EP0086815A1 - Cup for thin layer chromatography - Google Patents
Cup for thin layer chromatographyInfo
- Publication number
- EP0086815A1 EP0086815A1 EP19820902641 EP82902641A EP0086815A1 EP 0086815 A1 EP0086815 A1 EP 0086815A1 EP 19820902641 EP19820902641 EP 19820902641 EP 82902641 A EP82902641 A EP 82902641A EP 0086815 A1 EP0086815 A1 EP 0086815A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- carrier
- layer chromatography
- thin layer
- glass
- cup
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/90—Plate chromatography, e.g. thin layer or paper chromatography
Definitions
- the present invention relates to a dip chamber for thin layer chromatography.
- Detection reagents are often used in thin-layer or paper chromatography. DTese react with the substances to be detected and form reaction products which can be detected with simpler means and / or with higher sensitivity than the starting substance.
- the detection reagents are often sprayed on as a liquid mist in order to avoid flow processes in the carrier which change the position and / or shape of the substance stains.
- Other ways of supplying the detection reagents are gassing with reagent vapors or immersion in a reagent solution. Only rarely can the reagent be added to the carrier or the substance before the substance to be detected is applied.
- Spraying the carrier with a reagent solution is difficult to do uniformly, since the individual droplets of the spray mist form only individual, irregularly distributed spots on the carrier if the density is too low, and if the density is too high, on the other hand, there is the risk of flow processes in or on the carrier Carrier exists.
- Elaborate devices for the controlled relative movement of the spray can and carrier with respect to one another were developed in order to achieve the uniformity of spraying necessary for quantitative evaluation of the reaction products.
- complex devices are required in order to safely exclude the health hazard to persons from the spray mist and / or gases or vapors emanating therefrom.
- a horizontal position of the carrier in the reagent is possible in flat dishes with little reagent requirement, but flow processes in or on the carrier cannot be avoided when immersed and removed.
- the aim of the present invention is a diving chamber for thin-layer chromatography, which does not have the disadvantages described above of the diving chambers made of metal or plastic.
- This object is achieved according to the invention by using a narrow, vertical chamber made of glass.
- Glass is used as a material according to the invention, since only glass is used against the commonly used organic ones
- Solvent, acid, bases and / or oxidizing reagents is resistant.
- the narrow glass chamber can also be used with very aggressive means, e.g. Chromium sulfuric acid, clean from reagent lakes.
- immersion chambers of this type have not yet been manufactured, a suitable manufacturing technique first had to be developed. It was found that the inventive modern immersion chambers can be produced particularly successfully from two flat glass plates which are fused together on three edges.
- the inside thickness of the chamber is typically 5-10 mm, while the inside width is chosen to be larger than the width of the carrier.
- the inside height of the chamber can be 10-20 mm smaller than the height of the carrier so that the carrier protrudes from the top of the chamber for easier handling. But it is also possible holder for the support, the narrow glass chamber is immersed with the aid of the carrier in full in ⁇ .
- FIG. 1 shows an exemplary embodiment of the invention: the immersion chamber consists of two glass plates 1 and 2 at a distance of approximately 5 mm, which are fused together on three edges.
Abstract
La cuvette destinée à recevoir les réactifs utilisés en chromatographie à couche mince ou en chromatographie sur papier est constituée, contrairement aux cuvettes conventionnelles, en verre. Elle est obtenue en soudant par fusion les trois côtés de deux plaques de verre.Unlike the conventional cuvettes, the cuvette intended to receive the reagents used in thin layer chromatography or on paper chromatography is made of glass. It is obtained by fusion welding the three sides of two glass plates.
Description
Claims
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE8125003 | 1981-08-27 | ||
DE8125003U | 1981-08-27 |
Publications (1)
Publication Number | Publication Date |
---|---|
EP0086815A1 true EP0086815A1 (en) | 1983-08-31 |
Family
ID=6730687
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP19820902641 Withdrawn EP0086815A1 (en) | 1981-08-27 | 1982-08-26 | Cup for thin layer chromatography |
Country Status (3)
Country | Link |
---|---|
EP (1) | EP0086815A1 (en) |
CH (1) | CH656467A5 (en) |
WO (1) | WO1983000741A1 (en) |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB929578A (en) * | 1960-07-05 | 1963-06-26 | Shandon Scient Company Ltd | Improvements in paper-chromatography apparatus |
FR1469350A (en) * | 1966-02-14 | 1967-02-10 | Euratom | Development facility for thin-layer chromatography plates |
FR1546678A (en) * | 1967-10-09 | 1968-11-22 | Kodak Pathe | New plastic apparatus for chromatographic separation |
NL6903174A (en) * | 1968-03-04 | 1969-09-08 | ||
US3600306A (en) * | 1969-09-05 | 1971-08-17 | Tlc Corp | Thin layer chromatography method and apparatus |
JPS521353Y2 (en) * | 1972-10-19 | 1977-01-13 | ||
US3864250A (en) * | 1973-03-16 | 1975-02-04 | Regis Chem Co | Liquid-solid adsorption chromatography |
ES8103379A1 (en) * | 1979-02-20 | 1981-02-16 | Hoechst Ag | Microchromatographic system for checking the intake of medicines via urine samples. |
-
1982
- 1982-08-26 EP EP19820902641 patent/EP0086815A1/en not_active Withdrawn
- 1982-08-26 WO PCT/EP1982/000181 patent/WO1983000741A1/en not_active Application Discontinuation
- 1982-08-26 CH CH507382A patent/CH656467A5/en not_active IP Right Cessation
Non-Patent Citations (1)
Title |
---|
See references of WO8300741A1 * |
Also Published As
Publication number | Publication date |
---|---|
CH656467A5 (en) | 1986-06-30 |
WO1983000741A1 (en) | 1983-03-03 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PUAI | Public reference made under article 153(3) epc to a published international application that has entered the european phase |
Free format text: ORIGINAL CODE: 0009012 |
|
AK | Designated contracting states |
Designated state(s): AT DE FR GB |
|
17P | Request for examination filed |
Effective date: 19830827 |
|
STAA | Information on the status of an ep patent application or granted ep patent |
Free format text: STATUS: THE APPLICATION IS DEEMED TO BE WITHDRAWN |
|
18D | Application deemed to be withdrawn |
Effective date: 19850724 |
|
RIN1 | Information on inventor provided before grant (corrected) |
Inventor name: RIEGE, GUENTER Inventor name: BERKHAN, ERNST Inventor name: DETEMPLE, MANFRED |