EP1412686B8 - Kammer für eine gefriertrocknungseinrichtung - Google Patents

Kammer für eine gefriertrocknungseinrichtung Download PDF

Info

Publication number
EP1412686B8
EP1412686B8 EP02791452A EP02791452A EP1412686B8 EP 1412686 B8 EP1412686 B8 EP 1412686B8 EP 02791452 A EP02791452 A EP 02791452A EP 02791452 A EP02791452 A EP 02791452A EP 1412686 B8 EP1412686 B8 EP 1412686B8
Authority
EP
European Patent Office
Prior art keywords
chamber
freeze
drying device
tempered
adjusting surfaces
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP02791452A
Other languages
English (en)
French (fr)
Other versions
EP1412686B1 (de
EP1412686A1 (de
Inventor
Peter Haseley
Georg-Wilhelm Oetjen
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
GEA Lyophil GmbH
Original Assignee
GEA Lyophil GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by GEA Lyophil GmbH filed Critical GEA Lyophil GmbH
Publication of EP1412686A1 publication Critical patent/EP1412686A1/de
Publication of EP1412686B1 publication Critical patent/EP1412686B1/de
Application granted granted Critical
Publication of EP1412686B8 publication Critical patent/EP1412686B8/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B5/00Drying solid materials or objects by processes not involving the application of heat
    • F26B5/04Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
    • F26B5/06Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum the process involving freezing

Landscapes

  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Molecular Biology (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Drying Of Solid Materials (AREA)
  • Vending Machines For Individual Products (AREA)
  • Physical Deposition Of Substances That Are Components Of Semiconductor Devices (AREA)
EP02791452A 2001-07-27 2002-07-15 Kammer für eine gefriertrocknungseinrichtung Expired - Lifetime EP1412686B8 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE10136498 2001-07-27
DE10136498A DE10136498A1 (de) 2001-07-27 2001-07-27 Kammer für eine Gefriertrocknungseinrichtung
PCT/EP2002/007828 WO2003012355A1 (de) 2001-07-27 2002-07-15 Kammer für eine gefriertrocknungseinrichtung

Publications (3)

Publication Number Publication Date
EP1412686A1 EP1412686A1 (de) 2004-04-28
EP1412686B1 EP1412686B1 (de) 2007-03-21
EP1412686B8 true EP1412686B8 (de) 2007-05-09

Family

ID=7693223

Family Applications (2)

Application Number Title Priority Date Filing Date
EP01124001A Withdrawn EP1279913A1 (de) 2001-07-27 2001-10-09 Kammer für eine Gefriertrocknungseinrichtung
EP02791452A Expired - Lifetime EP1412686B8 (de) 2001-07-27 2002-07-15 Kammer für eine gefriertrocknungseinrichtung

Family Applications Before (1)

Application Number Title Priority Date Filing Date
EP01124001A Withdrawn EP1279913A1 (de) 2001-07-27 2001-10-09 Kammer für eine Gefriertrocknungseinrichtung

Country Status (10)

Country Link
US (1) US6920701B2 (de)
EP (2) EP1279913A1 (de)
JP (1) JP3984591B2 (de)
AT (1) ATE357638T1 (de)
AU (1) AU2002333243B2 (de)
DE (2) DE10136498A1 (de)
DK (1) DK1412686T3 (de)
ES (1) ES2284957T3 (de)
PT (1) PT1412686E (de)
WO (1) WO2003012355A1 (de)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007049278A1 (de) 2007-10-12 2009-04-16 Gea Lyophil Gmbh Vorrichtungen zum Gefriertrocknen

