EP0592267B1 - Metal can with closure of the easy-to-open type by tearing along a line of weakness and steel sheet for its manufacture - Google Patents
Metal can with closure of the easy-to-open type by tearing along a line of weakness and steel sheet for its manufacture Download PDFInfo
- Publication number
- EP0592267B1 EP0592267B1 EP93402311A EP93402311A EP0592267B1 EP 0592267 B1 EP0592267 B1 EP 0592267B1 EP 93402311 A EP93402311 A EP 93402311A EP 93402311 A EP93402311 A EP 93402311A EP 0592267 B1 EP0592267 B1 EP 0592267B1
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- EP
- European Patent Office
- Prior art keywords
- steel
- sheet
- content
- ratio
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/002—Ferrous alloys, e.g. steel alloys containing In, Mg, or other elements not provided for in one single group C22C38/001 - C22C38/60
Definitions
- the present invention relates to packaging of opening type by breaking a line of least resistance so-called easy opening box.
- They have a cover in which is arranged a line of least resistance, for example a incision, delimiting an opening panel.
- An actuating ring is fixed on the panel opening using a rivet.
- the opening is caused by an effort of traction on the actuation ring so as to break the metal at the incision, the opening panel possibly including a connection zone with the cover so as not to detach completely from this latest.
- a sheet made up When made from steel, for reduce their cost, a sheet made up is commonly used standard low carbon steel, annealed continuous at approximately 680 ° C and tinned.
- the steel used for the realization of such packaging must allow on the one hand to form the rivet of fixing the opening ring and, on the other hand, a breaking of the line of least resistance easily without having to exert too much effort.
- the breaking load Rm must not be too high because otherwise the opening effort to be exerted to break the line of least resistance will have to be important.
- the yield strength Re is approximately 415 MPa and the breaking load Rm of around 430 MPa results in a Re / Rm ratio of the order of 0.96.
- An easy opening lid made with a such steel has a high opening force, due the value of Rm and a residual thickness at the level relatively large incision.
- the yield point is important, which causes the formation of worms visible when the packaging is stamped, detrimental to the aesthetic appearance of the latter.
- the invention aims to provide an opening type package by breaking a line of least resistance, for which the overall effort required for opening is reduced, while having an improved appearance after stamping packaging, and good training ability rivet.
- the invention relates to packaging metallic type of opening by rupture of a line of least resistance arranged in a part of sheet steel wall, characterized in that steel constituting the sheet has a carbon content of between 0.02 and 0.08% by weight and a boron content included between 0.002 and 0.004% by weight, the steel also containing of nitrogen, the ratio of boron content to nitrogen content being greater than 0.8, the remainder being iron and residual impurities, said sheet being subjected to continuous rolling followed by annealing on base carried out for 8 to 10 hours at a temperature between 550 and 650 ° C approximately, then subjected to a cold re-rolling with an elongation rate included between 5 and 10%.
- the invention also relates to a sheet steel intended for making a packaging and characterized in that the ratio of its elastic limit on its breaking load is between 0.87 and 0.96, preferably between 0.91 and 0.92.
- Reducing the effort required to open involves the use of a steel with a limit relatively low elasticity, which further facilitates the winding of the opening panel after breaking of the incision, and by a high Re / Rm ratio.
- the appearance of the packaging and its resistance corrosion are improved by the use of a sheet having an equiaxed fine-grained structure and not exhibiting no yield strength plateau.
- the packaging according to the invention is made from a steel sheet of which the carbon content is between 0.02 and 0.08% by weight and boron content is 0.002 and 0.004% by weight, the steel also containing nitrogen in a amount less than 0.005%, the ratio of the content of boron on the nitrogen content being greater than 0.8.
- a carbon content of less than 0.02% is difficult to achieve with production processes conventional and can lead to mechanical resistance insufficient cover.
- the ratio of the boron content on the nitrogen content must be greater than 0.8, boron being limited to 0.004% because, for a higher content, has an increase in the mechanical characteristics of the sheet metal and we see a preferential oxidation appear in side of the product, which is unacceptable from the point of view aesthetic.
