EP0417288A1 - Appareil de sechage et de combustion de matieres inflammables solides a haute teneur en humidite - Google Patents

Appareil de sechage et de combustion de matieres inflammables solides a haute teneur en humidite Download PDF

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Publication number
EP0417288A1
EP0417288A1 EP89911098A EP89911098A EP0417288A1 EP 0417288 A1 EP0417288 A1 EP 0417288A1 EP 89911098 A EP89911098 A EP 89911098A EP 89911098 A EP89911098 A EP 89911098A EP 0417288 A1 EP0417288 A1 EP 0417288A1
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EP
European Patent Office
Prior art keywords
drying
solid
furnace
drier
gas
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP89911098A
Other languages
German (de)
English (en)
Other versions
EP0417288A4 (en
EP0417288B1 (fr
Inventor
Takashi 10-30 Wakabayashi Kikuchi
Shoji 105-1 Aza-Shinkawamukai Sakurai
Ikurou 2-16 Nishitaga 3-Chome Shisido
Touru 8-8 Kongou-Zawa Taihaku-Ku Yoshida
Hideo 6-5 Honcho Seki
Shinya 14-28 Kaigamori 3-Chome Aoba-Ku Watanabe
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
MIYAGI KEN
Takahashi Syokuhin Kogyo KK
Kameyama Tekkosho KK
Original Assignee
Takahashi Syokuhin Kogyo KK
Kameyama Tekkosho KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Takahashi Syokuhin Kogyo KK, Kameyama Tekkosho KK filed Critical Takahashi Syokuhin Kogyo KK
Priority to AT89911098T priority Critical patent/ATE107404T1/de
Publication of EP0417288A1 publication Critical patent/EP0417288A1/fr
Publication of EP0417288A4 publication Critical patent/EP0417288A4/en
Application granted granted Critical
Publication of EP0417288B1 publication Critical patent/EP0417288B1/fr
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
    • F23G—CREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
    • F23G5/00—Incineration of waste; Incinerator constructions; Details, accessories or control therefor
    • F23G5/02—Incineration of waste; Incinerator constructions; Details, accessories or control therefor with pretreatment
    • F23G5/04—Incineration of waste; Incinerator constructions; Details, accessories or control therefor with pretreatment drying
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
    • F23G—CREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
    • F23G5/00—Incineration of waste; Incinerator constructions; Details, accessories or control therefor
    • F23G5/02—Incineration of waste; Incinerator constructions; Details, accessories or control therefor with pretreatment
    • F23G5/033—Incineration of waste; Incinerator constructions; Details, accessories or control therefor with pretreatment comminuting or crushing
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
    • F23G—CREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
    • F23G5/00—Incineration of waste; Incinerator constructions; Details, accessories or control therefor
    • F23G5/44—Details; Accessories
    • F23G5/46—Recuperation of heat
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
    • F23G—CREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
    • F23G7/00—Incinerators or other apparatus for consuming industrial waste, e.g. chemicals
    • F23G7/001—Incinerators or other apparatus for consuming industrial waste, e.g. chemicals for sludges or waste products from water treatment installations
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
    • F23G—CREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
    • F23G7/00—Incinerators or other apparatus for consuming industrial waste, e.g. chemicals
    • F23G7/04—Incinerators or other apparatus for consuming industrial waste, e.g. chemicals of waste liquors, e.g. sulfite liquors
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B23/00—Heating arrangements
    • F26B23/02—Heating arrangements using combustion heating
    • F26B23/028—Heating arrangements using combustion heating using solid fuel; burning the dried product
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
    • F23G—CREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
    • F23G2206/00—Waste heat recuperation
    • F23G2206/10—Waste heat recuperation reintroducing the heat in the same process, e.g. for predrying

