EP0201311A2 - Extraktionsanlage und Extractionsprozess - Google Patents

Extraktionsanlage und Extractionsprozess Download PDF

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Publication number
EP0201311A2
EP0201311A2 EP86303422A EP86303422A EP0201311A2 EP 0201311 A2 EP0201311 A2 EP 0201311A2 EP 86303422 A EP86303422 A EP 86303422A EP 86303422 A EP86303422 A EP 86303422A EP 0201311 A2 EP0201311 A2 EP 0201311A2
Authority
EP
European Patent Office
Prior art keywords
pool
extractor
floor
pools
solvent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP86303422A
Other languages
English (en)
French (fr)
Other versions
EP0201311B1 (de
EP0201311A3 (en
Inventor
William L. Kratochwill
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Crown Iron Works Co
Original Assignee
Crown Iron Works Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Crown Iron Works Co filed Critical Crown Iron Works Co
Publication of EP0201311A2 publication Critical patent/EP0201311A2/de
Publication of EP0201311A3 publication Critical patent/EP0201311A3/en
Application granted granted Critical
Publication of EP0201311B1 publication Critical patent/EP0201311B1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0215—Solid material in other stationary receptacles
    • B01D11/0223—Moving bed of solid material
    • B01D11/023—Moving bed of solid material using moving bands, trays fixed on moving transport chains