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10218007A1 (de) 2002-04-23 2003-11-06 Bayer Ag Gefriertrockenvorrichtung
DE102004007526A1 (de) * 2004-02-17 2005-09-01 Oetjen, Georg-Wilhelm, Dr. Verfahren und Einrichtung zur Gefriertrocknung von Produkten
WO2008057001A1 (fr) * 2006-11-07 2008-05-15 Lev Kuzmich Kovalev Dispositif de déshydratation à basse température de matériaux sous vide
US8371039B2 (en) 2009-12-30 2013-02-12 Baxter International Inc. Thermal shielding to optimize lyophilization process for pre-filled syringes or vials
US8689460B2 (en) 2010-09-28 2014-04-08 Baxter International Inc. Optimization of nucleation and crystallization for lyophilization using gap freezing
US8966782B2 (en) 2010-09-28 2015-03-03 Baxter International Inc. Optimization of nucleation and crystallization for lyophilization using gap freezing
CN105501503B (zh) 2012-05-03 2018-01-12 肖特公开股份有限公司 用于处理或加工容器的方法和设备
US9180145B2 (en) * 2012-10-12 2015-11-10 Mimedx Group, Inc. Compositions and methods for recruiting and localizing stem cells
US10480855B2 (en) * 2014-10-08 2019-11-19 Robert M. Parker Heated shelf for a freeze-drying system having a leading folded edge that does not catch on food being removed from the system
ES2690269T3 (es) * 2015-03-16 2018-11-20 Martin Christ Gefriertrocknungsanlagen Gmbh Liofilizador con una ventanilla de visión
CN105004144B (zh) * 2015-07-17 2017-03-29 上海化工研究院 一种可变容积的迭加式真空干燥恒温箱
US10605527B2 (en) 2015-09-22 2020-03-31 Millrock Technology, Inc. Apparatus and method for developing freeze drying protocols using small batches of product
ES2774058T3 (es) * 2017-04-21 2020-07-16 Gea Lyophil Gmbh Un liofilizador y un método para inducir la nucleación en los productos
US10451346B1 (en) * 2019-03-31 2019-10-22 Vinamit Usa Llc Convection current freeze drying apparatus and method of operating the same
US10676797B1 (en) * 2019-01-27 2020-06-09 Vinamit Usa Llc Concentrated sugarcane juice powder and method for preparing the same using the convection current freeze drying apparatus
US10921058B2 (en) * 2019-01-27 2021-02-16 Vinamit Usa Llc Fully automatic convection current vacuum freeze drying method
US10966439B2 (en) * 2019-01-27 2021-04-06 Vinamit Usa Llc Concentrated fruit juice powder and method for preparing the same using a non-linear screw press juicer and convection current freeze drying apparatus
JP7390176B2 (ja) * 2019-12-06 2023-12-01 株式会社アルバック 真空乾燥装置、真空乾燥装置における棚の温度調節方法
JP2021096030A (ja) * 2019-12-17 2021-06-24 株式会社アルバック 真空乾燥装置、真空乾燥装置における棚の温度調節方法
US11054185B1 (en) * 2020-02-24 2021-07-06 Lyophilization Technology, Inc. Apparatus for lyophilization of products contained in product delivery units
US11506455B2 (en) * 2020-03-05 2022-11-22 Green Mountain Mechanical Design, Inc. Partial vacuum drying system and method
CN116045606B (zh) * 2023-01-13 2023-09-22 浙江毓昌生物技术有限公司 一种冷冻箱及操作方法
CN117847972B (zh) * 2024-01-18 2026-04-10 青岛永合创信电子科技有限公司 能维持温度均匀的真空冷冻干燥机
CN118935929A (zh) * 2024-07-24 2024-11-12 西安国康瑞金制药有限公司 一种氢化可的松琥珀酸钠注射液制备方法和装置

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3048928A (en) * 1959-04-27 1962-08-14 Raytheon Co Freeze-drying apparatus
NL144053C (nl) * 1962-04-09 1975-04-15 Hills Bros Coffee Werkwijze en inrichting voor het continu drogen van bevroren, waterbevattende materiaaldeeltjes.
US3311991A (en) * 1965-04-20 1967-04-04 Pillsbury Co Drying apparatus and method
US3762065A (en) * 1971-04-12 1973-10-02 Kamas Kvarnmaskiner Ab Apparatus for drying materials
AU4658296A (en) * 1995-01-20 1996-08-07 Freezedry Specialties, Inc. Freeze dryer
GB9505523D0 (en) * 1995-03-18 1995-05-03 Wellcome Found Lyophilization process
FR2740108B1 (fr) * 1995-08-22 1998-03-27 Lab Francais Du Fractionnement Emballage etanche pour sechage, notamment lyophilisation, et procede de sechage, notamment de lyophilisation, a l'aide d'un tel emballage
AT1399U1 (de) * 1995-11-29 1997-04-25 Immuno Ag Verfahren und einrichtung zum lyophilisieren
DE19719398A1 (de) * 1997-05-07 1998-11-12 Amsco Finn Aqua Gmbh Verfahren zur Steuerung eines Gefriertrocknungsprozesses

