EA199900838A1 - Способ очистки серной кислоты - Google Patents
Способ очистки серной кислотыInfo
- Publication number
- EA199900838A1 EA199900838A1 EA199900838A EA199900838A EA199900838A1 EA 199900838 A1 EA199900838 A1 EA 199900838A1 EA 199900838 A EA199900838 A EA 199900838A EA 199900838 A EA199900838 A EA 199900838A EA 199900838 A1 EA199900838 A1 EA 199900838A1
- Authority
- EA
- Eurasian Patent Office
- Prior art keywords
- sulfuric acid
- acid fraction
- aqueous solution
- fraction
- cleaning sulfuric
- Prior art date
Links
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
- F28F19/00—Preventing the formation of deposits or corrosion, e.g. by using filters or scrapers
- F28F19/008—Preventing the formation of deposits or corrosion, e.g. by using filters or scrapers by using scrapers
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/69—Sulfur trioxide; Sulfuric acid
- C01B17/90—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/69—Sulfur trioxide; Sulfuric acid
- C01B17/90—Separation; Purification
- C01B17/92—Recovery from acid tar or the like, e.g. alkylation acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2/00—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
- C07C2/54—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by addition of unsaturated hydrocarbons to saturated hydrocarbons or to hydrocarbons containing a six-membered aromatic ring with no unsaturation outside the aromatic ring
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
- F28F27/00—Control arrangements or safety devices specially adapted for heat-exchange or heat-transfer apparatus
- F28F27/02—Control arrangements or safety devices specially adapted for heat-exchange or heat-transfer apparatus for controlling the distribution of heat-exchange media between different channels
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/141—Feedstock
- Y02P20/145—Feedstock the feedstock being materials of biological origin
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Treatment Of Sludge (AREA)
Abstract
Процесс очистки водного раствора серной кислоты, включающий охлаждение водного раствора серной кислоты до температуры замерзания или близкой к ней величины для образования суспензии из твердой фазы и жидкой фазы. Суспензия имеет фракцию с высоким содержанием кислоты и фракцию с низким содержанием кислоты. Фракция с высоким содержанием кислоты отделяется от фракции с низким содержанием кислоты.Отчет о международном поиске был опубликован 1999.04.15.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US83133797A | 1997-03-31 | 1997-03-31 | |
PCT/US1998/006400 WO1998043716A2 (en) | 1997-03-31 | 1998-03-31 | Sulfuric acid purification process |
Publications (1)
Publication Number | Publication Date |
---|---|
EA199900838A1 true EA199900838A1 (ru) | 2000-04-24 |
Family
ID=25258821
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EA199900838A EA199900838A1 (ru) | 1997-03-31 | 1998-03-31 | Способ очистки серной кислоты |
Country Status (6)
Country | Link |
---|---|
US (1) | US6159382A (ru) |
EP (1) | EP0970016A2 (ru) |
AU (1) | AU6945498A (ru) |
CA (1) | CA2285418A1 (ru) |
EA (1) | EA199900838A1 (ru) |
WO (1) | WO1998043716A2 (ru) |
Families Citing this family (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1094047A1 (en) * | 1999-10-22 | 2001-04-25 | Technische Universiteit Delft | Crystallisation of materials from aqueous solutions |
US20040222157A1 (en) * | 2003-02-18 | 2004-11-11 | Minhas Bhupender S. | Process for the recovery of sulfuric acid using polymeric membranes |
US7976710B2 (en) | 2003-02-18 | 2011-07-12 | Exxonmobil Research And Engineering Company | Membrane and process for the recovery of acid |
US7837880B2 (en) | 2004-02-06 | 2010-11-23 | Exxonmobil Research And Engineering Company | Acid tolerant polymeric membrane and process for the recovery of acid using polymeric membranes |