Definitions

  • the present invention relates to an apparatus for drying and burning high-hydrous combustible solids or wet wastes, and more particularly to an improvement in or relating to a drying and burning system in which high-hydrous combustible solids such as bean-curd refuse, are put in and dried in an associated drier; the dried solids are brought and burnt in an associated furnace; and the hot waste gas is fed from the furnace to the drier to dry the wet waste.
  • high-hydrous combustible solids such as bean-curd refuse
  • high-hydrous combustible solids or wet wastes such as bean-curd refuse, sewage or raw sewage are treated by dewatering, drying and burning. Specifically, wet waste is subjected to these treatment sequentially in dehydrator, drier and furnace. These equipments were separate or independent from each other, not making up a composite or integrated system. In an attempt to meet energy-saving demand or reduce public nuisance the drier and furnace were combined to provide an integrated system.
  • the hot waste gas which is produced when drying the wet waste in the drier is fed to the furnace to be burnt and deodrized.
  • a part of so deodorized gas is fed to the drier, and is used as drying gas.
  • This system constitutes a closed deordizing system, and is advantageous from the energy saving point of view.
  • the conventional system dries the wet waste in its drier, and burns the odor gas in its furnace for the sake of deodorizing rather than burning. Therefore, the conventional system requires another furnace for burning the deodorized material to ash. Accordingly, the whole size disadvantageously increases.
  • the deodorizing furnace cannot be used to burn the dried waste because it is connected to the drier by a pipe whose size is large enough to allow the odor gas to pass to the furnace, preventing the dried waste from passing to the furnace.
  • One object of the present invention is to provide an apparatus for drying and burning high-hydrous combustible solids or wet wastes, in which high-hydrous combustible solids are dried in an associated drier, and the dried solids are brought and burnt to ash in an associated furnace while the deodorized gas is fed from the furnace to the drier to dry the wet waste therein.
  • the furnace is used as deodorizing furnace, too.
  • Another object of the present invention is to provide means for breaking dewatered waste into fragments by blowing air, which is used t o carry fragments of dried material to the furnace, thereby increasing the efficiency with which the waste material may be burnt in the furnace because of substantially increased surface area of the pulverized waste material.
  • Blowing air is used for expediting combustion in the furnace.
  • a single blower may be used for transporting dry waste material, breaking the material into fragments and supplying a sufficient amount of air to burn the fragments of waste material in the furnace.
  • an apparatus for drying and burning high-hydrous combustible solids is characterized in that it comprises: hopper 20 for containing high-hydrous combustible solids; drier 1 to receive high-hydrous combustible solids from hopper 20 for drying; furnace 23 to receive the dewatered combustible solids from drier 1 via pipe 22 for burning; and means for leading the deodorized gas from furnace 23 to drier 1, thus permitting use of the deodorized gas as drying gas.
  • Solid-gas separator 26 is provided in dried material transporting conduit 22 between drier 1 and furnace 23.
  • Hopper 20 communicates with solid-gas separator 26 by duct 39 including blower 38, thereby permitting the air-and-odor gas from the high-hydrous combustible solids in hopper 20 to flow to solid-gas separator 26 via air duct 39 and break there the dewatered combustible solids into fragments, thus increasing the burning efficiency in furnace 23.
  • the air flows out from ejector 27 at the lower part of solid-gas separator 26, transporting the so separated solid material into furnace 23. Also, the air is used as burning air in furnace 23.
  • Air duct 39 is in the form of branch downstream of blower 38, one branch being connected to solid-gas separator 26 while the other branch being connected to furnace 23 to supply secondary air.
  • Steam jacket 46 is provided to the circumference of combustion chamber 53 of furnace 23.
  • the steam thus generated by steam jacket 46 can be used in producing any products, and the resulting wet waste can be treated in the drying and burning system.
  • the wet waste in hopper 20 is dried in drier 1, and then the dried waste is transferred into furnace 23, where it is burnt by burner 24, and at the same time, the waste gas is sent to drier 1.
  • the waste gas is used as drying gas in drier 1.
  • the gas separated from the dried solid fragments in solid-gas separater 26 leaves exhaust duct 34 via exhaust tube 31 and cyclone 32.
  • blower 38 When blower 38 is put in operation, the air is drawn from hopper 20, and therefore the odor is removed from the wet waste in hopper 20. Also, the flowing air is used as secondary air for expediting combustion in furnace 23.
  • Steam jacket 46 surrounding combustion chamber 53 of furnace 23 generates steam, which may be used in producing any products. In the course of production wet waste may be left over, which waste, however, may be disposed by the drying-and-burning system.
  • Fig. 1 is a front view of the drier, partly broken to show some essential parts of the drier;
  • Fig. 2 shows how circular wind motion is used for drying and fracturing
  • Fig. 3 is a plane view of a perforated distribution plate
  • Fig. 4 is a side view of the perforated distribution plate
  • Fig. 5 is a plane view of a screw
  • Fig. 6 is a side view of the screw
  • Fig. 7 is a plane view of the blade
  • Fig. 8 is a side view of the blade
  • Fig. 9 is a plane view of an obstacle plate
  • Fig. 10 is a side view of the obstacle plate
  • Fig. 11 is a plane view of a fracturing blade
  • Fig. 12 is a side view of the fracturing blade.
  • Fig. 13 is a diagramatic view of the drying-and-burning apparatus. Best Mode of Carrying out the Present Invention:
  • Figs. 1 to 12 show drier 1 which may be used in the present invention.
  • a cylindrical drier is indicated at 1, and this drier has gas supplying vent 2 at its lower part; dried waste exhausting opening 3 at its upper part; and wet waste inlet opening 4 at a somewhat higher level than the intermediate level of the cylinder. These openings and vent are arranged longitudinally.
  • Cylindrical drier 1 has rotating shaft 5 along its longitudinal central axis, electric motor 5 is used to rotate shaft 5.
  • Perforated distribution plate 7 is laid adjacent to gas vent 2 at the bottom level of cylindrical drier 1 for distributing hot air.
  • Screw 9 is fixed to rotating shaft 5 above perforated distribution plate 7. Screw 9 is adapted to be rotated by shaft 5.
  • Blade 10 is provided at a higher level than screw 9. Screw 9 and blade 10 are arranged in such positions that dried waste may be brought upward by screw 9, and then may be made to fly by spiral wind motion, which is caused by blade 10.
