EP1466170A2 - Measuring and sensor assembly for determining a characteristic of a fluid and method for operating the same - Google Patents

Measuring and sensor assembly for determining a characteristic of a fluid and method for operating the same

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Publication number
EP1466170A2
EP1466170A2 EP02795239A EP02795239A EP1466170A2 EP 1466170 A2 EP1466170 A2 EP 1466170A2 EP 02795239 A EP02795239 A EP 02795239A EP 02795239 A EP02795239 A EP 02795239A EP 1466170 A2 EP1466170 A2 EP 1466170A2
Authority
EP
European Patent Office
Prior art keywords
sensor
measuring
fluid
capacitor
arrangement according
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP02795239A
Other languages
German (de)
French (fr)
Other versions
EP1466170B1 (en
Inventor
Mike Muhl
Jürgen HALL
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Testo SE and Co KGaA
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Testo SE and Co KGaA
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Application filed by Testo SE and Co KGaA filed Critical Testo SE and Co KGaA
Publication of EP1466170A2 publication Critical patent/EP1466170A2/en
Application granted granted Critical
Publication of EP1466170B1 publication Critical patent/EP1466170B1/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/02Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance
    • G01N27/22Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance by investigating capacitance
    • G01N27/221Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance by investigating capacitance by investigating the dielectric properties
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/02Food
    • G01N33/03Edible oils or edible fats

Definitions

  • Measuring arrangement and sensor arrangement for determining a property of a fluid and method for its operation Measuring arrangement and sensor arrangement for determining a property of a fluid and method for its operation.
  • the invention can be used in measurement technology, in particular when measuring the properties of fluids. Particularly in the case of oils, in particular in the case of liquid frying fats, certain properties can be determined on the basis of measurable dielectric properties by means of the present invention.
  • the invention relates to a measuring arrangement for determining a property, in particular the aging condition of a fluid, in particular a deep-frying fat, from a dielectric property of the fluid with a first sensor for measuring an electrical capacitance and with a second sensor for temperature measurement.
  • the invention relates to a sensor arrangement for measuring a dielectric property of a fluid with a dielectric sensor which can be immersed in the fluid and which has a measuring capacitor designed as a stray field capacitor.
  • oils used both for food and for industrial applications in mechanics are subject to an aging process which is determined, inter alia, by the influence of elevated temperatures. Various chemical reactions take place that change the quality of the respective oil. Often, the oil is first assessed based on the visual impression, i.e. the optical transmission or discoloration that decreases with time.
  • frying fat shows a loss of quality based on other parameters before a visible discoloration, which can lead to an exchange being necessary.
  • the decisive quality of an oil can be determined, for example, by chemical tests, also in connection with optical tests.
  • One difficulty here is the additional dependence of the dielectric constant on the temperature.
  • it can be provided, for example, to heat or cool an oil sample to a predetermined temperature in order to carry out a dielectric measurement at this temperature.
  • Such a measuring method is recognized, for example, in the US patent US 5818731 as prior art.
  • Measurement methods are also described there, by means of which an oil quality by means of several measured physical parameters ter should be determined, such as a dielectric parameter and the viscosity of the oil.
  • the measured dielectric constant is converted to the value at a standard temperature between 155 degrees Celsius and 185 degrees Celsius using a temperature measurement and a stored regression curve on the basis of the known temperature dependence. In conjunction with the measured transmission, this value should then allow a statement about the quality of the fat.
  • a disadvantage of the known measuring arrangements is that the measuring time is several minutes to about 10 minutes and that a certain amount of the oil used must be taken as a sample and tempered for the measurement. The sample container must be cleaned thoroughly before a new measurement.
  • the present invention is based on the object of creating a measuring arrangement and a sensor arrangement of the type mentioned at the outset, which are of simple construction and allow fast determination of the quality of the respective fluid with little construction effort and with simple and less complex operation.
  • the object is achieved in a measuring arrangement according to the invention in that the first sensor is designed as a dielectric sensor that is immersible in the fluid, has a stray field capacitor that serves as a measuring capacitor, and the second sensor is designed as a temperature sensor that is immersed in the fluid.
  • the dielectric constant and the temperature are measured, a statement about the state and the properties of the respective fluid can be derived.
  • the design of the sensors as immersible sensors allows measurement in situ without a sample having to be taken for filling in a measuring arrangement. This shortens the measurement time, on the one hand, with regard to the elimination of the need for sampling, and, on the other hand, by measuring at the temperature given in the fluid volume without a change in temperature. Although this makes the evaluation of the measured values more demanding, the measurement process itself can be carried out more easily and quickly.
  • the respective temperature at which measurements are being taken must be taken into account if the measured dielectric constant is used to derive a quality statement about the
  • Fluid is evaluated.
  • Such a measuring arrangement is easily transportable and can be used directly for measuring in containers in which the fluid is used, for example in fryers.
  • Such measuring arrangements can also be permanently installed or retrofitted in deep fryers for checking the frying fat used.
  • An advantageous embodiment of the invention provides that the first and the second sensor are connected to an evaluation device which in each case assigns a value of the property to be determined to a measured temperature value and a measured electrical capacitance value.
  • Either a computing algorithm or a value matrix can be stored in the evaluation device, by means of which a quality value of the fluid, for example an aging condition of a deep-frying fat, is assigned to the respectively measured temperature value and the measured capacitance value or the resulting dielectric constant.
  • a quality value of the fluid for example an aging condition of a deep-frying fat
  • the dielectric constant for example, previously empirically determined values from the dielectric constant and the temperature at which this was measured can be used to determine a concentration of certain polar constituents in the fluid, which in turn indicate the state of aging of the fluid.
  • a further advantageous embodiment of the invention provides that the value of the electrical capacitance measured by the dielectric sensor is compared in a comparison device of the evaluation device with a stored reference value assigned to the measured temperature value and a signal is output as a function of reaching or exceeding the reference value.
  • the evaluation device contains for each temperature value at which a measurement can be carried out, that is, for example, between 30 degrees Celsius and 200 degrees Celsius, at intervals of 0.5 degrees Celsius or 1 degree Celsius, a value of the measured capacitance or the value determined therefrom Dielectric constant, which is justifiable with regard to the resulting aging state of the fluid. If this value is exceeded as a reference value, after a comparison the evaluation device outputs a signal that warns the user, for example in the form of an optical or acoustic warning signal.
  • the invention can also be advantageously configured by a compensation device for correcting the measured value of the electrical capacitance, taking into account a reference measured value of a capacitance measured on an auxiliary capacitor arranged in the vicinity of the measuring capacitor.
  • the dielectric constant of the fluid is determined in that the influence of the fluid on the stray field capacitor serving as the measuring capacitor is determined when it is immersed in the fluid.
  • a high dielectric constant of the fluid results in an increase in the electrical capacitance of the measuring capacitor.
  • interfering influences can also occur when measuring the capacitance beyond the immersion of the measuring capacitor in the fluid.
  • there is also a capacitance between the leads of the measuring capacitor that can be changed by external influences. If the leads of the measuring capacitor are immersed in the fluid, the capacitance between them increases, too leads to a disturbance of the capacitance measurement to be carried out on the measuring capacitor itself.
  • an auxiliary capacitor is provided, the capacitance of which changes, for example, if the measuring capacitor is immersed too far in the fluid in the same sense as the capacitance of the leads of the measuring capacitor. If the capacitance of the auxiliary capacitor is monitored, an increase in the electrical capacitance of the auxiliary capacitor means that it is immersed in the fluid. This leads to a necessary compensation of the measurement on the measuring capacitor. The capacitance measured there is falsified by the effects on the supply line and must be compensated accordingly.
  • the compensation can also provide that when observing an increase in the capacitance of the auxiliary capacitor, the sensor is pulled out of the fluid to a certain extent until the capacitance of the auxiliary capacitor corresponds to the normal value. Then it is ensured that the leads of the measuring capacitor do not protrude into the fluid.
  • An advantageous embodiment of the invention also provides that in a sensor arrangement for measuring a dielectric property of a fluid with a dielectric sensor which is immersible in the fluid and which has a measuring capacitor designed as a stray field capacitor, the sensor has an auxiliary capacitor and that when it is introduced of the sensor in the fluid, the auxiliary capacitor is immersed in the fluid at the earliest when the measuring capacitor is completely immersed in the fluid.
  • Such a sensor arrangement can be used optimally for the measuring arrangement, which is also the subject of the present invention, in the sense described above. It can then be provided for the best possible compensation that supply lines of the measuring capacitor and the auxiliary capacitor are symmetrical and structurally identical to one another. They are then subject to the same interference in the same way.
  • the auxiliary capacitor consists of two stub lines ending in front of the measuring capacitor, which are designed and arranged in the same way as the leads of the measuring capacitor.