US7997426B2 (en) | 2004-02-06 | 2011-08-16 | Exxonmobil Research And Engineering Company | Acid tolerant polymeric membrane and process for the recovery of acid using polymeric membranes |
US20090136414A1 (en) * | 2004-08-26 | 2009-05-28 | Petrinec Bryan J | Method for downhole sulfur removal and recovery |
US20060129016A1 (en) * | 2004-12-10 | 2006-06-15 | Anderson Mark C | Methods for controlling water content of sulfuric acid in a sulfuric acid catalyzed process |
CN101746847B (zh) * | 2008-12-03 | 2011-12-07 | 上海轻工业研究所有限公司 | 自动化扩散渗析工业废酸或废碱回收设备 |
WO2010071616A1 (en) * | 2008-12-15 | 2010-06-24 | Crystatech, Inc. | Method for downhole sulfur removal and recovery |
EP2663529B1 (en) * | 2010-08-08 | 2020-03-18 | Norbert Nathan Buchsbaum | Process and apparatus for water purification |
US8491795B2 (en) * | 2011-09-01 | 2013-07-23 | Kenneth Yat-Yi Chen | Conversion of seawater to drinking water at room temperature |
DE102011116699A1 (de) * | 2011-10-24 | 2013-04-25 | Frederick Simon Oosthuizen | Verfahren und Vorrichtung zur Aufbereitung von anfallendem Abwasser einer Entsalzungsanlage |
US9150440B2 (en) | 2012-05-10 | 2015-10-06 | The National Titanium Dioxide Co. Ltd. (Cristal) | Method for purification of spent sulfuric acid from titanium dioxide rutile industry |
CN107754816B (zh) * | 2016-08-17 | 2020-02-14 | 中国科学院过程工程研究所 | 一种利用烷基化废酸制备炭基酸性材料的方法 |
CN108069405B (zh) * | 2016-11-10 | 2021-05-07 | 天津大学(青岛)海洋工程研究院有限公司 | 一种熔融结晶法浓缩稀硫酸的方法 |
CN108069406B (zh) * | 2016-11-15 | 2019-12-13 | 中国石油化工股份有限公司 | 一种烷基化废硫酸的再生方法 |
CN111072005B (zh) * | 2018-10-22 | 2021-11-16 | 天津工业大学 | 一种碳材料氧化物的制备方法 |
CN111773749B (zh) * | 2020-07-13 | 2022-02-01 | 青岛海湾精细化工有限公司 | 一种稀硫酸真空浓缩系统 |
CN114988433A (zh) * | 2022-05-07 | 2022-09-02 | 北京中矿博能节能科技有限公司 | 一种高盐水冷冻结晶真空洗脱水处理系统 |
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CH150902A (de) * | 1930-12-03 | 1931-11-30 | Sulzer Ag | Verfahren zur Gewinnung von Salz. |
US2287732A (en) * | 1939-09-02 | 1942-06-23 | Phillips Petroleum Co | Process for reclaiming sulphuric acid |
US2254788A (en) * | 1940-01-08 | 1941-09-02 | Shell Dev | Acid recovery process |
US2593128A (en) * | 1948-05-06 | 1952-04-15 | California Research Corp | Process for sulfuric acid recovery |
US2662812A (en) * | 1949-11-03 | 1953-12-15 | Koppers Co Inc | Regeneration of spent pickle liquor and recovery of ferrous sulfate monohydrate |
US2716592A (en) * | 1952-09-23 | 1955-08-30 | Kellogg M W Co | Method of purifying sulfuric acid |
US2816822A (en) * | 1954-08-31 | 1957-12-17 | Texas Co | High pressure crystallization apparatus containing a fluid pressure transfer device |
GB796343A (en) * | 1955-05-31 | 1958-06-11 | Kellogg M W Co | Improvements in or relating to method of purifying sulphuric acid by fractional crystallization |
US2862791A (en) * | 1955-07-08 | 1958-12-02 | Kellogg M W Co | Sulfuric acid purification |
US2857247A (en) * | 1955-10-06 | 1958-10-21 | Stratford Eng Corp | Method for recovering spent alkylation acid |
US3049889A (en) * | 1958-01-02 | 1962-08-21 | Carrier Corp | Method and apparatus for rendering brine solution potable |
US3158004A (en) * | 1961-11-02 | 1964-11-24 | Klencke Siegfried | Apparatus for freeze concentration |
US3248890A (en) * | 1963-03-06 | 1966-05-03 | Oman Erik | Process to concentrate sulphite-lye or other liquors by freezing |
US3344616A (en) * | 1963-08-23 | 1967-10-03 | Owen Margaret Louise | Desalinization |
US3277667A (en) * | 1964-06-03 | 1966-10-11 | Struthers Scientific Int Corp | Freezing |
US3410335A (en) * | 1965-02-13 | 1968-11-12 | Svenska Carbon Black Aktiebola | Coolers for mixtures of gases and solid particles |
US3400548A (en) * | 1965-06-25 | 1968-09-10 | Marathon Oil Co | Crystal separation of dimethylnaphthalene |
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US3616268A (en) * | 1969-02-24 | 1971-10-26 | Lummus Co | Acetic acid recovery from aqueous solution by distillation and crystallization |