  • An obstacle plate 11 is fixed to rotating shaft 5 at a higher level than blade 10. Obstacle plate 11 has small apertures 12 and pins 13 on its opposite surfaces. There is an annular gap between the circumference 16 of obstacle plate 11 and inside surface 17 of cylindrical drier 1. The gap is broad enough to allow pieces of dried waste solid. Circular wind motion zone 18 is defined between obstacle plate 11 and blade 10.
  • Inlet 4 for pieces of wet waste opens at the second circular wind motion zone 18, in which fracturing cross blade 14 having fracturing pins 15, is fixed to rotating shaft 5.
  • Hopper for containing wet waste is indicated at 20.
  • Hopper 20 communicates with inlet 4 of drier 1 via screw conveyer 21.
  • Exit 3 for discharging fragments of dried waste solid communicates with furnace 23 via transportation conduit 22. More specifically, exit 3 communicates with the circular wind motion zone 25 of burner 24 in furnace 23 via transportation conduit 22.
  • Solid-gas separater 26 is situated in transportation conduit 22. Specifically, solid-gas separater 26 has transportation conduit 22 at its upper level, and ejector 27 at its lower level. Ejector 27 is connected on its primary side to gas chamber 29, which is provided to side wall 28 of solid-gas separater 26, and ejector 27 is connected on its secondary side to the circular wind motion zone 25 of furnace 23.
  • Exhaust duct 31 extends from the upper part of the separating space 30 of funnel-shaped solid-gas separator 26, thus permitting ejection of the gas from solid-gas separator 26 through cyclon 32, drawing fan 33 and exhaust duct 34. Dust box 35 is attached to the bottom of cyclon 32.
  • Hopper 20 is designed to contain high-hydrous combustible solids or wet waste such as bean-curd refuse, and it has inlet 35' for wet waste on its ceiling, and air inlet 36 on its side.
  • Another inlet 37 of hopper 20 is connected to inlet 40 of solid-gas separator 26 via air duct 39, which has blower 38.
  • Wastegas outlet 41 of furnace 23 is connected to gas inlet 2 of drier 1 by wastegas return tube 42.
  • Air duct 39 has a secondary air inlet tube 44 extending therefrom in the form of branch 43 downstream of blower 38, and connected to secondary air nozzle 45, which opens in combustion chamber 53.
  • This combustion chamber 53 has steam jacket 46 surrounding therearound, and water supply tank 48 having water softner 47 associated therewith, is connected to steam jacket 46 by water supply tube 49.
  • the steam generated by steam jacket 46 may be used in producing related products.
  • Wasteoil tank 51 is connected to burner 24 by wasteoil supply pipe 52.
  • High-hydrous combustible solids or wet wastes such as bean-curd refuse are put in hopper 20 from its inlet 35'. Then, wet waste is transported to inlet 4 of drier 1 by screw conveyer 21, and bulks of wet waste are thrown in drier 1 where they are broken into fragments by pins 15 of fracturing blade 14. The fragments of wet waste fall downward. In the course of descent by gravity the fragments of wet waste are struck and sprung upwards by rotating blade 10 on the second stage. While this takes place, the fragments of wet waste is brought in counter contact with rising flow of hot gas, thereby expediting the drying of wet waste. At the outset the fragments of wet waste have relatively high water content, and therefore they are relatively heavy.
  • Rotating obstacle plate 11 has pins 13 thereon, and falling fragments are struck and sprung as indicated by arrow B in Fig. 2 so that they are struck against the inside surface 17 of drier 1, and they fall down along the inside surface 17 of drier 1 in the annular space between the circumference 16 of rotating blade 11 and the inside surface 17 of drier 1.
  • fragments of waste are in contact with hot wind, and accordingly they are being dried all the time.
  • rotating screw 9 gas supply inlet 2 and the apertures of destribution plate 7 cannot be blocked with fragments.
  • fragments of waste are transferred to rotating blade 10, and as indicated by arrow F in Fig. 2, again they are sprung up by rotating blade 10. Then, Smaller fragments of waste are carried upwards by circular wind motion, which is caused by rotating blade 10. During the process described so far fragment size is reduced gradually, and accordingly the surface of each fragment increases, thus increasing the efficiency with which fragments of waste are brought in contact with gas. Also, as indicated by arrow G, fragments of waste are struck and sprung against the inner surface 17 of drier 1 by pins 13 on the lower surface of obstacle plate 11. Again, fragments of waste are broken and reduced in size. Then, they fall down along the inner surface 17 of drier 1.
  • pieces of wet waste material are brought by circular wind motion in zone 18 as indicated by arrows C-D-E-F-G-C until they are broken to small fragments, accordingly increasing the surface area of each fragment and expediting the drying of wet waste.
  • Particles of dried solid is carried by hot wind which blows upwards from the apertures 12 of obstacle plate 11.
  • particles of dried solid are subjected to same treatment in circular wind motion zone 18 at the second stage, where solid particles are reduced in size, and dried even more. In this second stage the temperature of heated gas lowers somewhat, and the heated gas come to contain water. Therefore, heat and water will be deprived with an extremely high efficiency.
  • blower 38 When blower 38 is driven, air is supplied to the solid-gas separating space 40 of solid-gas separator 26 via inlet 37 of hopper 20 and air duct 39, thus collecting the odor from the inside of hopper 20.
  • the supplying of air to solid-gas separator permits separation of dried particles into solid and gas, and solid particles are reduced in size.
  • the gas is discharged through air duct 31, cyclon 32 and exhaust duct 34.
  • a part of supplied air is led to ejector 27 via air chamber 29, and pulverized solid is drawn and brought to circular wind motion zone 25 of furnace 23, where it is burnt by burner 24.
  • the pulverized solid can be burnt well because of its minute particle size.
  • This combustion is effected by using the air which carries the pulverized solid.
  • the combustion uses the secondary air which is drawn into combustion chamber 53 through secondary air supply conduit 44 branching downstream of blower 38.
  • Dried particles are burnt there, and the waste gas flows back to gas inlet 2 of drier 1 via gas return pipe 42 to be used in drying process.
  • the wet waste is dried in drier 1, and then the dried solid is brought to furnace 23, where it is burnt.
  • furnace 23 This permits reduction of the size of the wet waste disposing system in designing.
  • the waste gas from furnace 23 is made to return to drier 1 to be used as drying gas, and accodingly energy is saved.
  • a single blower 38 is used to effect transportation of waste solid from drier 1 to furnace 23, reduction of dried waste solid in size, supply of air for combustion and collection of the odor from the wet waste in hopper 20.