  • the symmetry of the leads of the measuring capacitor and the auxiliary capacitor can be used to optimally compensate for any interference that has a uniform effect on both leads, for example by subtracting the measured values.
  • a further advantageous embodiment of the sensor arrangement according to the invention provides that the measuring capacitor is formed by a plurality of flat conductor tracks, in particular in the form of an interdigital capacitor.
  • the sensor arrangement can, for example, be particularly simple in that the conductor tracks are printed on an insulating carrier using thin-film or thick-film technology.
  • the conductor tracks can, for example, be applied to a flat, but also to a round or cylindrical body.
  • the cylindrical shape is characterized by the fact that it is particularly space-saving, while the flat design requires a very short time for temperature compensation in the fluid due to the larger interaction area with the fluid.
  • the temperature sensor can advantageously be designed in the form of an NTC resistor, a PCT resistor or a temperature element.
  • the temperature sensor is connected to the dielectric sensor to form a structural unit.
  • the temperature sensor can for example be attached to the carrier for the conductor tracks of the measuring capacitor.
  • the use of the sensor arrangement or the measuring arrangement is simplified, since only a single probe with the two sensors has to be introduced into the fluid or into the frying fat.
  • the leads of the temperature sensor are applied to the insulating carrier in the form of conductor tracks.
  • This structural design makes the sensor arrangement particularly simple and inexpensive, and there is no interference with the capacitance measurements due to the leads of the temperature sensor.
  • the invention is shown on the basis of an exemplary embodiment in a drawing and then described. 1 schematically shows a measuring arrangement according to the invention in a first embodiment
  • FIG. 2 schematically, the measuring arrangement according to the invention in a second embodiment
  • FIGS. 3, 4, 5 different configurations of a dielectric sensor, in FIG. 5 with a temperature sensor.
  • FIG. 1 schematically shows a measuring arrangement which has a sensor arrangement 1 which is immersed in a fluid 2, for example a deep-frying fat.
  • the sensor arrangement 1 has a dielectric sensor and a temperature sensor, which are described in more detail below.
  • the sensor arrangement 1 is connected to a digital evaluation device 4 via electrical feed lines 3.
  • the evaluation device 4 has a first computing device 5, in which a capacitance, a dielectric constant or a value corresponding to this is determined from the measurement data.
  • the temperature of the fluid is determined in a second computing device 6 from the data supplied by the temperature sensor.
  • the value of the dielectric constant and the measured temperature are assigned a temperature-independent value of the dielectric constant, which represents an objective criterion for the condition of the fluid, in this case the aging condition of the frying fat.
  • This can, for example, be based on a fixed ratur related value.
  • This value determined in this way is shown in the display 8 and output to the user.
  • an interface for transferring the data to a further data processing device can also be provided.
  • FIG. 2 shows a measurement arrangement similar to that in FIG. 1, the same elements being designated with the same reference numerals as in FIG. 1.
  • the dielectric constant or a corresponding variable is determined in the first computing device.
  • the temperature is determined in the second computing device 6.
  • a specific dielectric constant or a corresponding value for example the measured capacitance for the frying fat to be measured, is assigned to the temperature on the basis of stored reference data for different temperature values.
  • the reference data are stored in a storage unit 9.
  • the value of the dielectric constant or the corresponding size determined by the first computing device 5 is compared in the comparison device 10 with the just still permissible reference size assigned by the second computing device 6 to the measured temperature.
  • the comparison is evaluated in such a way that if the two values match or the reference value is undershot, a corresponding first display device 11 is actuated, which indicates that the frying fat is still in order and can be used. If the dielectric constant or corresponding size determined by the first computing device 5 exceeds the assigned reference value, then the second display device 12 is confirmed, by which it is indicated that the frying fat is no longer used but should be replaced.
  • the first display device 11 can be designed, for example, as a green light, the second display device 12 as a red light.
  • the comparison device 10 can also be set up such that if the measured value for the dielectric constant matches the reference value, the frying fat is discarded and a necessary change is indicated by means of the second display device.
  • FIG. 3 shows part of the sensor arrangement 1 shown in FIGS. 1 and 2 in a side view.
  • FIG. 3 shows a flat ceramic carrier, 13, on which flat conductor tracks are printed using thin-film or thick-film technology.
  • the conductor tracks are advantageously made of precious metal, for example gold.
  • four feed lines are shown which are of the same design and run parallel to one another.
  • the right part of the illustration shows the measuring capacitor 14, which is designed in the form of a stray field capacitor with meandering interconnects.
  • the measuring capacitor is shown a second time in the circular enlarged detail and can be seen better there. It has two feed lines 15, 16 which lead from the measuring capacitor 14 to the first computing device 5 of the evaluation device 4.
  • the capacitance of the measuring capacitor 14 is dependent on the medium in which the measuring capacitor 14 is located, since the field lines penetrate its immediate surroundings. If, as shown in FIGS. 1 and 2, the measuring capacitor is immersed in a fluid 2 which has a higher dielectric constant than air, the capacitance of the measuring capacitor 14 increases considerably. The increase in the measured capacitance allows conclusions to be drawn about the dielectric constant of the medium surrounding the measuring capacitor 14.
  • the leads 17, 18 are provided on the ceramic carrier 13, which end as blind stub lines in front of the measuring capacitor 14 and which form an auxiliary capacitor, the capacitance of which is also monitored in the evaluation device 4. Changes in the surroundings of the leads 15, 16 of the measuring capacitor, which would falsify the capacitance measurement on the measuring capacitor 14, also change the measurement of the auxiliary capacitor, which is formed by the leads 17, 18.
  • the capacitance of the auxiliary capacitor By changing the capacitance of the auxiliary capacitor, the size of the disturbance can be determined and the disturbance of the measurement on the measuring capacitor can be compensated. This can become important, for example, if the sensor arrangement 1 is immersed so deeply in the fluid 2 that the supply lines 15, 16, 17, 18 are partially immersed in the fluid and thus the capacity of the supply lines is significantly increased.
  • This compensation which takes place in a compensation device 5a of the first computing unit 5, Solution of the dielectric constant of the fluid much less susceptible to errors and regardless of an ideal handling of the sensor arrangement.
  • the calibration of the measuring arrangement can also be carried out much less frequently than known measuring arrangements.
  • FIG. 4 shows an arrangement in which the two feed lines of the measuring capacitor 14 and the two blind ones
  • Stub lines of the auxiliary capacitor are arranged directly next to each other.
  • the distance between the feed lines is selected such that the total width of the feed lines running side by side and in parallel corresponds approximately to the width of the measuring capacitor 14.
  • FIG. 5 shows an arrangement in which the supply lines of the measuring capacitor 14 are arranged directly next to one another and likewise the stub lines are arranged directly next to one another and parallel to one another, but all four lines are very closely parallel to one another, which leads to an increase in the supply line capacity , This makes the arrangement more sensitive, for example, to whether the sensor is so deeply immersed in the fluid that the supply lines are already surrounded by the fluid.
  • a temperature sensor 19 in the form of a temperature element is shown schematically as an example. With this, when the measuring capacitor 14 is immersed, the temperature of the fluid is measured in its immediate vicinity.
  • the temperature sensor 19 is by means of two leads that run on the back of the ceramic carrier 13 and in the figure are not shown, connected to the evaluation device 4 and there to the second computing device 6 for determining the temperature.
  • the leads shown in FIGS. 3, 4 and 5 each end at the end of the ceramic carrier 13 with widened conductor track pieces 20, which can serve as plug contacts for a plug to be placed there, which forms the end of a flexible cable, the other end of which is connected to the evaluation device 4 connected is.
  • the flexible cable can be shielded accordingly to prevent influences on the capacitance of the capacitors' supply lines.
  • the measuring arrangement shown in conjunction with the sensor arrangement used for this purpose, gives short measuring times, high measuring accuracies and reduced calibration effort when determining the dielectric properties of oils, in particular frying fats.
  • the measuring device can also be used to determine other sizes of fluids related to the dielectric constant.

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
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  • Food Science & Technology (AREA)
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Abstract

The aim of the invention is to provide a simple and reliable method of measuring the quality of a fluid (2), in particular an oil or fat. This is achieved by a dielectric measurement in conjunction with a temperature measurement, which are carried out in situ by means of a measuring assembly and a sensor assembly (1) used with the latter, whereby the sensor assembly is submerged in the fluid. This permits information concerning the condition of the fluid, in particular concerning the age of the frying oil or fat, to be obtained in a rapid, low-cost manner.

Description

Beschreibungdescription
Messanordnung und Sensoranordnung zur Bestimmung einer Eigenschaft eines Fluides sowie Verfahren zu ihrem Betrieb.Measuring arrangement and sensor arrangement for determining a property of a fluid and method for its operation.