Definitions

  • the present invention is related to the field of equipments for extracting a liquid from a solid carrier medium in which the liquid is entrained.
  • Such equipments utilize a solvent for treating the liquid entraining solid carrier medium in order to extract the liquid.
  • Methods utilizing these equipments perform extraction basically in one of two ways: percolation and immersion.
  • a preferred embodiment of the present invention operates utilizing both of these methods.
  • Tar sand deposits are located at numerous locations around the world, and a number of deposits are located on the North American continent. These locations are primarily in the states of California, Kentucky, Oklahoma, Texas, and Utah of the United States and at various locations in Canada.
  • the particular products being worked in extraction processes can vary quite significantly.
  • the solid carrier is fairly homogenously granular.
  • the viscosity of the liquid by-product to be recovered the consistency of the product being worked tends to be clumpy, the size of agglomerations varying significantly.
  • the distribution of the petroleum product throughout the tar sand mass is not uniform, and what might prove to be sufficient processing for a portion of the mass might prove inadequate for other portions.
  • Percolation a method wherein the solvent flows -through the extractable material, might function well to remove oils from meal because of the relatively uniform granularity of the meal.
  • tar sands With tar sands, however, percolation is difficult because of the compactness of the raw product to be processed. Nevertheless, percolation, if it can be performed, is a method of extraction which provides advantages in extracting the liquid by-product from its solid carrier.
  • the present invention is directed. It is an improved extractor which functions well to process heavy sedimentary, liquid-entraining solids to remove and recover the liquid by-products entrained in those solids. Although particularly useful for processing tar sand deposit materials to recover petroleum products embedded in such sands, it will be understood that the invention is designed to function equally as well in processing other heavy sedimentary solids.
  • the present invention is an extractor for separating liquids embedded in heavy sedimentary solids from the solid carrier medium. It includes a plurality of pools arranged relative to one another so that a liquid solvent introduced into the uppermost of the pools will cascade successively into subsequently lower pools. Means are provided for introducing a solvent agent into an uppermost of the pools. The solvent overflows through an outlet end of the uppermost pool and into an inlet end of the next lower pool. The solvent, in turn, overflows through an outlet end of that pool into the inlet end of the next successive pool.
  • Means are provided for depositing raw, liquid-entraining, solid carrier medium into the lowermost of the pools and for conveying the solid medium upwardly along a floor of each pool which slopes downwardly from the inlet end of the pool to the outlet end. The solid medium is, thereby, conveyed upwardly into the next subsequently higher pool.
  • Each pool can be constructedI-with an inlet at the inlet end being spaced vertically above an overflow at the outlet end.
  • the floor of the pool can have its upper end at the inlet to the pool and its lower end spaced vertically downwardly from the overflow.
  • a solvent introduced into the uppermost pool will rise to a level at the overflow of that pool.
  • sedimentary solids entraining the liquid to be extracted are being conveyed counter-current into the upper pool from the immediately lower pool.
  • percolation will occur with respect to the solids entering the uppermost pool.
  • those solids are deposited onto the lower end of the floor of the uppermost pool, they will be submerged beneath the solvent in the pool, and immersion extraction will occur.
  • a preferred embodiment of the invention includes a bath, constructed similarly to each of the pools, and disposed above the uppermost pool. As in the case of transmission of the sedimentary solids upwardly through the pools, the solids can be deposited from the uppermost pool into the bath.
  • the bath can be provided with a transmission means for passing the solids beneath sprinkler introduction of the solvent into the bath to effect a final percolation extraction stage upon the solids before they are recovered.
  • figure 1 illustrates an end view of an extractor 10 in accordance with the present invention.
  • the view illustrates an end at which solids, from which an extractable liquid entrained therein have been removed, are recovered from the extraction process.
  • a preferred embodiment of the invention envisions an extractor 10 relatively narrow as compared to the height dimension.
  • the width of the extractor 10 is even smaller relative to its length.
  • the extractor 10 is divided, along its longitudinal axis, into a plurality of pools 12, 12' and, in a preferred embodiment, a final stage bath 14.
  • a chute 16 extends downwardly from a leftmost end of the final bath 14, and solid materials having gone through the extraction process are deposited into the chute 16 for recovery.
  • FIG. 2 illustrates a cover 18 superimposed over the extractor 10, although it will be understood that, if desired, the extractor 10 could be open on its top.
  • an aperture 20 is provided therein to afford entry into the extractor 10 to sedimentary solids having an extractable liquid entrained therein.
  • One of a number of types of equipments known in the art can be utilized for conducting the sedimentary solids to the aperture 20 and dumping them therethrough. Such equipments might typically include augers or other components to effect movement of the solids.
  • the pool 12 has an inclined floor 22 which angles upwardly and to the left as seen in figure 2.
  • the uppermost end of the floor 22 is at a height the same as is the inlet 24 end (that is, the leftmost end) of the pool 12.
  • the floor 22 of the pool 12 thereafter, slopes downwardly until it intersects a wall 26 of the extractor 10 at the end at which the sedimentary solids are introduced.
  • a discharge aperture 28 is provided in that wall 26 at a height lower than the inlet end 24 of the pool.
  • a pair of sprockets 30 are mounted on axles 32 which are journaled between the side walls 34, 36 of the extractor 10, one of each of said sprockets 30 proximate each end of the pool 12.
  • An endless chain 38 extends around the sprockets 30 and is driven by the sprockets 30 in a clockwise direction as viewed in the figure.
  • a plurality of staves 40 extend generally transversely to a plane defined by the run of the chain 38, a portion of each stave 40 extending laterally from the chain 38 in opposite directions, when the chain 38 is positioned centrally between the walls 34, 36 of the extractor 10, substantially to its respective side wall 34, 36.
  • the stave portions can be welded to chain lengths 38 as at 42 as seen in figure 3. With the staves 40 so secured to the chain length 38, they will not impede passage of the chain 38 over the drive sprockets 30.
  • a single chain 38 having stave portions extending on both sides thereof is not an exclusive manner of conducting sedimentary solids along the floor 22 of a pool 12.
  • Dual chains, one running substantially along each side wall 34, 36 of the extractor 10 can also function to effect the intended purpose of the chain/stave conveyor assembly. When such dual chains would be used, each stave would comprise a single portion extending across between the chains.
  • a single chain and accompanying pair of drive sprockets is believed to be optimum in order to minimize the number of moving parts which might become clogged by the solids being processed.
  • a baffle 46 can be provided extending downwardly from the aperture 20 and angled away from the extractor wall 26.
  • the second lowermost pool 12' has an overflow 48' substantially coinciding with the inlet 44 to the lowermost pool 12. Solids moved through the lowermost pool 12, therefore, will be deposited into this second pool 12'.
  • the construction of this pool 12' is substantially identical to that of the lowermost pool 12.
  • the specific construction of baffles provided in order to direct solids away from the lower of conveyor drive sprockets 30', however, is different because of the smaller vertical distance through which the solids will tumble down to the floor 22' of the- pool 12'.
  • the angle of the baffle 50 relative to the vertical is greater in this second pool 12'.
  • the angle of the floor 22' of the pool 12', the floor's length, and the construction of the chain conveyor with its staves 40' can be, however, the same as in the lowermost pool 12.
  • the direction of rotation of the conveyor is clockwise as viewed in figure 2 and, consequently, sedimentary solids deposited on the floor 22' of the pool 12' will be moved upwardly therealong by the conveyor.
  • a liquid solvent is introduced into the uppermost pool 12' to flow in a direction counter-current to the direction of movement of the sedimentary solids through the extractor 10.
  • the solvent can be introduced through a sprinkler arrangement 52 into a final bath 14 through which the solids can pass.
  • the solvent will be introduced into the uppermost pool 12' by passing over an overflow 54 at the output end of the bath 14 and into the uppermost pool 12'.
  • As solvent is so introduced into the uppermost pool 12' it will wash through solids passing upwardly along the floor 22' of that pool 12' and proximate the inlet end 44' thereof. At such a location, percolation extraction will be effected.
  • a final bath 14 through which the solids will pass can be provided at a level above that of the uppermost pool 12'.
  • a floor 56 over which the solids are transmitted can be provided at a location elevated above the floor 58 of the bath 14.
  • a conveyor 57 similar in construction to those utilized in the various pools 12, 12' can be provided in the bath 14. The rotation of the conveyor 57, however, would be counter-clockwise as viewed in figure 2, the upper run of the conveyor 57 moving across the elevated floor 56.
  • the elevated floor 56 can be porous so that solvent sprinkled over solids passing up the elevated floor 57 will pass through the elevated floor 57 and fill the bath 14 to a level of its overflow 54.
  • the solvent will, thereafter, cascade into the uppermost pool 12' and, sequentially, into the other pools 12.
  • the final bath 14 stage of extraction is one of percolation since the solvent washes through the sedimentary solids passing up the elevated floor 57 of the bath 14.
  • the extractor 10 can incorporate a tank 60 for receiving miscella (that is, a solution of the solvent and extracted liquid) once it passes out of the terminal wall 26 of the lowermost pool 12. Similarly, the miscella can, thereafter, be worked to recover the liquid extract therefrom. Appropriate equipment 62 can be used in combination with the extractor 10 to effect this separation.
  • miscella that is, a solution of the solvent and extracted liquid