- the process used to make the suitable sheet for packaging according to the invention consists in that after continuous rolling of the steel described above, the sheet is subjected to an annealing on base carried out during 8 at 10 a.m. at a temperature between 550 and 650 ° C approximately, the rise in temperature from the temperature ambient being carried out in approximately 20 hours. The sheet is then subjected to a cold re-rolling with a rate elongation between 5 and 10%.
- the ratio of the elastic limit to the breaking load is between 0.91 and 0.92.
- the remaining thickness at the bottom of the incision should not not be less than 70 microns under penalty of damage unacceptable, while this remaining thickness in bottom of incision can go down to 50 microns in the case of the steel according to the invention.
- This packaging made from a sheet metal fine-grained equiaxed structure avoids, during training of the rivet, the appearance of deformation roughness due to subsidence, which is detrimental to the appearance of the packaging and the holding of any varnish.
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Heat Treatment Of Sheet Steel (AREA)
- Containers Opened By Tearing Frangible Portions (AREA)
- Heat Treatment Of Steel (AREA)
- Wrappers (AREA)
- Cartons (AREA)
- Laminated Bodies (AREA)
Abstract
Description
La présente invention concerne les emballages du type à ouverture par rupture d'une ligne de moindre résistance dite boíte à ouverture facile.The present invention relates to packaging of opening type by breaking a line of least resistance so-called easy opening box.
On connaít de tels emballages qui sont par exemple destinés à contenir une boisson, des conserves ou autres produits.We know such packaging which are by example intended to contain a drink, preserves or others products.
Ils comportent un couvercle dans lequel est agencée une ligne de moindre résistance, par exemple une incision, délimitant un panneau d'ouverture.They have a cover in which is arranged a line of least resistance, for example a incision, delimiting an opening panel.
Un anneau d'actionnement est fixé sur le panneau d'ouverture à l'aide d'un rivet.An actuating ring is fixed on the panel opening using a rivet.
L'ouverture est provoquée par un effort de traction sur l'anneau d'actionnement de manière à rompre le métal au niveau de l'incision, le panneau d'ouverture pouvant éventuellement comporter une zone de liaison avec le couvercle pour ne pas se détacher complètement de ce dernier.The opening is caused by an effort of traction on the actuation ring so as to break the metal at the incision, the opening panel possibly including a connection zone with the cover so as not to detach completely from this latest.
De tels emballages peuvent être réalisés en aluminium mais ils sont alors relativement coûteux.Such packaging can be produced in aluminum but they are then relatively expensive.
Lorsqu'ils sont réalisés à partir d'acier, pour diminuer leur coût, on utilise couramment une tôle constituée d'acier standard à bas carbone traitée en recuit continu à 680°C environ et étamée.When made from steel, for reduce their cost, a sheet made up is commonly used standard low carbon steel, annealed continuous at approximately 680 ° C and tinned.
Les caractéristiques mécaniques d'un tel acier à l'état étamé sont les suivantes :
- limite d'élasticité (Re) en sens travers de l'ordre de 415 MPa,
- charge à la rupture (Rm) en sens travers de l'ordre de 430 MPa.
- elastic limit (Re) in transverse direction of the order of 415 MPa,
- load at break (Rm) in cross direction of around 430 MPa.
L'acier utilisé pour la réalisation de tels emballages doit permettre d'une part de former le rivet de fixation de l'anneau d'ouverture et, d'autre part, une rupture de la ligne de moindre résistance aisée sans avoir à exercer un effort trop important. The steel used for the realization of such packaging must allow on the one hand to form the rivet of fixing the opening ring and, on the other hand, a breaking of the line of least resistance easily without having to exert too much effort.
Pour cela, la charge à la rupture Rm ne doit pas être trop élevée car sinon l'effort d'ouverture à exercer pour rompre la ligne de moindre résistance devra être important.For this, the breaking load Rm must not be too high because otherwise the opening effort to be exerted to break the line of least resistance will have to be important.