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007049278A1 (de) 2007-10-12 2009-04-16 Gea Lyophil Gmbh Vorrichtungen zum Gefriertrocknen
DE102007049278B4 (de) * 2007-10-12 2010-08-05 Gea Lyophil Gmbh Vorrichtungen zum Gefriertrocknen

Also Published As

Publication number Publication date
JP2004537025A (ja) 2004-12-09
DE10136498A1 (de) 2003-02-06
PT1412686E (pt) 2007-06-29
US6920701B2 (en) 2005-07-26
DE50209781D1 (de) 2007-05-03
US20040250441A1 (en) 2004-12-16
EP1279913A1 (de) 2003-01-29
JP3984591B2 (ja) 2007-10-03
AU2002333243B2 (en) 2007-05-24
WO2003012355A1 (de) 2003-02-13
EP1412686B1 (de) 2007-03-21
EP1412686A1 (de) 2004-04-28
DK1412686T3 (da) 2007-07-30
ATE357638T1 (de) 2007-04-15
ES2284957T3 (es) 2007-11-16

Similar Documents

Publication Publication Date Title
DK1412686T3 (da) Kammer til en frysetörringsanordning
AU2001280793A1 (en) Dispensing device for dispensing scents
AU6718494A (en) 2-substituted-3,4-diarylthiophene derivatives as inhibitors of cyclooxygenase
AU2003247798A1 (en) Nozzles and components thereof and methods for making the same
AU2001260109A1 (en) Mixture comprising an inhibitor or suppressor of a gene and molecule binding to an expression product of that gene
AU5425794A (en) Process for the preparation of taxane derivatives, novel taxanes so obtained and antitumour and antileukaemia compositions containing same
AU2002333243A1 (en) Chamber for a freeze-drying device
WO2002069728A3 (en) Luminescent lollipop
WO2003001171A3 (en) A resonance-type microelectronic pressure sensor that withstands high pressures
AU2001253297A1 (en) Sterilization process for air, liquid and surfaces
MY116421A (en) New formulation
AU1628597A (en) Treatment and prophylaxis of pancreatitis
HU0201837D0 (de)
AU1559501A (en) Apoptosis inducing proteinaceous substance
AU2002304685A1 (en) Thermally curable, thixotropic mixtures containing carbamate and/or allophanate groups
CA2342525A1 (en) Reciprocating optical modulation system
AU3315200A (en) 1,5-anhydro-d-fructose substituted with a hydrophobic group for use as anti-oxidant and/or emulsifier
WO2002078049A3 (en) Multi-spectral uniform light source
CA2353943A1 (en) Method of drying a lactulose solution
DE60236623D1 (de) Amorphe substanz eines tricyclischen triazolobenzazepinderivats
AU2001284476A1 (en) Novel crystals of 1,3,4-oxadiazole derivative, process for producing the crystals and medicines containing the same as the active ingredient
AU2002305461A1 (en) Preservation of competent cells at ambient temperatures
WO2002004405A3 (en) 13-substituted methacycline compounds
AU4550197A (en) A circuit for maintaining the temperature of a light source, and use of the circuit
AU2002239977A1 (en) Atmospheric pressure, glow discharge, optical emission source for the direct sampling of liquid media

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

17P Request for examination filed

Effective date: 20040205

AK Designated contracting states

Kind code of ref document: A1

Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR IE IT LI LU MC NL PT SE SK TR

GRAP Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOSNIGR1

GRAS Grant fee paid

Free format text: ORIGINAL CODE: EPIDOSNIGR3

GRAA (expected) grant

Free format text: ORIGINAL CODE: 0009210

AK Designated contracting states

Kind code of ref document: B1

Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR IE IT LI LU MC NL PT SE SK TR

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: FI

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20070321

REG Reference to a national code

Ref country code: GB

Ref legal event code: FG4D

Free format text: NOT ENGLISH

REG Reference to a national code

Ref country code: CH

Ref legal event code: EP

RAP2 Party data changed (patent owner data changed or rights of a patent transferred)

Owner name: GEA LYOPHIL GMBH

REF Corresponds to:

Ref document number: 50209781

Country of ref document: DE

Date of ref document: 20070503

Kind code of ref document: P

REG Reference to a national code

Ref country code: IE

Ref legal event code: FG4D

Free format text: LANGUAGE OF EP DOCUMENT: GERMAN

REG Reference to a national code

Ref country code: PT

Ref legal event code: SC4A

Free format text: AVAILABILITY OF NATIONAL TRANSLATION

Effective date: 20070620

NLT2 Nl: modifications (of names), taken from the european patent patent bulletin

Owner name: GEA LYOPHIL GMBH

Effective date: 20070502

GBT Gb: translation of ep patent filed (gb section 77(6)(a)/1977)

Effective date: 20070619

REG Reference to a national code

Ref country code: SE

Ref legal event code: TRGR

REG Reference to a national code

Ref country code: DK

Ref legal event code: T3

REG Reference to a national code

Ref country code: CH

Ref legal event code: NV

Representative=s name: R. A. EGLI & CO. PATENTANWAELTE

ET Fr: translation filed
REG Reference to a national code

Ref country code: ES

Ref legal event code: FG2A

Ref document number: 2284957

Country of ref document: ES

Kind code of ref document: T3

PLBE No opposition filed within time limit

Free format text: ORIGINAL CODE: 0009261

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT

26N No opposition filed

Effective date: 20071227

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: GR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20070622

Ref country code: MC

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20070731

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: CZ

Payment date: 20080626

Year of fee payment: 7

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: TR

Payment date: 20080624

Year of fee payment: 7

Ref country code: PT

Payment date: 20080620

Year of fee payment: 7

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: DK

Payment date: 20080729

Year of fee payment: 7

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: AT

Payment date: 20080619

Year of fee payment: 7

Ref country code: IE

Payment date: 20080725

Year of fee payment: 7

Ref country code: SK

Payment date: 20080701

Year of fee payment: 7

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: EE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20070321

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: BE

Payment date: 20080818

Year of fee payment: 7

Ref country code: SE

Payment date: 20080729

Year of fee payment: 7

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: CY

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20070321

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LU

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20070715

Ref country code: BG

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20070621

REG Reference to a national code

Ref country code: PT

Ref legal event code: MM4A

Free format text: LAPSE DUE TO NON-PAYMENT OF FEES

Effective date: 20100115

BERE Be: lapsed

Owner name: GEA LYOPHIL GMBH

Effective date: 20090731

REG Reference to a national code

Ref country code: DK

Ref legal event code: EBP

EUG Se: european patent has lapsed
REG Reference to a national code

Ref country code: SK

Ref legal event code: MM4A

Ref document number: E 2338

Country of ref document: SK

Effective date: 20090715

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: PT

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20100115

Ref country code: CZ

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20090715

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SK

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20090715

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: BE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20090731

Ref country code: AT

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20090715

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20090715

Ref country code: DK

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20090731

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20090716

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: TR

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20090715

REG Reference to a national code

Ref country code: FR

Ref legal event code: PLFP

Year of fee payment: 15

REG Reference to a national code

Ref country code: FR

Ref legal event code: PLFP

Year of fee payment: 16

REG Reference to a national code

Ref country code: FR

Ref legal event code: PLFP

Year of fee payment: 17

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: DE

Payment date: 20180727

Year of fee payment: 17

Ref country code: IT

Payment date: 20180719

Year of fee payment: 17

Ref country code: FR

Payment date: 20180726

Year of fee payment: 17

Ref country code: NL

Payment date: 20180726

Year of fee payment: 17

Ref country code: ES

Payment date: 20180801

Year of fee payment: 17

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: CH

Payment date: 20180801

Year of fee payment: 17

Ref country code: GB

Payment date: 20180727

Year of fee payment: 17

REG Reference to a national code

Ref country code: DE

Ref legal event code: R119

Ref document number: 50209781

Country of ref document: DE

REG Reference to a national code

Ref country code: CH

Ref legal event code: PL

GBPC Gb: european patent ceased through non-payment of renewal fee

Effective date: 20190715

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: NL

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20190801

Ref country code: GB

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20190715

Ref country code: DE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20200201

REG Reference to a national code

Ref country code: NL

Ref legal event code: MM

Effective date: 20190801

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: CH

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20190731

Ref country code: LI

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20190731

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: FR

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20190731

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IT

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20190715

REG Reference to a national code

Ref country code: ES

Ref legal event code: FD2A

Effective date: 20201130

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: ES

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20190716