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Extraction Or Liquid Replacement (AREA)
EP86303422A 1985-05-06 1986-05-06 Extraktionsanlage und Extractionsprozess Expired - Lifetime EP0201311B1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US06/730,960 US4751060A (en) 1985-05-06 1985-05-06 Extractor
US730960 2003-12-09

Publications (3)

Publication Number Publication Date
EP0201311A2 true EP0201311A2 (de) 1986-11-12
EP0201311A3 EP0201311A3 (en) 1987-06-03
EP0201311B1 EP0201311B1 (de) 1991-08-07

Family

ID=24937496

Family Applications (1)

Application Number Title Priority Date Filing Date
EP86303422A Expired - Lifetime EP0201311B1 (de) 1985-05-06 1986-05-06 Extraktionsanlage und Extractionsprozess

Country Status (4)

Country Link
US (1) US4751060A (de)
EP (1) EP0201311B1 (de)
CA (1) CA1253672A (de)
DE (1) DE3680704D1 (de)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0804953A1 (de) * 1996-05-02 1997-11-05 Crown Iron Works Company Selbstreinigende Extraktionsvorrichtung
WO2016044237A1 (en) 2014-09-18 2016-03-24 Bridgestone Corporation Extractor and related methods
EP3419733A4 (de) * 2016-02-26 2019-11-06 Crown Iron Works Company Schirm für entnahmesystem