De même le rapport limite d'élasticité Re sur charge à la rupture Rm doit être voisin de 1 afin que l'acier soit suffisamment fragilisé pour provoquer une ouverture aisée.Likewise the elastic limit ratio Re on breaking load Rm must be close to 1 so that the steel is sufficiently weakened to cause a easy opening.
En revanche ce rapport Re/Rm ne doit pas être trop élevé, c'est à dire trop proche de 1, car dans ce cas, l'acier étant très fragilisé, il devient quasiment impossible de former le rivet, cette opération nécessitant un emboutissage profond de l'acier du couvercle de l'emballage.However, this Re / Rm ratio should not be too high, i.e. too close to 1, because in this case, the steel being very weakened, it becomes almost impossible to form the rivet, this operation requiring deep drawing of the steel of the packaging lid.
Or l'acier standard couramment utilisé dont la limite d'élasticité Re est égale à environ 415 MPa et la charge à la rupture Rm de l'ordre de 430 MPa aboutit à un rapport Re/Rm de l'ordre de 0,96.Now the standard steel commonly used, the yield strength Re is approximately 415 MPa and the breaking load Rm of around 430 MPa results in a Re / Rm ratio of the order of 0.96.
Un couvercle à ouverture facile réalisé avec un tel acier présente un effort d'ouverture élevé, en raison de la valeur de Rm et d'une épaisseur résiduelle au niveau de l'incision relativement importante.An easy opening lid made with a such steel has a high opening force, due the value of Rm and a residual thickness at the level relatively large incision.
Par ailleurs, le palier de limite d'élasticité est important, ce qui provoque la formation de vermiculures apparentes lors de l'emboutissage de l'emballage, préjudiciable à l'aspect esthétique de ce dernier.In addition, the yield point is important, which causes the formation of worms visible when the packaging is stamped, detrimental to the aesthetic appearance of the latter.
Pour remédier à ces inconvénients, l'invention a pour but de fournir un emballage du type à ouverture par rupture d'une ligne de moindre résistance, pour lequel l'effort global nécessaire à l'ouverture soit diminué, tout en ayant un aspect amélioré après emboutissage de l'emballage, et une bonne aptitude à la formation du rivet.To remedy these drawbacks, the invention aims to provide an opening type package by breaking a line of least resistance, for which the overall effort required for opening is reduced, while having an improved appearance after stamping packaging, and good training ability rivet.
A cet effet, l'invention a pour objet un emballage métallique du type à ouverture par rupture d'une ligne de moindre résistance agencée dans une partie de paroi en tôle d'acier, caractérisé en ce que l'acier constituant la tôle a une teneur en carbone comprise entre 0,02 et 0,08% en poids et une teneur en bore comprise entre 0,002 et 0,004% en poids, l'acier contenant également de l'azote, le rapport de la teneur en bore sur la teneur en azote étant supérieur à 0,8, le reste étant du fer et des impuretés résiduelles, ladite tôle étant soumise à un laminage en continu suivi d'un recuit sur base effectué pendant 8 à 10 heures à une température comprise entre 550 et 650°C environ, puis soumise à un relaminage à froid avec un taux d'allongement compris entre 5 et 10%.To this end, the invention relates to packaging metallic type of opening by rupture of a line of least resistance arranged in a part of sheet steel wall, characterized in that steel constituting the sheet has a carbon content of between 0.02 and 0.08% by weight and a boron content included between 0.002 and 0.004% by weight, the steel also containing of nitrogen, the ratio of boron content to nitrogen content being greater than 0.8, the remainder being iron and residual impurities, said sheet being subjected to continuous rolling followed by annealing on base carried out for 8 to 10 hours at a temperature between 550 and 650 ° C approximately, then subjected to a cold re-rolling with an elongation rate included between 5 and 10%.
Selon d'autres caractéristiques :
- la composition pondérale de l'acier constituant
la tôle est de préférence la suivante, en millième
de pour cent :
- carbone : 50
- manganèse : 200
- phosphore : 10
- azote : 3,5
- aluminium : 30
- silicium : 5
- bore : 3
- le reste étant du fer et des impuretés résiduelles.