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Combustion & Propulsion (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Sustainable Development (AREA)
  • Water Supply & Treatment (AREA)
  • Drying Of Solid Materials (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

La présente invention se rapporte à un appareil de séchage et de combustion de matières inflammables solides à haute teneur en humidité, qui comprend une trémie (20) servant à stocker les matières inflammables solides à haute teneur en humidité, un séchoir (1) servant à sécher les matières inflammables solides à haute teneur en humidité chargées à partir de la trémie (20) ainsi qu'un incinérateur (23) servant à recevoir les matières solides séchées par le séchoir (1) à travers un conduit de transfert (22) et à les brûler, et qui permet d'introduire les gaz d'échappement provenant de l'incinérateur (23) dans le séchoir (1) et de les utiliser comme gaz de séchage. Après que les matières inflammables solides à haute teneur en humidité aient été séchées par le séchoir (1), elles sont immédiatement transférées et brûlées dans l'incinérateur (23). Les gaz d'échappement provenant de l'incinérateur (23) sont utilisés comme gaz de séchage par le séchoir (1).
EP89911098A 1989-03-30 1989-10-04 Appareil de sechage et de combustion de matieres inflammables solides a haute teneur en humidite Expired - Lifetime EP0417288B1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AT89911098T ATE107404T1 (de) 1989-10-04 1989-10-04 Trocknungs- und verbrennungsvorrichtung für feste entflammbare materialien mit hoher feuchtigkeit.