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4981785A (en) * 1988-06-06 1991-01-01 Ventrex Laboratories, Inc. Apparatus and method for performing immunoassays
US5853488A (en) * 1993-08-13 1998-12-29 Silver; Barnard Stewart Processes for extracting sugars from dates and for making novel food products
ZA945796B (en) * 1993-08-13 1995-03-14 Barnard Stewart Silver Method and apparatus for extracting with liquids soluble substances from subdivided solids
US5700464A (en) * 1993-08-13 1997-12-23 Silver; Barnard Stewart Process for extracting with liquids soluble substances from subdivided solids
US5891433A (en) * 1993-08-13 1999-04-06 Silver; Barnard Stewart Extracting soluble substances from subdivided solids with a water-base liquid extraction medium
US5409100A (en) * 1994-02-15 1995-04-25 Star Recycling, Inc. Recycling assembly having three conveying belts
US6440381B1 (en) 1998-01-15 2002-08-27 Cabot Corporation Continuous production of silica via ion exchange
JP2003531789A (ja) 2000-04-27 2003-10-28 シーメンス アクチエンゲゼルシヤフト コンベアシステムと物品の分離整列方法
CN101991970B (zh) * 2009-08-28 2013-06-19 新奥科技发展有限公司 物料连续提取系统和方法
US9826757B2 (en) 2013-03-15 2017-11-28 Advance International Inc. Automated method and system for recovering protein powder meal, pure omega 3 oil and purified distilled water from animal tissue
WO2015179530A1 (en) * 2014-05-20 2015-11-26 Crown Iron Works Company Extractor with screen washing system
US10668401B2 (en) 2015-08-07 2020-06-02 Crown Iron Works Company Extractor with settling zone near solvent discharge
US20180291307A1 (en) * 2015-08-07 2018-10-11 Crown Iron Works Company Extractor with drop zone mixing
US10899993B2 (en) 2015-08-07 2021-01-26 Crown Iron Works Company Extractor having a solvent drainage zone
BR112018002464A2 (pt) 2015-08-21 2018-09-18 Crown Iron Works Co disposição de extrator para processar materiais com partículas finas
US10988327B1 (en) * 2018-07-06 2021-04-27 Span Tech Llc Sortation system and related methods

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE91514C (de) * 1900-01-01
US2227605A (en) * 1938-09-19 1941-01-07 Corn Prod Refining Co Apparatus for extraction
US2359929A (en) * 1941-12-23 1944-10-10 Stauffer Chemical Co Process and apparatus for the treatment of fruit pomace
FR945754A (fr) * 1947-04-14 1949-05-13 Emile Gazagne Ets Procédé et dispositif de diffusion continue

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US448895A (en) * 1891-03-24 Apparatus for scalding vegetables or fruit
US1561043A (en) * 1924-10-08 1925-11-10 Roscoe C Zuckerman Potato cleaner and sterilizer
US1705544A (en) * 1925-01-23 1929-03-19 Sprague Sells Corp Machine for washing fruits and vegetables
US3565587A (en) * 1966-10-31 1971-02-23 Gen Electric Liquid sealed gas tight dissolver with vibrating tray means

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE91514C (de) * 1900-01-01
US2227605A (en) * 1938-09-19 1941-01-07 Corn Prod Refining Co Apparatus for extraction
US2359929A (en) * 1941-12-23 1944-10-10 Stauffer Chemical Co Process and apparatus for the treatment of fruit pomace
FR945754A (fr) * 1947-04-14 1949-05-13 Emile Gazagne Ets Procédé et dispositif de diffusion continue

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0804953A1 (de) * 1996-05-02 1997-11-05 Crown Iron Works Company Selbstreinigende Extraktionsvorrichtung
WO2016044237A1 (en) 2014-09-18 2016-03-24 Bridgestone Corporation Extractor and related methods
EP3194044A4 (de) * 2014-09-18 2018-06-13 Bridgestone Corporation Extraktor und zugehörige verfahren
US10245526B2 (en) 2014-09-18 2019-04-02 Bridgestone Corporation Extractor and related methods
US10843103B2 (en) 2014-09-18 2020-11-24 Bridgestone Corporation Extractor and related methods
US11458415B2 (en) 2014-09-18 2022-10-04 Bridgestone Corporation Extractor and related methods
EP3419733A4 (de) * 2016-02-26 2019-11-06 Crown Iron Works Company Schirm für entnahmesystem

Also Published As

Publication number Publication date
CA1253672A (en) 1989-05-09
EP0201311B1 (de) 1991-08-07
DE3680704D1 (de) 1991-09-12
EP0201311A3 (en) 1987-06-03
US4751060A (en) 1988-06-14

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