US3607035A (en) * | 1969-02-24 | 1971-09-21 | Universal Oil Prod Co | Process for treating a sulfuric acid-olefinic hydrocarbon mixture |
US3565168A (en) * | 1969-04-01 | 1971-02-23 | Pennwalt Corp | Cone dryer |
US3689217A (en) * | 1970-06-15 | 1972-09-05 | Inventa Ag | Process for freeing 55-85% sulphuric acid from its impurities due to metals and/or semi-metals |
US3885399A (en) * | 1973-03-27 | 1975-05-27 | Robert J Campbell | Means for and method of purifying contaminated water |
US3890097A (en) * | 1974-05-06 | 1975-06-17 | Agrico Chem Co | Method of purifying wet process phosphoric acid |
JPS52140497A (en) * | 1976-05-20 | 1977-11-24 | Nippon Mining Co Ltd | Recovery of arsenic from arsenic-contg. solution of sulfuric acid |
DE2630196A1 (de) * | 1976-07-05 | 1978-01-19 | Bayer Ag | Verfahren zur herstellung von schwefelsaeure aus abfallsaeure und eisensulfat |
US4091635A (en) * | 1976-08-18 | 1978-05-30 | Avco Corporation | Apparatus for concentrating a feed stream |
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IT1086097B (it) * | 1977-09-21 | 1985-05-28 | Montedison Spa | Procedimento per preparare soluzioni acquose limpide di acido solforico |
CH637351A5 (de) * | 1977-11-16 | 1983-07-29 | Sandoz Ag | Verfahren zum aufarbeiten von borsaeurehaltiger schwefelsaeure. |
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US4314455A (en) * | 1980-06-16 | 1982-02-09 | Chicago Bridge & Iron Company | Freeze concentration apparatus and process |
US4328677A (en) * | 1980-09-23 | 1982-05-11 | Milton Meckler | Peltier freeze concentration process |
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US4740281A (en) * | 1986-10-14 | 1988-04-26 | Allied Corporation | Recovery of acids from materials comprising acid and salt |
FR2634751B1 (ru) * | 1988-07-29 | 1991-02-08 | Metaleurop Sa | |
FI81501C (fi) * | 1988-09-28 | 1990-11-12 | Inventio Oy | FOERFARANDE FOER ISNING. SIIRRETTY PAEIVAEMAEAERAE-FOERSKJUTET DATUM PL 14 ç 21.10.1988 |
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US4894170A (en) * | 1989-02-27 | 1990-01-16 | Billmyre Richard D | Liquid recovery system and method |
US4936114A (en) * | 1989-06-23 | 1990-06-26 | Chicago Bridge & Iron Technical Services Company | Apparatus and method of freeze concentrating aqueous waste and process streams to separate water from precipitable salts |
US5059228A (en) * | 1990-04-30 | 1991-10-22 | Cheng Chen Yen | Cool thermal storage and/or water purification by direct contact in-situ crystal formation and crystal melting operations |
DE4029737C1 (ru) * | 1990-09-20 | 1991-12-05 | Metallgesellschaft Ag, 6000 Frankfurt, De | |
US5220802A (en) * | 1991-11-07 | 1993-06-22 | Air Products And Chemicals, Inc. | Method and apparatus for individually quick freezing small surface moist articles |
US5275701A (en) * | 1993-03-15 | 1994-01-04 | Air Products And Chemicals, Inc. | Process for purification and concentration of sulfuric acid |
US5394706A (en) * | 1993-05-20 | 1995-03-07 | Waterworks International, Inc. | Freeze crystallization for the removal of water from a solution of dissolved solids |
-
1998
- 1998-03-31 EA EA199900838A patent/EA199900838A1/ru unknown
- 1998-03-31 WO PCT/US1998/006400 patent/WO1998043716A2/en not_active Application Discontinuation
- 1998-03-31 AU AU69454/98A patent/AU6945498A/en not_active Abandoned
- 1998-03-31 EP EP98915212A patent/EP0970016A2/en not_active Withdrawn
- 1998-03-31 CA CA002285418A patent/CA2285418A1/en not_active Abandoned
- 1998-10-07 US US09/167,563 patent/US6159382A/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
US6159382A (en) | 2000-12-12 |
CA2285418A1 (en) | 1998-10-08 |
WO1998043716A3 (en) | 1999-04-15 |
WO1998043716A2 (en) | 1998-10-08 |
AU6945498A (en) | 1998-10-22 |
EP0970016A2 (en) | 2000-01-12 |
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