Die Erfindung ist in der Messtechnik einsetzbar und zwar insbesondere bei der Messung von Eigenschaften von Fluiden. Besonders bei Ölen, insbesondere bei flüssigen Frittierfetten, lassen sich bestimmte Eigenschaften aufgrund messbarer die- lektrischer Eigenschaften mittels der vorliegenden Erfindung bestimmen.The invention can be used in measurement technology, in particular when measuring the properties of fluids. Particularly in the case of oils, in particular in the case of liquid frying fats, certain properties can be determined on the basis of measurable dielectric properties by means of the present invention.
Die Erfindung bezieht sich auf eine Messanordnung zur Bestimmung einer Eigenschaft, insbesondere des Alterungszustandes eines Fluides insbesondere eines Frittierf ttes, aus einer dielektrischen Eigenschaft des Fluides mit einem ersten Sensor zur Messung einer elektrischen Kapazität und mit einem zweiten Sensor zur Temperaturmessung.The invention relates to a measuring arrangement for determining a property, in particular the aging condition of a fluid, in particular a deep-frying fat, from a dielectric property of the fluid with a first sensor for measuring an electrical capacitance and with a second sensor for temperature measurement.
Außerdem bezieht sich die Erfindung auf eine Sensoranordnung zur Messung einer dielektrischen Eigenschaft eines Fluides mit einem in das Fluid eintauchbaren dielektrischen Sensor, der einen als Streufeldkondensator ausgebildeten Messkondensator aufweist.In addition, the invention relates to a sensor arrangement for measuring a dielectric property of a fluid with a dielectric sensor which can be immersed in the fluid and which has a measuring capacitor designed as a stray field capacitor.
Es ist bekannt, dass sowohl für Speisezwecke verwendete als auch für industrielle Anwendungen in der Mechanik verwendete Öle einem Alterungsprozess unterliegen, der unter anderem durch den Einfluss erhöhter Temperaturen bestimmt ist. Es finden verschiedene chemische Reaktionen statt, die die Qualität des jeweiligen Öls verändern. Oft findet eine Begutachtung des Öls zunächst aufgrund des optischen Eindrucks, das heißt der mit der Zeit abnehmenden optischen Transmission oder Verfärbung statt.It is known that oils used both for food and for industrial applications in mechanics are subject to an aging process which is determined, inter alia, by the influence of elevated temperatures. Various chemical reactions take place that change the quality of the respective oil. Often, the oil is first assessed based on the visual impression, i.e. the optical transmission or discoloration that decreases with time.
Diese Größe stellt jedoch nur einen einzelnen Parameter dar, der zur Beurteilung der Qualität im allgemeinen unzureichend ist.However, this quantity represents only a single parameter, which is generally insufficient to assess the quality.
Beispielsweise lässt Frittierfett schon vor einer sichtbaren Verfärbung anhand anderer Parameter einen Qualitätsverlust erkennen, der dazu führen kann, dass ein Austausch notwendig wird.For example, frying fat shows a loss of quality based on other parameters before a visible discoloration, which can lead to an exchange being necessary.
Die maßgebliche Qualität eines Öls kann beispielsweise durch chemische Tests, auch in Verbindung mit optischen Tests festgestellt werden.The decisive quality of an oil can be determined, for example, by chemical tests, also in connection with optical tests.
Seit einiger Zeit ist auch die Möglichkeit bekannt, den Alterungszustand eines Öls anhand der gemessenen Dielektrizi- tätskonstante zu beurteilen.For some time now, the possibility has also been known of assessing the aging condition of an oil on the basis of the measured dielectric constant.
Eine Schwierigkeit stellt dabei die zusätzliche Abhängigkeit der Dielektrizitätskonstante von der Temperatur dar. Es kann zur Lösung dieses Problems beispielsweise vorgesehen sein, eine Ölprobe auf eine fest vorgegebene Temperatur zu erhitzen oder abzukühlen, um bei dieser Temperatur eine Dielektrizi- tätsmessung durchzuführen. Eine derartige Meßmethode ist beispielsweise in der US-Patentschrift US 5818731 als Stand der Technik gewürdigt.One difficulty here is the additional dependence of the dielectric constant on the temperature. To solve this problem, it can be provided, for example, to heat or cool an oil sample to a predetermined temperature in order to carry out a dielectric measurement at this temperature. Such a measuring method is recognized, for example, in the US patent US 5818731 as prior art.
Dort sind außerdem Meßmethoden beschrieben, durch die eine Ölqualität mittels mehrerer gemessener physikalischer Parame- ter bestimmt werden soll, wie beispielsweise einer dielektrischen Messgröße und der Viskosität des Öls.Measurement methods are also described there, by means of which an oil quality by means of several measured physical parameters ter should be determined, such as a dielectric parameter and the viscosity of the oil.
Da die Farbe eines Frittierfettes eine der sensitivsten Grö- ßen für die Bestimmung der Qualität ist, wird gemäß der US- Patentschrift 5818731 vorgeschlagen, eine Dielektrizitätsmes- sung mit einer Messung der optischen Transmission in einem bestimmten Wellenlängenbereich zu verbinden, um eine umfassende Bewertung der Ölqualität durchzuführen. Dazu wird eine Ölprobe in einen Messbehälter gefüllt und dort mit Licht aus einer Laserdiode mit Licht der Wellenlänge 675 Nanometer bestrahlt, um die Transmission in diesem Wellenlängenbereich zu messen. Außerdem wird mittels eines Messkondensators die Dielektrizitätskonstante gemessen. Die Messung findet dort statt, nachdem die Probe auf eine Temperatur zwischen 155 Grad Celsius und 185 Grad Celsius aufgeheizt worden ist. Nachdem die Dielektrizitätsmessung durchgeführt worden ist, wird mit Hilfe einer Temperaturmessung und einer gespeicherten Regressionskurve die gemessene Dielektrizitätskonstante aufgrund der bekannten Temperaturabhängigkeit auf den Wert bei einer Standardtemperatur zwischen 155 Grad Celsius und 185 Grad Celsius umgerechnet. Dieser Wert soll dann in Verbindung mit der gemessenen Transmission eine Aussage über die Qualität des Fettes erlauben.Since the color of a frying fat is one of the most sensitive parameters for determining the quality, it is proposed according to US Pat. No. 5,818,731 to combine a dielectric measurement with a measurement of the optical transmission in a specific wavelength range in order to carry out a comprehensive evaluation of the oil quality perform. For this purpose, an oil sample is filled into a measuring container and irradiated there with light from a laser diode with light of the wavelength 675 nanometers in order to measure the transmission in this wavelength range. In addition, the dielectric constant is measured using a measuring capacitor. The measurement takes place after the sample has been heated to a temperature between 155 degrees Celsius and 185 degrees Celsius. After the dielectric measurement has been carried out, the measured dielectric constant is converted to the value at a standard temperature between 155 degrees Celsius and 185 degrees Celsius using a temperature measurement and a stored regression curve on the basis of the known temperature dependence. In conjunction with the measured transmission, this value should then allow a statement about the quality of the fat.
Ein Nachteil der bekannten Messanordnungen ist, dass die Messdauer mehrere Minuten bis etwa 10 Minuten beträgt und dass zur Messung eine bestimmte Menge des verwendeten Öles als Probe entnommen und temperiert werden muss . Vor einer neuen Messung muss der Probenbehälter gründlich gereinigt werden. Der vorliegenden Erfindung liegt demgegenüber die Aufgabe zugrunde, eine Messanordnung und eine Sensoranordnung der eingangs genannten Art zu schaffen, die einfach aufgebaut sind und mit geringem konstruktiven Aufwand sowie bei einfa- eher und wenig aufwendiger Bedienung eine schnelle Bestimmung der Qualität des jeweiligen Fluides erlauben.A disadvantage of the known measuring arrangements is that the measuring time is several minutes to about 10 minutes and that a certain amount of the oil used must be taken as a sample and tempered for the measurement. The sample container must be cleaned thoroughly before a new measurement. In contrast, the present invention is based on the object of creating a measuring arrangement and a sensor arrangement of the type mentioned at the outset, which are of simple construction and allow fast determination of the quality of the respective fluid with little construction effort and with simple and less complex operation.
Die Aufgabe wird bei einer Messanordnung gemäß der Erfindung dadurch gelöst, dass der erste Sensor als ein in das Fluid eintauchbarer, einen als Messkondensator dienenden Streufeldkondensator aufweisender dielektrischer Sensor und der zweite Sensor als in das Fluid eintauchbarer Temperatursensor ausgebildet ist.The object is achieved in a measuring arrangement according to the invention in that the first sensor is designed as a dielectric sensor that is immersible in the fluid, has a stray field capacitor that serves as a measuring capacitor, and the second sensor is designed as a temperature sensor that is immersed in the fluid.