- the weight composition of the steel constituting the sheet is preferably as follows, in thousandths of a percent:
- carbon: 50
- manganese: 200
- phosphorus: 10
- nitrogen: 3.5
- aluminum: 30
- silicon: 5
- boron: 3
- the remainder being iron and residual impurities.
L'invention a également pour objet une tôle d'acier destinée à la réalisation d'un emballage et caractérisée en ce que le rapport de sa limite d'élasticité sur sa charge à la rupture est compris entre 0,87 et 0,96, de préférence entre 0,91 et 0,92. The invention also relates to a sheet steel intended for making a packaging and characterized in that the ratio of its elastic limit on its breaking load is between 0.87 and 0.96, preferably between 0.91 and 0.92.
L'invention sera mieux comprise à la lecture de la description détaillée qui va suivre, faite à titre d'exemple.The invention will be better understood on reading the detailed description which will follow, given as example.
La réduction de l'effort nécessaire à l'ouverture passe par l'utilisation d'un acier ayant une limite d'élasticité relativement basse, ce qui de plus facilite l'enroulement du panneau d'ouverture après rupture de l'incision, et par un rapport Re/Rm élevé.Reducing the effort required to open involves the use of a steel with a limit relatively low elasticity, which further facilitates the winding of the opening panel after breaking of the incision, and by a high Re / Rm ratio.
Au contraire la bonne aptitude à la formation du rivet passe par l'utilisation d'un acier ayant un rapport Re/Rm faible.On the contrary, the good aptitude for training the rivet requires the use of a steel having a ratio Low Re / Rm.
L'aspect de l'emballage ainsi que sa résistance à la corrosion sont améliorés par l'utilisation d'une tôle ayant une structure à grains fins équiaxes et ne presentant pas de palier de limite d'élasticité.The appearance of the packaging and its resistance corrosion are improved by the use of a sheet having an equiaxed fine-grained structure and not exhibiting no yield strength plateau.
L'obtention des caractéristiques mécaniques demandées et la micro structure équiaxe sont le résultat de :
- l'utilisation d'une tôle constituée d'un acier ayant une composition déterminée,
- l'adaptation d'un procédé de fabrication de tôle comportant un recuit sur base et un relaminage à froid.
- the use of a sheet made of steel having a determined composition,
- the adaptation of a sheet metal manufacturing process comprising annealing on base and cold re-rolling.
De manière plus précise l'emballage selon l'invention est réalisé à partir d'une tôle en acier dont la teneur en carbone est comprise entre 0,02 et 0,08% en poids et la teneur en bore est comprise 0,002 et 0,004 % en poids, l'acier contenant également de l'azote dans une quantité inférieure à 0,005 %, le rapport de la teneur en bore sur la teneur en azote étant supérieur 0,8.More precisely the packaging according to the invention is made from a steel sheet of which the carbon content is between 0.02 and 0.08% by weight and boron content is 0.002 and 0.004% by weight, the steel also containing nitrogen in a amount less than 0.005%, the ratio of the content of boron on the nitrogen content being greater than 0.8.
Une teneur en carbone inférieure à 0,02% est difficilement réalisable avec les procédés d'élaboration classiques et peut conduire à une résistance mécanique insuffisante du couvercle.A carbon content of less than 0.02% is difficult to achieve with production processes conventional and can lead to mechanical resistance insufficient cover.
Si la teneur en carbone était supérieure à 0,08 % en poids, la charge à la rupture Rm de la tôle destinée à réaliser l'emballage serait trop importante.If the carbon content was greater than 0.08% by weight, the breaking load Rm of the sheet intended to carry out the packaging would be too important.
On a constaté que pour obtenir une tôle permettant de réaliser un emballage selon l'invention, dont la structure est equiaxe, le rapport de la teneur en bore sur la teneur en azote doit être supérieur à 0,8, le bore étant limité à 0,004 % car, pour une teneur supérieure, on a une augmentation des caractéristiques mécaniques de la tôle et on voit apparaítre une oxydation préférentielle en rive du produit, ce qui est rédhibitoire du point de vue esthétique.It has been found that to obtain a sheet allowing to produce packaging according to the invention, including the structure is equiaxial, the ratio of the boron content on the nitrogen content must be greater than 0.8, boron being limited to 0.004% because, for a higher content, has an increase in the mechanical characteristics of the sheet metal and we see a preferential oxidation appear in side of the product, which is unacceptable from the point of view aesthetic.
