 2012-12-05 | 2014-06-05 | Ge Oil & Gas Esp, Inc. | High temperature downhole motors with advanced polyimide insulation materials |
KR101748477B1 (ko) | 2013-02-07 | 2017-06-16 | 후루카와 덴키 고교 가부시키가이샤 | 에나멜 수지 절연 적층체 및 그것을 이용한 절연 와이어 및 전기ㆍ전자 기기 |
WO2015033820A1 (fr) | 2013-09-06 | 2015-03-12 | 古河電気工業株式会社 | Câble plat ainsi que procédé de fabrication de celui-ci, et appareil électrique |
EP3043355A4 (fr) | 2013-09-06 | 2017-04-26 | Furukawa Electric Co., Ltd. | Câble plat ainsi que procédé de fabrication de celui-ci, et appareil électrique |
US9324476B2 (en) * | 2014-02-05 | 2016-04-26 | Essex Group, Inc. | Insulated winding wire |
US10199138B2 (en) * | 2014-02-05 | 2019-02-05 | Essex Group, Inc. | Insulated winding wire |
WO2015130681A1 (fr) * | 2014-02-25 | 2015-09-03 | Essex Group, Inc. | Fil de bobinage isolé |
DE102014107117B4 (de) * | 2014-05-20 | 2018-09-06 | Schwering & Hasse Elektrodraht Gmbh | Lackdraht, Wickelkörper und Verfahren zur Herstellung eines Lackdrahtes |
CA3019562A1 (fr) * | 2016-03-31 | 2017-10-05 | Essex Group, Inc. | Articles de fil d'enroulement isoles ayant des revetements conformes |
US10079080B2 (en) | 2016-06-20 | 2018-09-18 | Marmon Aerospace & Defense LLC | Coated wire |
AT521301B1 (de) | 2018-05-29 | 2020-04-15 | Miba Ag | Stator mit Isolationsschicht |
US11688527B2 (en) * | 2020-08-07 | 2023-06-27 | Essex Furukawa Magnet Wire Usa Llc | Magnet wire with thermoplastic insulation |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5606152A (en) * | 1992-10-28 | 1997-02-25 | The Furukawa Electric Co., Ltd. | Multilayer insulated wire and a manufacturing method therefor |
US5483020A (en) * | 1994-04-12 | 1996-01-09 | W. L. Gore & Associates, Inc. | Twin-ax cable |
US6296935B1 (en) * | 1996-08-22 | 2001-10-02 | The Furukawa Electric Co., Ltd. | Multilayer insulated wire and transformer using the same |
US5861578A (en) * | 1997-01-27 | 1999-01-19 | Rea Magnet Wire Company, Inc. | Electrical conductors coated with corona resistant, multilayer insulation system |
DE19748529A1 (de) * | 1997-11-03 | 1999-03-04 | Siemens Ag | Elektrische Maschine mit Wickeldrähten |
US6392153B1 (en) * | 1998-12-18 | 2002-05-21 | Equistar Chemicals, Lp | Electrical conductive assembly |
TW412754B (en) * | 1999-02-12 | 2000-11-21 | Tai I Electric Wire & Cable Co | Anti-inrush varnished wire |
TW594799B (en) * | 2001-06-01 | 2004-06-21 | Furukawa Electric Co Ltd | Multilayer insulated wire and transformer using the same |
-
2005
- 2005-12-05 WO PCT/EP2005/056456 patent/WO2006061360A1/fr active Application Filing
- 2005-12-05 EP EP05850434A patent/EP1829059A1/fr not_active Withdrawn
- 2005-12-05 CN CNA2005800419283A patent/CN101073127A/zh active Pending
- 2005-12-05 US US11/792,307 patent/US20080128154A1/en not_active Abandoned
- 2005-12-05 JP JP2007543862A patent/JP2008523544A/ja not_active Abandoned
Non-Patent Citations (1)
Title |
---|
See references of WO2006061360A1 * |
Also Published As
Publication number | Publication date |
---|---|
US20080128154A1 (en) | 2008-06-05 |
WO2006061360A1 (fr) | 2006-06-15 |
JP2008523544A (ja) | 2008-07-03 |
CN101073127A (zh) | 2007-11-14 |
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