Dadurch, dass die Dielektrizitätskonstante und die Temperatur gemessen wird, ist grundsätzlich eine Aussage über den Zustand und die Eigenschaften des jeweiligen Fluids ableitbar. Die Ausführung der Sensoren als eintauchbare Sensoren erlaubt die Messung in situ, ohne dass eine Probe zur Einfüllung in eine Messanordnung entnommen werden muss. Dadurch wird die Messzeit verkürzt einerseits hinsichtlich der entfallenden Notwendigkeit der Probenentnahme, andererseits dadurch, dass bei der in dem Fluidvolumen gegebenen Temperatur ohne eine Temperaturänderung gemessen wird. Dadurch wird zwar die Auswertung der Messwerte anspruchsvoller, jedoch wird der Mess- vorgang selbst einfacher und schneller ausführbar. Bei der Auswertung muss die jeweilige Temperatur, bei der gemessen wird, berücksichtigt werden, wenn die gemessene Dielektrizi- tätskonstante zur Ableitung einer Qualitätsaussage über dasBecause the dielectric constant and the temperature are measured, a statement about the state and the properties of the respective fluid can be derived. The design of the sensors as immersible sensors allows measurement in situ without a sample having to be taken for filling in a measuring arrangement. This shortens the measurement time, on the one hand, with regard to the elimination of the need for sampling, and, on the other hand, by measuring at the temperature given in the fluid volume without a change in temperature. Although this makes the evaluation of the measured values more demanding, the measurement process itself can be carried out more easily and quickly. When evaluating, the respective temperature at which measurements are being taken must be taken into account if the measured dielectric constant is used to derive a quality statement about the
Fluid ausgewertet- wird. Eine derartige Messanordnung ist leicht transportabel und kann zur Messung in Behältern, in denen das Fluid verwendet wird beispielsweise in Friteusen, direkt verwendet werden. Derartige Messanordnungen können auch dauerhaft in Friteusen zur Überprüfung des verwendeten Frittierfettes eingebaut werden beziehungsweise nachgerüstet werden.Fluid is evaluated. Such a measuring arrangement is easily transportable and can be used directly for measuring in containers in which the fluid is used, for example in fryers. Such measuring arrangements can also be permanently installed or retrofitted in deep fryers for checking the frying fat used.
Eine vorteilhafte Ausgestaltung der Erfindung sieht vor, dass der erste und der zweite Sensor mit einer Auswerteeinrichtung verbunden sind, die jeweils einem gemessenen Temperaturwert und einem gemessenen elektrischen Kapazitätswert einen Wert der zu bestimmenden Eigenschaft zuordnet.An advantageous embodiment of the invention provides that the first and the second sensor are connected to an evaluation device which in each case assigns a value of the property to be determined to a measured temperature value and a measured electrical capacitance value.
In der Auswerteeinrichtung kann entweder ein Rechnenalgo- rithmus oder eine Wertematrix hinterlegt sein, mittels deren dem jeweils gemessen Temperaturwert und dem gemessenen Kapazitätswert beziehungsweise der daraus sich ergebenden Dielektrizitätskonstante ein Qualitätswert des Fluides, beispielsweise ein Alterungszustand eines Frittierfettes zuge- ordnet wird. Beispielsweise kann mittels vorher empirisch ermittelter Werte aus der Dielektrizitätskonstanten und der Temperatur, bei der diese gemessen wurde, eine Konzentration von bestimmten polaren Stoffanteilen in dem Fluid bestimmt werden, die ihrerseits auf den Alterungszustand des Fluids schließen lassen.Either a computing algorithm or a value matrix can be stored in the evaluation device, by means of which a quality value of the fluid, for example an aging condition of a deep-frying fat, is assigned to the respectively measured temperature value and the measured capacitance value or the resulting dielectric constant. For example, previously empirically determined values from the dielectric constant and the temperature at which this was measured can be used to determine a concentration of certain polar constituents in the fluid, which in turn indicate the state of aging of the fluid.
Eine weitere vorteilhafte Ausgestaltung der Erfindung sieht vor, dass in einer Vergleichseinrichtung der Auswerteeinrichtung der jeweils durch den dielektrischen Sensor gemessene Wert der elektrischen Kapazität mit einem dem gemessenen Temperaturwert zugeordneten gespeicherten Referenzwert verglichen und in Abhängigkeit vom Erreichen oder Überschreiten des Referenzwertes ein Signal ausgegeben wird. In diesem Fall enthält die Auswerteeinrichtung für jeden Temperaturwert, bei dem eine Messung durchgeführt werden kann, also beispielsweise zwischen 30 Grad Celsius und 200 Grad Celsius, in Abständen von 0,5 Grad Celsius oder 1 Grad Celsius einen Wert der gemessenen Kapazität beziehungsweise der daraus ermittelten Dielektrizitätskonstante, der bezüglich des sich ergebenden Alterungszustandes des Fluides gerade noch vertretbar ist. Wird dieser Wert als Referenzwert über- schritten, so gibt die Auswerteeinrichtung nach einem Vergleich ein Signal aus, das den Benutzer warnt, beispielsweise in Form eines optischen oder akustischen Warnsignals.A further advantageous embodiment of the invention provides that the value of the electrical capacitance measured by the dielectric sensor is compared in a comparison device of the evaluation device with a stored reference value assigned to the measured temperature value and a signal is output as a function of reaching or exceeding the reference value. In this case, the evaluation device contains for each temperature value at which a measurement can be carried out, that is, for example, between 30 degrees Celsius and 200 degrees Celsius, at intervals of 0.5 degrees Celsius or 1 degree Celsius, a value of the measured capacitance or the value determined therefrom Dielectric constant, which is justifiable with regard to the resulting aging state of the fluid. If this value is exceeded as a reference value, after a comparison the evaluation device outputs a signal that warns the user, for example in the form of an optical or acoustic warning signal.
Die Erfindung kann außerdem vorteilhaft ausgestaltet sein durch eine Kompensationseinrichtung zur Korrektur des Mess- wertes der elektrischen Kapazität unter Berücksichtigung eines an einem in der Nähe des Messkondensators angeordneten Hilfskondensator gemessenen Referenzmesswertes einer Kapazität.The invention can also be advantageously configured by a compensation device for correcting the measured value of the electrical capacitance, taking into account a reference measured value of a capacitance measured on an auxiliary capacitor arranged in the vicinity of the measuring capacitor.
Die Dielektrizitätskonstante des Fluids wird dadurch bestimmt, dass der Einfluss des Fluids auf den als Messkondensator dienenden Streufeldkondensator bestimmt wird, wenn dieser in das Fluid eingetaucht ist. Durch eine hohe Dielektri- zitätskonstante des Fluids ergibt sich eine Vergrößerung der elektrischen Kapazität des Messkondensators. Dabei ist jedoch zu berücksichtigen, dass auch über das Eintauchen des Messkondensators in das Fluid hinaus störende Einflüsse bei der Messung der Kapazität auftreten können. Beispielsweise be- steht auch zwischen den Zuleitungen des Messkondensators eine Kapazität, die durch- äußere Einflüsse geändert werden kann. Tauchen die Zuleitungen des Messkondensators in das Fluid ein, so erhöht sich auch zwischen ihnen die Kapazität, was zu einer Störung der durchzuführenden Kapazitätsmessung an dem Messkondensator selbst führt. Aus diesem Grund ist ein Hilfskondensator vorgesehen, dessen Kapazität sich beispielsweise bei einem zu weiten Eintauchen des Messkondensators in das Fluid in dem selben Sinn ändert, wie die Kapazität der Zuleitungen des Messkondensators. Wird die Kapazität des Hilfskondensators überwacht, so ergibt eine Erhöhung der elektrischen Kapazität des Hilfskondensators, dass dieser in das Fluid eingetaucht ist. Dies führt zu einer notwendigen Kompensation der Messung am Messkondensator. Die dort gemessene Kapazität ist durch die Einwirkungen auf die Zuleitung verfälscht und muss entsprechend kompensiert werden.The dielectric constant of the fluid is determined in that the influence of the fluid on the stray field capacitor serving as the measuring capacitor is determined when it is immersed in the fluid. A high dielectric constant of the fluid results in an increase in the electrical capacitance of the measuring capacitor. However, it must be taken into account here that interfering influences can also occur when measuring the capacitance beyond the immersion of the measuring capacitor in the fluid. For example, there is also a capacitance between the leads of the measuring capacitor that can be changed by external influences. If the leads of the measuring capacitor are immersed in the fluid, the capacitance between them increases, too leads to a disturbance of the capacitance measurement to be carried out on the measuring capacitor itself. For this reason, an auxiliary capacitor is provided, the capacitance of which changes, for example, if the measuring capacitor is immersed too far in the fluid in the same sense as the capacitance of the leads of the measuring capacitor. If the capacitance of the auxiliary capacitor is monitored, an increase in the electrical capacitance of the auxiliary capacitor means that it is immersed in the fluid. This leads to a necessary compensation of the measurement on the measuring capacitor. The capacitance measured there is falsified by the effects on the supply line and must be compensated accordingly.