La composition pondérale de l'acier constituant la tôle destinée à l'emballage selon l'invention, est de préférence la suivante, en millième de pour cent:
- carbone : 50
- manganèse : 200
- phosphore : 10
- azote : 3,5
- aluminium : 30
- silicium : 5
- bore : 3
- le reste étant du fer et des impuretés résiduelles.
- carbon: 50
- manganese: 200
- phosphorus: 10
- nitrogen: 3.5
- aluminum: 30
- silicon: 5
- boron: 3
- the remainder being iron and residual impurities.
Le procédé utilisé pour réaliser la tôle adaptée pour l'emballage selon l'invention, consiste en ce qu'après laminage en continu de l'acier décrit ci-dessus, la tôle est soumise à un recuit sur base effectué pendant 8 à 10 heures à une température comprise entre 550 et 650°C environ, la montée en température depuis la température ambiante étant effectuée en 20 heures environ. La tôle est ensuite soumise à un relaminage à froid avec un taux d'allongement compris entre 5 et 10 %. The process used to make the suitable sheet for packaging according to the invention, consists in that after continuous rolling of the steel described above, the sheet is subjected to an annealing on base carried out during 8 at 10 a.m. at a temperature between 550 and 650 ° C approximately, the rise in temperature from the temperature ambient being carried out in approximately 20 hours. The sheet is then subjected to a cold re-rolling with a rate elongation between 5 and 10%.
L'association de la composition de l'acier et du procédé de fabrication adapté permet d'obtenir les caractéristiques mécaniques suivantes :
- Re = 310 MPa environ,
- Rm = 340 MPa environ.
- Re = 310 MPa approximately,
- Rm = 340 MPa approximately.
Le rapport de la limite d'élasticité sur la charge à la rupture est compris entre 0,91 et 0,92.The ratio of the elastic limit to the breaking load is between 0.91 and 0.92.
On obtient ainsi un emballage dont l'ouverture est assez aisée et ayant une bonne aptitude à la formation du rivet.This produces a package whose opening is fairly comfortable and has good training ability of the rivet.
D'autre part, un tel acier permet de supporter une indentation importante avant endommagement rédhibitoire, c'est à dire que l'incision peut être plus profonde, permettant de ce fait un effort d'ouverture moindre.On the other hand, such steel allows to support significant indentation before unacceptable damage, that is, the incision can be deeper, thereby allowing an effort of openness lesser.
En effet, dans le cas de l'acier bas carbone standard, l'épaisseur restante en fond d'incision ne doit pas être inférieure à 70 microns sous peine d'endommagement rédhibitoire, alors que cette épaisseur restante en fond d'incision peut descendre jusqu'à 50 microns dans le cas de l'acier selon l'invention.Indeed, in the case of low carbon steel standard, the remaining thickness at the bottom of the incision should not not be less than 70 microns under penalty of damage unacceptable, while this remaining thickness in bottom of incision can go down to 50 microns in the case of the steel according to the invention.
Cet emballage réalisé à partir d'une tôle à structure équiaxe à grains fins évite, lors de la formation du rivet, l'apparition de rugosités de déformation dues à des affaissements, qui sont préjudiciables à l'aspect de l'emballage et à la tenue d'un vernis éventuel.This packaging made from a sheet metal fine-grained equiaxed structure avoids, during training of the rivet, the appearance of deformation roughness due to subsidence, which is detrimental to the appearance of the packaging and the holding of any varnish.
La présence de bore permet également de freiner la coalescence de la cémentite ce qui se traduit par une plus grande régularité de l'effort à fournir lors de l'ouverture de l'emballage.The presence of boron also makes it possible to brake the coalescence of the cementite which results in a greater regularity of effort to be provided during opening the package.