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP7933989 1989-03-30
PCT/JP1989/001023 WO1990012250A1 (fr) 1989-03-30 1989-10-04 Appareil de sechage et de combustion de matieres inflammables solides a haute teneur en humidite

Publications (3)

Publication Number Publication Date
EP0417288A1 true EP0417288A1 (fr) 1991-03-20
EP0417288A4 EP0417288A4 (en) 1992-04-01
EP0417288B1 EP0417288B1 (fr) 1994-06-15

Family

ID=13687143

Family Applications (1)

Application Number Title Priority Date Filing Date
EP89911098A Expired - Lifetime EP0417288B1 (fr) 1989-03-30 1989-10-04 Appareil de sechage et de combustion de matieres inflammables solides a haute teneur en humidite

Country Status (4)

Country Link
EP (1) EP0417288B1 (fr)
KR (1) KR940010659B1 (fr)
DE (1) DE68916245T2 (fr)
WO (1) WO1990012250A1 (fr)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0692679A3 (fr) * 1994-07-13 1997-01-02 Kloeckner Humboldt Deutz Ag Procédé et schéma d'installation pour le séchage et l'incinération de boues d'égout
WO1997007904A1 (fr) * 1995-08-29 1997-03-06 Jean Couturier Procede pour la valorisation et la reutilisation des cendres volantes des centrales thermiques fonctionnant au charbon
AT406509B (de) * 1996-01-18 2000-06-26 Andritz Patentverwaltung Verfahren und anlage zur trocknung von schlamm, insbesondere klärschlamm
WO2021064606A1 (fr) * 2019-09-30 2021-04-08 Ceres Intellectual Property Company Limited Dispositif de refroidissement et de déshydratation de gaz d'échappement et véhicule sofc

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60221613A (ja) * 1984-04-18 1985-11-06 Kawasaki Heavy Ind Ltd 脱水汚泥の焼却方法

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SE419974C (sv) * 1978-10-10 1984-06-12 Modo Chemetics Ab Forfarande for torkning och brenning av vattenhaltiga fasta brenslen
JPS6014257B2 (ja) * 1979-05-16 1985-04-12 日本フア−ネス工業株式会社 下水汚泥処理用不完全燃焼炉
JPS6467300A (en) * 1987-09-08 1989-03-13 Toshiba Corp Combustion dryer

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60221613A (ja) * 1984-04-18 1985-11-06 Kawasaki Heavy Ind Ltd 脱水汚泥の焼却方法

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
PATENT ABSTRACTS OF JAPAN vol. 10, no. 81 (M-465)(2138) 29 March 1986 & JP-A-60 221 613 ( KAWASAKI JUKOGYO K.K. ) 6 November 1985 *
See also references of WO9012250A1 *

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0692679A3 (fr) * 1994-07-13 1997-01-02 Kloeckner Humboldt Deutz Ag Procédé et schéma d'installation pour le séchage et l'incinération de boues d'égout
WO1997007904A1 (fr) * 1995-08-29 1997-03-06 Jean Couturier Procede pour la valorisation et la reutilisation des cendres volantes des centrales thermiques fonctionnant au charbon
FR2738169A1 (fr) * 1995-08-29 1997-03-07 Couturier Jean Procede pour la valorisation et la reutilisation des cendres volantes des centrales thermiques fonctionnant au charbon
AT406509B (de) * 1996-01-18 2000-06-26 Andritz Patentverwaltung Verfahren und anlage zur trocknung von schlamm, insbesondere klärschlamm
WO2021064606A1 (fr) * 2019-09-30 2021-04-08 Ceres Intellectual Property Company Limited Dispositif de refroidissement et de déshydratation de gaz d'échappement et véhicule sofc

Also Published As

Publication number Publication date
KR940010659B1 (ko) 1994-10-24
EP0417288A4 (en) 1992-04-01
KR920700378A (ko) 1992-02-19
WO1990012250A1 (fr) 1990-10-18
DE68916245T2 (de) 1995-01-19
EP0417288B1 (fr) 1994-06-15
DE68916245D1 (de) 1994-07-21

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