Die Kompensation kann auch vorsehen, dass bei der Beobachtung einer Erhöhung der Kapazität des Hilfskondensators der Sensor aus dem Fluid ein Stück weit herausgezogen wird, bis die Kapazität des Hilfskondensators dem Normalwert entspricht. Dann ist' sichergestellt, dass auch die Zuleitungen des Messkondensators nicht in das Fluid hineinragen.The compensation can also provide that when observing an increase in the capacitance of the auxiliary capacitor, the sensor is pulled out of the fluid to a certain extent until the capacitance of the auxiliary capacitor corresponds to the normal value. Then it is ensured that the leads of the measuring capacitor do not protrude into the fluid.
Aber auch andere Umgebungseinflüsse auf die Zuleitungen des Messkondensators beziehungsweise auf den Messkondensator selbst, beispielsweise Temperatureinflüsse, die über die Abhängigkeit der Dielektrizitätskonstanten des Fluids von der Temperatur hinausgehen, können durch die Einbeziehung des Verhaltens des Hilfskondensators kompensiert werden.However, other environmental influences on the leads of the measuring capacitor or on the measuring capacitor itself, for example temperature influences that go beyond the dependence of the dielectric constant of the fluid on the temperature, can be compensated for by including the behavior of the auxiliary capacitor.
Eine vorteilhafte Ausgestaltung der Erfindung sieht außerdem vor, dass bei einer Sensoranordnung zur Messung einer die- lektrischen Eigenschaft eines Fluides mit einem in das Fluid eintauchbaren dielektrischen Sensor, der einen als Streufeldkondensator ausgebildeten Messkondensator aufweist, der Sensor einen Hilfskondensator aufweist und dass beim Einbringen des Sensors in das Fluid der Hilfskondensator frühestens dann in das Fluid eintaucht, wenn der Messkondensator in das Fluid völlig eingetaucht ist.An advantageous embodiment of the invention also provides that in a sensor arrangement for measuring a dielectric property of a fluid with a dielectric sensor which is immersible in the fluid and which has a measuring capacitor designed as a stray field capacitor, the sensor has an auxiliary capacitor and that when it is introduced of the sensor in the fluid, the auxiliary capacitor is immersed in the fluid at the earliest when the measuring capacitor is completely immersed in the fluid.
Eine derartige Sensoranordnung ist in dem oben geschilderten Sinne optimal für die Messanordnung die ebenfalls Gegenstand der vorliegenden Erfindung ist, zu verwenden. Es kann dann für eine möglichst gute Kompensation vorgesehen sein, dass Zuleitungen des Messkondensators und des Hil skondensators symmetrisch und baugleich zueinander ausgebildet sind. Sie unterliegen dann denselben Störungseinflüssen in derselben Weise.Such a sensor arrangement can be used optimally for the measuring arrangement, which is also the subject of the present invention, in the sense described above. It can then be provided for the best possible compensation that supply lines of the measuring capacitor and the auxiliary capacitor are symmetrical and structurally identical to one another. They are then subject to the same interference in the same way.
Außerdem kann die erfindungsgemäße Sensoranordnung so ausgestaltet sein, dass der Hilfskondensator aus zwei vor dem Mess- kondensator endenden Stichleitungen besteht, die gleichartig wie die Zuleitungen des Messkondensators ausgebildet und angeordnet sind. Durch die Symmetrie der Zuleitungen des Mess- kondensators und des Hilfskondensators können eventuelle Störeinflüsse, die auf beide Zuleitungen gleichmäßig wirken, optimal kompensiert werden, beispielsweise durch Subtraktion der Messwerte.In addition, the sensor arrangement according to the invention can be designed such that the auxiliary capacitor consists of two stub lines ending in front of the measuring capacitor, which are designed and arranged in the same way as the leads of the measuring capacitor. The symmetry of the leads of the measuring capacitor and the auxiliary capacitor can be used to optimally compensate for any interference that has a uniform effect on both leads, for example by subtracting the measured values.
Eine weitere vorteilhafte Ausgestaltung der erfindungsgemäßen Sensoranordnung sieht vor, dass der Messkondensator durch ei- ne Mehrzahl von flachen Leiterbahnen insbesondere in Form eines Interdigitalkondensators gebildet ist.A further advantageous embodiment of the sensor arrangement according to the invention provides that the measuring capacitor is formed by a plurality of flat conductor tracks, in particular in the form of an interdigital capacitor.
Die Sensoranordnung kann beispielsweise dadurch besonders einfach aufgebaut sein, dass die Leiterbahnen in Dünnschicht- oder Dickschichttechnik auf einen isolierenden Träger aufgedruckt sind. Die Leiterbahnen können beispielsweise auf einen flachen, jedoch auch auf einen runden oder zylindrischen Körper aufgebracht sein.The sensor arrangement can, for example, be particularly simple in that the conductor tracks are printed on an insulating carrier using thin-film or thick-film technology. The conductor tracks can, for example, be applied to a flat, but also to a round or cylindrical body.
Die zylindrische Form zeichnet sich dadurch aus, dass sie besonders platzsparend ist, während die flache Bauform durch die größere Interaktionsfläche mit dem Fluid eine sehr geringe Zeit zum Temperaturausgleich in dem Fluid benötigt .The cylindrical shape is characterized by the fact that it is particularly space-saving, while the flat design requires a very short time for temperature compensation in the fluid due to the larger interaction area with the fluid.
Vorteilhaft kann bei der erfindungsgemäßen Sensoranordnung der Temperatursensor in Form eines NTC-Widerstandes, eines PCT-Widerstandes oder eines Temperaturelementes ausgeführt sein. Diese Temperatursensoren sind kostengünstig, gut eichbar und widerstandsfähig sowie in ihrem Verhalten stabil, so dass die gesamte Sensoranordnung nicht allzu häufig kalibriert werden muss .In the sensor arrangement according to the invention, the temperature sensor can advantageously be designed in the form of an NTC resistor, a PCT resistor or a temperature element. These temperature sensors are inexpensive, easily calibrated and resistant, and their behavior is stable, so that the entire sensor arrangement does not have to be calibrated too often.
Es erweist sich als günstig, wenn der Temperatursensor mit dem dielektrischen Sensor zu einer konstruktiven Einheit ver- bunden ist. Der Temperatursensor kann beispielsweise an dem Träger für die Leiterbahnen des Messkondensators befestigt sein. In diesem Falle vereinfacht sich die Verwendung der Sensoranordnung beziehungsweise der Messanordnung, da nur eine einzige Sonde mit den beiden Sensoren in das Fluid bezie- hungsweise in das Frittierfett eingebracht werden muss.It has proven to be advantageous if the temperature sensor is connected to the dielectric sensor to form a structural unit. The temperature sensor can for example be attached to the carrier for the conductor tracks of the measuring capacitor. In this case, the use of the sensor arrangement or the measuring arrangement is simplified, since only a single probe with the two sensors has to be introduced into the fluid or into the frying fat.
Als vorteilhaft ergibt sich außerdem, dass die Zuleitungen des Temperatursensors auf den isolierenden Träger in Form von Leiterbahnen aufgebracht sind. Durch diese bauliche Ausfüh- rung ist die Sensoranordnung besonders einfach und kostengünstig aufgebaut und es ergibt sich durch die Zuleitungen des Temperatursensors auch keine Störung bei den Kapazitäts- messungen. Im folgenden wird die Erfindung anhand eines Ausführungsbei- spiels in einer Zeichnung gezeigt und anschließend beschrieben. Dabei zeigt Figur 1 schematisch eine erfindungsgemäße Messanordnung in einer ersten Ausführung,It is also advantageous that the leads of the temperature sensor are applied to the insulating carrier in the form of conductor tracks. This structural design makes the sensor arrangement particularly simple and inexpensive, and there is no interference with the capacitance measurements due to the leads of the temperature sensor. In the following, the invention is shown on the basis of an exemplary embodiment in a drawing and then described. 1 schematically shows a measuring arrangement according to the invention in a first embodiment,
Figur 2 schematisch die erfindungsgemäße Messanordnung in einer zweiten Ausführung,FIG. 2 schematically, the measuring arrangement according to the invention in a second embodiment,
Figuren 3, 4, 5 verschiedene Ausgestaltungen eines dielektri- sehen Sensors, in Figur 5 mit einem Temperatursensor.FIGS. 3, 4, 5 different configurations of a dielectric sensor, in FIG. 5 with a temperature sensor.