Claims (5)
- Metallic container of the type which is opened by tearing along a line of least resistance provided in a part of the sheet steel wall, characterised in that the steel which forms the sheet has a carbon content lying between 0.02 and 0.08% by weight and a boron content of between 0.002 and 0.004% by weight, the steel also containing nitrogen, the ratio of the boron content to the nitrogen content being greater than 0.8, the balance being iron and residual impurities, the said sheet being subjected to continuous lamination followed by basic annealing carried out over 8 to 10 hours at a temperature lying between about 550 and 650°C, then subjected to cold relamination with an elongation rate between 5 and 10%.
- Container according to claim 1, characterised in that the composition by weight of the steel which forms the sheet is preferably the following, in thousandths of a percent:carbon: 50manganese : 200phosphorus : 10nitrogen : 3.5aluminium : 30silicon : 5boron : 3the balance being iron and residual impurities.
- Container according to claim 1, characterised in that the rise in temperature in the basic annealing in relation to the ambient temperature is carried out over about 20 hours.
- Sheet steel for a container according to any one of claims 1 to 3, characterised in that the ratio of its elastic limit to its rupture strength lies between 0.87 and 0.96.
- Sheet steel according to claim 4, characterised in that the ratio of its elastic limit to its rupture strength lies between 0.91 and 0.92.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR9211788A FR2696421B1 (en) | 1992-10-05 | 1992-10-05 | Steel for opening packaging by breaking a line of least resistance. |
FR9211788 | 1992-10-05 |
Publications (2)
Publication Number | Publication Date |
---|---|
EP0592267A1 EP0592267A1 (en) | 1994-04-13 |
EP0592267B1 true EP0592267B1 (en) | 1998-06-24 |
Family
ID=9434156
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP93402311A Expired - Lifetime EP0592267B1 (en) | 1992-10-05 | 1993-09-21 | Metal can with closure of the easy-to-open type by tearing along a line of weakness and steel sheet for its manufacture |
Country Status (6)
Country | Link |
---|---|
EP (1) | EP0592267B1 (en) |
JP (1) | JP3304173B2 (en) |
AT (1) | ATE167704T1 (en) |
DE (1) | DE69319292T2 (en) |
ES (1) | ES2118918T3 (en) |
FR (1) | FR2696421B1 (en) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL1003762C2 (en) * | 1996-08-08 | 1998-03-04 | Hoogovens Staal Bv | Steel type, steel strip and method of manufacture thereof. |
KR20010101348A (en) * | 1998-12-30 | 2001-11-14 | 추후기재 | Steel band with good forming properties and method for producing same |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3725143A (en) * | 1971-02-03 | 1973-04-03 | Steel Corp | Aging resistant cold rolled sheet products |
JPS5144486B2 (en) * | 1971-09-30 | 1976-11-29 | ||
FR2179008B1 (en) * | 1972-04-03 | 1975-12-26 | Nippon Steel Corp | |
US3950191A (en) * | 1974-10-21 | 1976-04-13 | Kawasaki Steel Corporation | Cold rolled steel sheets having an excellent enamelability and a method for producing said cold rolled steel sheets |
-
1992
- 1992-10-05 FR FR9211788A patent/FR2696421B1/en not_active Expired - Fee Related
-
1993
- 1993-09-21 ES ES93402311T patent/ES2118918T3/en not_active Expired - Lifetime
- 1993-09-21 AT AT93402311T patent/ATE167704T1/en not_active IP Right Cessation
- 1993-09-21 DE DE69319292T patent/DE69319292T2/en not_active Expired - Fee Related
- 1993-09-21 EP EP93402311A patent/EP0592267B1/en not_active Expired - Lifetime
- 1993-10-05 JP JP24926293A patent/JP3304173B2/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
ATE167704T1 (en) | 1998-07-15 |
DE69319292T2 (en) | 1998-11-12 |
ES2118918T3 (en) | 1998-10-01 |
EP0592267A1 (en) | 1994-04-13 |
DE69319292D1 (en) | 1998-07-30 |
JP3304173B2 (en) | 2002-07-22 |
FR2696421A1 (en) | 1994-04-08 |
FR2696421B1 (en) | 1995-01-06 |
JPH06220575A (en) | 1994-08-09 |
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