DK3194065T3 - Fremgangsmåde til phosgenering af forbindelser indeholdende hydroxyl-, thiol-, amino- og/eller formamidgrupper - Google Patents

Fremgangsmåde til phosgenering af forbindelser indeholdende hydroxyl-, thiol-, amino- og/eller formamidgrupper Download PDF

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Publication number
DK3194065T3
DK3194065T3 DK15760100.6T DK15760100T DK3194065T3 DK 3194065 T3 DK3194065 T3 DK 3194065T3 DK 15760100 T DK15760100 T DK 15760100T DK 3194065 T3 DK3194065 T3 DK 3194065T3
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Denmark
Prior art keywords
phos
thiol
amino
procedure
generation
Prior art date
Application number
DK15760100.6T
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English (en)
Inventor
Jens Stefan Roggan
Leslaw Mleczko
Konstantinos Metaxas
Ilja Peckermann
Stephan Schubert
Ekkehard Barth
Michael Gottfried
Original Assignee
Bayer Ag
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Publication of DK3194065T3 publication Critical patent/DK3194065T3/da

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/065—Feeding reactive fluids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C68/00—Preparation of esters of carbonic or haloformic acids
    • C07C68/02—Preparation of esters of carbonic or haloformic acids from phosgene or haloformates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/18—Carbon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/615—100-500 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0278—Feeding reactive fluids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067—Heating or cooling the reactor
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/80—Phosgene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/96—Esters of carbonic or haloformic acids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00309—Controlling the temperature by indirect heat exchange with two or more reactions in heat exchange with each other, such as an endothermic reaction in heat exchange with an exothermic reaction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/0004—Processes in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00054—Controlling or regulating the heat exchange system
    • B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058—Temperature measurement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00085—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02—Apparatus characterised by their chemically-resistant properties
    • B01J2219/0204—Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
    • B01J2219/0236—Metal based

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
DK15760100.6T 2014-08-20 2015-08-18 Fremgangsmåde til phosgenering af forbindelser indeholdende hydroxyl-, thiol-, amino- og/eller formamidgrupper DK3194065T3 (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102014111903 2014-08-20
PCT/EP2015/068883 WO2016026826A1 (de) 2014-08-20 2015-08-18 Verfahren zur phosgenierung von hydroxyl-, thiol-, amino- und/oder formamidgruppen enthaltenden verbindungen

Publications (1)

Publication Number Publication Date
DK3194065T3 true DK3194065T3 (da) 2020-03-16

Family

ID=54065320

Family Applications (1)

Application Number Title Priority Date Filing Date
DK15760100.6T DK3194065T3 (da) 2014-08-20 2015-08-18 Fremgangsmåde til phosgenering af forbindelser indeholdende hydroxyl-, thiol-, amino- og/eller formamidgrupper

Country Status (9)

Country Link
US (1) US10118145B2 (da)
EP (1) EP3194065B1 (da)
JP (1) JP6567653B2 (da)
KR (1) KR101842501B1 (da)
CN (1) CN107001233B (da)
DK (1) DK3194065T3 (da)
ES (1) ES2774898T3 (da)
PL (1) PL3194065T3 (da)
WO (1) WO2016026826A1 (da)

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3327274A1 (de) * 1983-07-28 1985-02-07 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von phosgen unter gleichzeitiger erzeugung von dampf
US5380909A (en) * 1991-06-24 1995-01-10 The Dow Chemical Company Captive carbonyl halide process for production of diaryl carbonates
DE19848668A1 (de) * 1998-10-22 2000-04-27 Bayer Ag Tetrachlorkohlenstoffarmes Phosgen
JP4290793B2 (ja) * 1999-01-22 2009-07-08 帝人化成株式会社 ホスゲンの製造方法
DE60042195D1 (de) 1999-12-28 2009-06-25 Mitsubishi Chem Corp Verfahren zum Herstellen von Diarylcarbonat
BR0307973A (pt) 2002-02-27 2004-12-21 Basf Ag Reator, dispositivo e processo para preparar fosgênio por meio de reação em fase gasosa de monóxido de carbono e cloro na presença de um catalisador de leito fixo
DE102004041777A1 (de) * 2004-08-28 2006-03-02 Bayer Materialscience Ag Verfahren und Vorrichtung zur Herstellung von Phosgen
JP4750448B2 (ja) * 2005-04-04 2011-08-17 三井化学株式会社 化学処理装置における固体触媒の寿命の判断方法
KR20080082958A (ko) * 2006-01-17 2008-09-12 테이진 카세이 가부시키가이샤 폴리카보네이트 올리고머의 연속 제조 방법
PT2379216T (pt) * 2008-12-16 2018-01-10 Basf Se Reator e processo para a produção de fosgénio
FR2965490B1 (fr) 2010-09-30 2013-01-11 Aet Group Dispositif et procede pour la phosgenation en continu
JP5775347B2 (ja) * 2011-03-31 2015-09-09 出光興産株式会社 ポリカーボネートオリゴマー連続製造の制御方法
US8545775B2 (en) * 2011-10-20 2013-10-01 Kellogg Brown & Root Llc Reforming exchanger system with intermediate shift conversion
JP6258313B2 (ja) * 2012-07-11 2018-01-10 コベストロ、ドイチュラント、アクチエンゲゼルシャフトＣｏｖｅｓｔｒｏ Ｄｅｕｔｓｃｈｌａｎｄ Ａｇ ホスゲンを製造する装置および方法

Also Published As

Publication number Publication date
KR20170046700A (ko) 2017-05-02
ES2774898T3 (es) 2020-07-23
CN107001233B (zh) 2019-02-26
PL3194065T3 (pl) 2020-06-29
EP3194065A1 (de) 2017-07-26
EP3194065B1 (de) 2019-12-25
US20170274341A1 (en) 2017-09-28
US10118145B2 (en) 2018-11-06
WO2016026826A1 (de) 2016-02-25
JP6567653B2 (ja) 2019-08-28
KR101842501B1 (ko) 2018-03-27
JP2017533076A (ja) 2017-11-09
CN107001233A (zh) 2017-08-01

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