In der Figur 1 ist schematisch eine Messanordnung dargestellt, die eine Sensoranordnung 1 aufweist, die in ein Fluid 2, beispielsweise ein Frittierfett eingetaucht ist. Die Sen- soranordnung 1 weist einen dielektrischen Sensor sowie einen Temperatursensor auf, die weiter unten näher beschrieben werden.FIG. 1 schematically shows a measuring arrangement which has a sensor arrangement 1 which is immersed in a fluid 2, for example a deep-frying fat. The sensor arrangement 1 has a dielectric sensor and a temperature sensor, which are described in more detail below.
Die Sensoranordnung 1 ist über elektrische Zuleitungen 3 mit einer digitalen Auswerteeinrichtung 4 verbunden. Die Auswerteeinrichtung 4 weist eine erste Recheneinrichtung 5 auf, in der aus den Messdaten eine Kapazität, eine Dielektrizitätskonstante oder ein dieser entsprechender Wert bestimmt wird. In einer zweiten Recheneinrichtung 6 wird aus den von dem Temperatursensor gelieferten Daten die Temperatur des Fluids bestimmt .The sensor arrangement 1 is connected to a digital evaluation device 4 via electrical feed lines 3. The evaluation device 4 has a first computing device 5, in which a capacitance, a dielectric constant or a value corresponding to this is determined from the measurement data. The temperature of the fluid is determined in a second computing device 6 from the data supplied by the temperature sensor.
In einer dritten Recheneinrichtung 7 wird dem Wert der Die- lektizitätskonstante und der gemessenen Temperatur ein tempe- raturunabhängiger Wert der Dielektrizitätskonstante zugeordnet, der ein objektives Kriterium für den Zustand des Fluides, in diesem Fall den Alterungszustand des Frittierfettes darstellt. Dies kann beispielsweise ein auf eine feste Tempe- ratur bezogener Wert sein. Dieser so bestimmte Wert wird in der Anzeige 8 dargestellt und an den Benutzer ausgegeben. Anstelle der Anzeige 8 kann auch ein Interface zur Übergabe der Daten an ein weiteres Datenverarbeitungsgerät vorgesehen sein.In a third computing device 7, the value of the dielectric constant and the measured temperature are assigned a temperature-independent value of the dielectric constant, which represents an objective criterion for the condition of the fluid, in this case the aging condition of the frying fat. This can, for example, be based on a fixed ratur related value. This value determined in this way is shown in the display 8 and output to the user. Instead of the display 8, an interface for transferring the data to a further data processing device can also be provided.
In der Figur 2 ist eine ähnliche Messanordnung wie in Figur 1 dargestellt, wobei gleiche Elemente mit dem selben Bezugszeichen bezeichnet sind wie in der Figur 1.FIG. 2 shows a measurement arrangement similar to that in FIG. 1, the same elements being designated with the same reference numerals as in FIG. 1.
Ebenso wie in dem oben beschriebenen Beispiel wird in der ersten Recheneinrichtung die Dielektrizitätskonstante oder eine entsprechende Größe bestimmt. In der zweiten Recheneinrichtung 6 wird die Temperatur bestimmt.As in the example described above, the dielectric constant or a corresponding variable is determined in the first computing device. The temperature is determined in the second computing device 6.
Zusätzlich wird in der zweiten Recheneinrichtung 6 der Temperatur aufgrund von gespeicherten Referenzdaten für verschiedene Temperaturwerte eine bestimmte, bei der jeweiligen Temperatur gerade noch zulässige Dielektrizitätskonstante oder ein entsprechender Wert, beispielsweise die gemessene Kapazität für das zu vermessende Frittierfett zugeordnet. Die Referenzdaten sind in einer Speichereinheit 9 gespeichert. Der durch die erste Recheneinrichtung 5 bestimmte Wert der Dielektrizitätskonstante oder der entsprechenden Größe wird mit dem durch die zweite Recheneinrichtung 6 der gemessenen Temperatur zugeordneten gerade noch zulässigen Referenzgröße in der Vergleichseinrichtung 10 verglichen. Der Vergleich wird derart bewertet, dass bei einer Übereinstimmung der beiden Werte oder einer Unterschreitung des Referenzwertes eine ent- sprechende erste Anzeigeeinrichtung 11 betätigt wird, die anzeigt,- dass das Frittierfett noch in Ordnung und verwendbar ist . Übersteigt die durch die erste Recheneinrichtung 5 bestimmte Dielektrizitätskonstante oder entsprechende Größe den zugeordneten Referenzwert, so wird die zweite Anzeigeeinrichtung 12 bestätigt, durch die angezeigt wird, dass das Frittierfett nicht mehr verwendet, sondern ausgetauscht werden soll.In addition, in the second computing device 6, a specific dielectric constant or a corresponding value, for example the measured capacitance for the frying fat to be measured, is assigned to the temperature on the basis of stored reference data for different temperature values. The reference data are stored in a storage unit 9. The value of the dielectric constant or the corresponding size determined by the first computing device 5 is compared in the comparison device 10 with the just still permissible reference size assigned by the second computing device 6 to the measured temperature. The comparison is evaluated in such a way that if the two values match or the reference value is undershot, a corresponding first display device 11 is actuated, which indicates that the frying fat is still in order and can be used. If the dielectric constant or corresponding size determined by the first computing device 5 exceeds the assigned reference value, then the second display device 12 is confirmed, by which it is indicated that the frying fat is no longer used but should be replaced.
Die erste Anzeigeeinrichtung 11 kann beispielsweise als grüne Leuchte, die zweite Anzeigeeinrichtung 12 als rote Leuchte ausgestaltet sein. Die Vergleichseinrichtung 10 kann auch so eingerichtet sein, dass bereits bei einer Übereinstimmung des gemessenen Wertes für die Dielektrizitätskonstante mit dem Referenzwert das Frittierfett verworfen und ein notwendiger Wechsel mittels der zweiten Anzeigeeinrichtung angezeigt wird.The first display device 11 can be designed, for example, as a green light, the second display device 12 as a red light. The comparison device 10 can also be set up such that if the measured value for the dielectric constant matches the reference value, the frying fat is discarded and a necessary change is indicated by means of the second display device.
Im folgenden soll genauer die Gewinnung der Messwerte für die Dielektrizitätskonstante und die Temperatur beschrieben werden. Dabei wird zunächst auf die Figuren 3, 4 und 5 bezug genommen. In der Figur 3 ist ein Teil der in den Figuren 1 und 2 dargestellten Sensoranordnung 1 in einer Seitenansicht dar- gestellt. Die Figur 3 zeigt einen flachen Keramikträger, 13, auf den flache Leiterbahnen mittels Dünnschicht- oder Dickschichttechnik aufgedruckt sind. Die Leiterbahnen bestehen vorteilhaft aus Edelmetall, zum Beispiel Gold. Im linken Teil der Darstellung sind vier Zuleitungen gezeigt, die gleichar- tig ausgebildet sind und parallel zueinander verlaufen.The acquisition of the measured values for the dielectric constant and the temperature will be described in more detail below. Reference is first made to FIGS. 3, 4 and 5. FIG. 3 shows part of the sensor arrangement 1 shown in FIGS. 1 and 2 in a side view. FIG. 3 shows a flat ceramic carrier, 13, on which flat conductor tracks are printed using thin-film or thick-film technology. The conductor tracks are advantageously made of precious metal, for example gold. In the left part of the illustration, four feed lines are shown which are of the same design and run parallel to one another.
Im rechten Teil der Darstellung ist der Messkondensator 14 dargestellt, der in Form eines Streufeldkondensators mit mä- anderförmig ineinander verschlungenen Leiterbahnen ausgebil- det ist. Der Messkondensator ist in der kreisförmig dargestellten Detailvergrößerung ein- zweites Mal gezeigt und dort besser zu erkennen. Er weist zwei Zuleitungen 15, 16 auf, die von dem Messkondensator 14 bis zu der ersten Recheneinrichtung 5 der Auswerteeinrichtung 4 führen.The right part of the illustration shows the measuring capacitor 14, which is designed in the form of a stray field capacitor with meandering interconnects. The measuring capacitor is shown a second time in the circular enlarged detail and can be seen better there. It has two feed lines 15, 16 which lead from the measuring capacitor 14 to the first computing device 5 of the evaluation device 4.
Die Kapazität des Messkondensators 14 ist, da die Feldlinien dessen unmittelbare Umgebung durchsetzen, von dem Medium abhängig, in dem der Messkondensator 14 sich befindet. Wird der Messkondensator, wie in den Figuren 1 und 2 dargestellt, in ein Fluid 2 eingetaucht, das eine höhere Dielektrizitätskonstante aufweist als Luft, so vergrößert sich die Kapa- zität des Messkondensators 14 erheblich. Von der Vergrößerung der gemessenen Kapazität kann auf die Dielektrizitätskonstante des den Messkondensator 14 umgebenden Mediums geschlossen werden .The capacitance of the measuring capacitor 14 is dependent on the medium in which the measuring capacitor 14 is located, since the field lines penetrate its immediate surroundings. If, as shown in FIGS. 1 and 2, the measuring capacitor is immersed in a fluid 2 which has a higher dielectric constant than air, the capacitance of the measuring capacitor 14 increases considerably. The increase in the measured capacitance allows conclusions to be drawn about the dielectric constant of the medium surrounding the measuring capacitor 14.
Außer den Zuleitungen 15, 16 des Messkondensators sind auf dem Keramikträger 13 die Zuleitungen 17, 18 vorgesehen, die als blinde Stichleitungen vor dem Messkondensator 14 enden und die einen Hilfskondensator bilden, dessen Kapazität in der Auswerteeinrichtung 4 ebenfalls überwacht wird. Änderun- gen der Umgebung der Zuleitungen 15, 16 des Messkondensators, die die Kapazitätsmessung an dem Messkondensator 14 verfälschen würden, verändern ebenfalls die Messung des Hilfskondensators, der durch die Zuleitungen 17, 18 gebildet ist. Durch die Änderung der Kapazität des Hilfskondensators kann die Größe der Störung bestimmt und die Störung der Messung an dem Messkondensator kompensiert werden. Dies kann zum Beispiel dann wichtig werden, wenn die Sensoranordnung 1 so tief in das Fluid 2 eingetaucht wird, dass die Zuleitungen 15, 16, 17, 18 zu einem Teil in das Fluid eintauchen und somit die Kapazität der Zuleitungen signifikant erhöht wird.In addition to the leads 15, 16 of the measuring capacitor, the leads 17, 18 are provided on the ceramic carrier 13, which end as blind stub lines in front of the measuring capacitor 14 and which form an auxiliary capacitor, the capacitance of which is also monitored in the evaluation device 4. Changes in the surroundings of the leads 15, 16 of the measuring capacitor, which would falsify the capacitance measurement on the measuring capacitor 14, also change the measurement of the auxiliary capacitor, which is formed by the leads 17, 18. By changing the capacitance of the auxiliary capacitor, the size of the disturbance can be determined and the disturbance of the measurement on the measuring capacitor can be compensated. This can become important, for example, if the sensor arrangement 1 is immersed so deeply in the fluid 2 that the supply lines 15, 16, 17, 18 are partially immersed in the fluid and thus the capacity of the supply lines is significantly increased.
Durch diese Kompensation, die in einer Kompensationseinrichtung 5a der ersten Recheneinheit 5 geschieht, wird die Mes- sung der Dielektrizitätskonstante des Fluids wesentlich weniger fehleranfällig und unabhängig von einer idealen Handhabung der Sensoranordnung. Auch die Kalibrierung der Messanordnung kann gegenüber bekannten Messanordnungen wesentlich seltener erfolgen.This compensation, which takes place in a compensation device 5a of the first computing unit 5, Solution of the dielectric constant of the fluid much less susceptible to errors and regardless of an ideal handling of the sensor arrangement. The calibration of the measuring arrangement can also be carried out much less frequently than known measuring arrangements.
Während gemäß der Figur 3 die Zuleitungen 15, 16 des Messkondensators und 17, 18 abwechselnd zueinander angeordnet sind, zeigt die Figur 4 eine Anordnung, bei der jeweils die beiden Zuleitungen des Messkondensators 14 und die beiden blindenWhile the feed lines 15, 16 of the measuring capacitor and 17, 18 are arranged alternately to one another according to FIG. 3, FIG. 4 shows an arrangement in which the two feed lines of the measuring capacitor 14 and the two blind ones
Stichleitungen des Hilfskondensators direkt nebeneinander angeordnet sind. Dabei ist der Abstand zwischen den Zuleitungen so gewählt, dass die gesamte Breite der nebeneinander und parallel verlaufenden Zuleitungen etwa der Breite des Messkon- densators 14 entspricht.Stub lines of the auxiliary capacitor are arranged directly next to each other. The distance between the feed lines is selected such that the total width of the feed lines running side by side and in parallel corresponds approximately to the width of the measuring capacitor 14.
In der Figur 5 ist dagegen eine Anordnung dargestellt, bei der die Zuleitungen des Messkondensators 14 direkt nebeneinander und ebenso die Stichleitungen direkt nebeneinander und parallel zueinander angeordnet sind, wobei jedoch alle vier Leitungen sehr eng parallel zueinander geführt sind, was zu einer Erhöhung der Zuleitungskapazität führt. Dadurch wird die Anordnung beispielsweise sensitiver dafür, ob der Sensor so tief in das Fluid eingetaucht ist, dass auch die Zuleitun- gen bereits von dem Fluid umgeben sind.In contrast, FIG. 5 shows an arrangement in which the supply lines of the measuring capacitor 14 are arranged directly next to one another and likewise the stub lines are arranged directly next to one another and parallel to one another, but all four lines are very closely parallel to one another, which leads to an increase in the supply line capacity , This makes the arrangement more sensitive, for example, to whether the sensor is so deeply immersed in the fluid that the supply lines are already surrounded by the fluid.
An dem Ende des in der Figur 5 dargestellten Keramikträgers 13 ist beispielhaft und schematisch ein Temperatursensor 19 in Form eines Temperaturelementes dargestellt. Durch dieses wird bei eingetauchtem Messkondensator 14 in dessen unmittelbarer Umgebung die Temperatur des Fluids gemessen. Der Temperatursensor 19 ist mittels zweier Zuleitungen, die auf der Rückseite des Keramikträgers 13 verlaufen und in der Figur nicht dargestellt sind, mit der Auswerteeinrichtung 4 und dort mit der zweiten Recheneinrichtung 6 zur Bestimmung der Temperatur verbunden.At the end of the ceramic carrier 13 shown in FIG. 5, a temperature sensor 19 in the form of a temperature element is shown schematically as an example. With this, when the measuring capacitor 14 is immersed, the temperature of the fluid is measured in its immediate vicinity. The temperature sensor 19 is by means of two leads that run on the back of the ceramic carrier 13 and in the figure are not shown, connected to the evaluation device 4 and there to the second computing device 6 for determining the temperature.
Die in den Figuren 3, 4 und 5 dargestellten Zuleitungen enden am Ende des Keramikträgers 13 jeweils mit verbreiterten Leiterbahnstücken 20, die als Steckkontakte für einen dort aufzusetzenden Stecker dienen können der das Ende eines flexiblen Kabels bildet, dessen anderes Ende mit der Auswerteein- richtung 4 verbunden ist. Das flexible Kabel kann entsprechend abgeschirmt werden, um Einflüsse auf die Kapazität der Zuleitungen der Kondensatoren zu verhindern.The leads shown in FIGS. 3, 4 and 5 each end at the end of the ceramic carrier 13 with widened conductor track pieces 20, which can serve as plug contacts for a plug to be placed there, which forms the end of a flexible cable, the other end of which is connected to the evaluation device 4 connected is. The flexible cable can be shielded accordingly to prevent influences on the capacitance of the capacitors' supply lines.
Durch die dargestellte Messanordnung in Verbindung mit der hierfür verwendeten Sensoranordnung sind kurze Messzeiten, hohe Messgenauigkeiten und ein reduzierter Kalibrieraufwand bei der Bestimmung von dielektrischen Eigenschaften von Ölen, insbesondere Frittierfetten gegeben. Die Messeinrichtung kann jedoch auch bei der Bestimmung anderer, mit der Dielektrizi- tätskonstanten zusammenhängender Größen von Fluiden dienen.The measuring arrangement shown, in conjunction with the sensor arrangement used for this purpose, gives short measuring times, high measuring accuracies and reduced calibration effort when determining the dielectric properties of oils, in particular frying fats. However, the measuring device can also be used to determine other sizes of fluids related to the dielectric constant.
Dies beschränkt sich nicht auf Flüssigkeiten sondern die Anwendung ist beispielsweise auch in Gasen, beispielsweise Isoliergasen für elektrische Anlagen denkbar. Als Massenprodukt ist beispielsweise auch der serienmäßige Einsatz einer Mess- einrichtung, wie sie hier dargestellt ist, bei der Überwachung der Qualität von Motoröl von Kraftfahrzeugen denkbar. Die Benachrichitung des Kraftfahrzeugführers wird dann nicht nur in Abhängigkeit von der Motorlaufleistung, sondern nach tatsächlich erfolgter Qualitätsmessung des Motoröls durch ei- ne Leuchte am Armaturenbrett erfolgen können. This is not limited to liquids, but the application is also conceivable, for example, in gases, for example insulating gases for electrical systems. As a mass product, for example, the series use of a measuring device, as shown here, for monitoring the quality of motor oil in motor vehicles is also conceivable. The notification of the motor vehicle driver will then be possible not only as a function of the engine mileage, but after the quality of the engine oil has actually been measured by a lamp on the dashboard.

Claims

Patentansprüche claims
1. Messanordnung zur Bestimmung einer Eigenschaft, insbesondere des Alterungszustandes eines Fluides (2) , insbesondere eines Frittierfettes, aus einer dielektrischen Eigenschaft des Fluides mit einem ersten Sensor (14) zur Messung einer elektrischen Kapazität und mit einem zweiten Sensor (19) zur Temperaturmessung, d a d u r c h g e k e n n z e i c h n e t , d a ß der erste Sensor als ein in das Fluid eintauchbarer, einen als Messkondensator dienenden Streufeldkondensator aufweisender dielektrischer Sensor (14) und der zweite Sensor als in das Fluid (2) eintauchbarer Temperatursensor (19) ausgebildet ist .1. Measuring arrangement for determining a property, in particular the aging condition of a fluid (2), in particular a deep-frying fat, from a dielectric property of the fluid with a first sensor (14) for measuring an electrical capacitance and with a second sensor (19) for temperature measurement, characterized in that the first sensor is designed as a dielectric sensor (14) which can be immersed in the fluid and has a stray field capacitor serving as a measuring capacitor, and the second sensor is designed as a temperature sensor (19) which is immersed in the fluid (2).
2. Messanordnung nach Anspruch 1, d a d u r c h g e k e n n z e i c h n e t, d a ß der erste und der zweite Sensor (14, 19) mit einer Auswerteeinrichtung (4) verbunden sind, die jeweils einem gemessenen Temperaturwert und einem gemessenen elektrischen Kapazitätswert einen Wert der zu bestimmenden Eigenschaft zuordnet.2.Measuring arrangement according to claim 1, where the first and second sensors (14, 19) are connected to an evaluation device (4), each of which assigns a value of the property to be determined to a measured temperature value and a measured electrical capacitance value.
3. Messanordnung nach Anspruch 1 oder 2, d a d u r c h g e k e n n z e i c h n e t, d a ß in einer Vergleichseinrichtung der Auswerteeinrichtung (4) der jeweils durch den dielektrischen Sensor (14) gemessenen Wert der elektrischen Kapazität mit einem dem gemessenen Temperaturwert zugeordneten gespeicherten Referenzwert verglichen und in Abhängigkeit vom Erreichen oder Überschreiten des Referenzwertes ein Signal ausgegeben wird.3. Measuring arrangement according to claim 1 or 2, characterized in that in a comparison device of the evaluation device (4) the value of the electrical capacitance measured in each case by the dielectric sensor (14) is compared with a stored reference value assigned to the measured temperature value and as a function of reaching or If the reference value is exceeded, a signal is output.
4. Messanordnung nach einem der Ansprüche 1, 2 oder 3, g e k e n n z e i c h n e t d u r c h eine Kompensationseinrichtung (5a) zur Korrektur des Messwer- tes der elektrischen Kapazität unter Berücksichtigung eines an einem in der Nähe des Messkondensators (14) angeordneten Hilfskondensator (17, 18) gemessenen Referenzmesswertes einer Kapazität.4. Measuring arrangement according to one of claims 1, 2 or 3, characterized by a compensation device (5a) for correcting the measured value of the electrical capacitance, taking into account one arranged in the vicinity of the measuring capacitor (14) Auxiliary capacitor (17, 18) measured reference measured value of a capacitance.
5. Sensoranordnung zur Messung einer dielektrischen Eigen- Schaft eines Fluides mit einem in das Fluid (2) eintauchbaren dielektrischen Sensor (14) , der einen als Streufeldkondensator ausgebildeten Messkondensator aufweist, d a d u r c h g e k e n n z e i c h n e t, d a ß der Sensor einen Hilfskondensator (17, 18) aufweist, und dass beim Einbringen des Sensors (14) in das Fluid der Hilfskondensator (17, 18) frühestens dann in das Fluid (2) eintaucht, wenn der Messkondensator in das Fluid (2) völlig eingetaucht ist .5. Sensor arrangement for measuring a dielectric property of a fluid with a dielectric sensor (14) which can be immersed in the fluid (2) and which has a measuring capacitor designed as a stray field capacitor, characterized in that the sensor has an auxiliary capacitor (17, 18), and that when the sensor (14) is introduced into the fluid, the auxiliary capacitor (17, 18) is immersed in the fluid (2) at the earliest when the measuring capacitor is completely immersed in the fluid (2).
6. Sensoranordnung nach Anspruch 5, d a d u r c h g e k e n n z e i c h n e t, d a ß Zuleitungen (15, 16, 17, 18) des Messkondensators und des Hilfskondensators (17, 18) symmetrisch und baugleich zueinander ausgebildet sind.6. Sensor arrangement according to claim 5, d a d u r c h g e k e n n z e i c h n e t, d a ß leads (15, 16, 17, 18) of the measuring capacitor and the auxiliary capacitor (17, 18) are symmetrical and structurally identical to each other.
7. Sensoranordnung nach Anspruch 5 oder 6 , d a d u r c h g e k e n n z e i c h n e t, d a ß, der Hilfskondensator (17, 18) aus zwei vor dem Messkondensator endenden Stichleitungen besteht, die gleichartig wie die Zuleitungen (15, 16) des Messkondensators ausgebildet und angeordnet sind.7. Sensor arrangement according to claim 5 or 6, d a d u r c h g e k e n n e e c h n e t, d a ß, the auxiliary capacitor (17, 18) consists of two stub lines ending in front of the measuring capacitor, which are constructed and arranged in the same way as the feed lines (15, 16) of the measuring capacitor.
8. Sensoranordnung nach Anspruch 5 oder einem der folgenden, d a d u r c h g e k e n n z e i c h n e t, d a ß der Messkondensator durch eine Mehrzahl von flachen Leiterbahnen insbesondere in Form eines Interdigitalkondensators gebildet ist.8. Sensor arrangement according to claim 5 or one of the following, that is, that the measuring capacitor is formed by a plurality of flat conductor tracks, in particular in the form of an interdigital capacitor.
9. Sensoranordnung nach Anspruch 8 , d a d u r c h g e k e n n z e i c h n e t, d a ß die Leiterbahnen in Dünnschicht- oder Dickschichttechnik auf einen isolierenden Träger (13) aufgedruckt sind. 9. Sensor arrangement according to claim 8, characterized in that ß the conductor tracks in thin-film or thick-film technology are printed on an insulating carrier (13).
10. Sensoranordnung nach einem der Ansprüche 5 - 9, g e k e n n z e i c h n e t d u r c h einen Temperatursensor10. Sensor arrangement according to one of claims 5 - 9, g e k e n n z e i c h n e t d u r c h a temperature sensor
(19) in Form eines NTC-Widerstandes, eines PTC—Widerstandes oder eines Temperaturelementes .(19) in the form of an NTC resistor, a PTC resistor or a temperature element.
11. Sensoranordnung nach Anspruch 10, d a d u r c h g e k e n n z e i c h n e , d a ß, der Temperatursensor (19) mit dem dielektrischen Sensor (14) zu einer konstruktiven Einheit verbunden ist.11. Sensor arrangement according to claim 10, d a d u r c h g e k e n n z e i c h n e, d a ß, the temperature sensor (19) with the dielectric sensor (14) is connected to a structural unit.
12. Sensoranordnung nach Anspruch 11 und 9, d a d u r c h g e k e n n z e i c h n e , d a ß, die Zuleitungen des Temperatursensors auf den isolierenden Träger (13) in Form von Leiterbahnen aufgebracht sind. 12. Sensor arrangement according to claim 11 and 9, d a d u r c h g e k e n n z e i c h n e, d a ß, the leads of the temperature sensor on the insulating carrier (13) are applied in the form of conductor tracks.
EP02795239A 2002-01-17 2002-12-19 Measuring assembly for determining a characteristic of a fluid Expired - Lifetime EP1466170B1 (en)

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DE10202002A DE10202002A1 (en) 2002-01-17 2002-01-17 Measuring arrangement and sensor arrangement for determining a property of a fluid and method for its operation
DE10202002 2002-01-17
PCT/EP2002/014585 WO2003060499A2 (en) 2002-01-17 2002-12-19 Measuring and sensor assembly for determining a characteristic of a fluid and method for operating the same

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DE20221466U1 (en) 2005-12-29
JP2005515436A (en) 2005-05-26
JP4147482B2 (en) 2008-09-10
US7523006B2 (en) 2009-04-21
WO2003060499A2 (en) 2003-07-24
ES2275944T3 (en) 2007-06-16
EP1466170B1 (en) 2006-11-22
WO2003060499A3 (en) 2004-01-15
US20050222783A1 (en) 2005-10-06

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