DK2910610T3 - Fremgangsmåde til fremstilling af et calciumcarbonatfyldstofprodukt - Google Patents
Fremgangsmåde til fremstilling af et calciumcarbonatfyldstofprodukt Download PDFInfo
- Publication number
- DK2910610T3 DK2910610T3 DK14156165.4T DK14156165T DK2910610T3 DK 2910610 T3 DK2910610 T3 DK 2910610T3 DK 14156165 T DK14156165 T DK 14156165T DK 2910610 T3 DK2910610 T3 DK 2910610T3
- Authority
- DK
- Denmark
- Prior art keywords
- maleic anhydride
- mineral filler
- styrene
- grinding
- calcium carbonate
- Prior art date
Links
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 title claims description 171
- 229910000019 calcium carbonate Inorganic materials 0.000 title claims description 78
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- 239000000945 filler Substances 0.000 title description 14
- 238000000227 grinding Methods 0.000 claims description 156
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical group O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 claims description 146
- 239000012764 mineral filler Substances 0.000 claims description 132
- 239000003795 chemical substances by application Substances 0.000 claims description 121
- 239000000203 mixture Substances 0.000 claims description 117
- 239000000463 material Substances 0.000 claims description 114
- 238000000034 method Methods 0.000 claims description 98
- 229920000147 Styrene maleic anhydride Polymers 0.000 claims description 84
- 239000000047 product Substances 0.000 claims description 66
- 229920001577 copolymer Polymers 0.000 claims description 65
- PYSRRFNXTXNWCD-UHFFFAOYSA-N 3-(2-phenylethenyl)furan-2,5-dione Chemical compound O=C1OC(=O)C(C=CC=2C=CC=CC=2)=C1 PYSRRFNXTXNWCD-UHFFFAOYSA-N 0.000 claims description 63
- 230000008569 process Effects 0.000 claims description 63
- 229920000642 polymer Polymers 0.000 claims description 44
- 238000009837 dry grinding Methods 0.000 claims description 37
- 239000000178 monomer Substances 0.000 claims description 32
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 30
- 239000002245 particle Substances 0.000 claims description 30
- 125000003011 styrenyl group Chemical group [H]\C(*)=C(/[H])C1=C([H])C([H])=C([H])C([H])=C1[H] 0.000 claims description 28
- 238000001035 drying Methods 0.000 claims description 25
- -1 chalk Substances 0.000 claims description 19
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 17
- 239000011575 calcium Substances 0.000 claims description 17
- 229910052791 calcium Inorganic materials 0.000 claims description 17
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 16
- 229910052708 sodium Inorganic materials 0.000 claims description 16
- 239000011734 sodium Substances 0.000 claims description 16
- 150000001768 cations Chemical class 0.000 claims description 15
- 229910052757 nitrogen Inorganic materials 0.000 claims description 15
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims description 14
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 14
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 14
- 229910052744 lithium Inorganic materials 0.000 claims description 14
- 239000011777 magnesium Substances 0.000 claims description 14
- 229910052749 magnesium Inorganic materials 0.000 claims description 14
- 229910052700 potassium Inorganic materials 0.000 claims description 14
- 239000011591 potassium Substances 0.000 claims description 14
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 13
- 239000003973 paint Substances 0.000 claims description 9
- 239000004579 marble Substances 0.000 claims description 8
- 238000000576 coating method Methods 0.000 claims description 7
- 239000002952 polymeric resin Substances 0.000 claims description 7
- 229920003002 synthetic resin Polymers 0.000 claims description 7
- 235000019738 Limestone Nutrition 0.000 claims description 6
- 239000006028 limestone Substances 0.000 claims description 6
- 239000000853 adhesive Substances 0.000 claims description 5
- 230000001070 adhesive effect Effects 0.000 claims description 5
- 239000010459 dolomite Substances 0.000 claims description 5
- 229910000514 dolomite Inorganic materials 0.000 claims description 5
- 239000002537 cosmetic Substances 0.000 claims description 4
- 239000000565 sealant Substances 0.000 claims description 4
- 239000011247 coating layer Substances 0.000 claims 1
- 238000012986 modification Methods 0.000 description 21
- 230000004048 modification Effects 0.000 description 21
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 17
- 239000007795 chemical reaction product Substances 0.000 description 17
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 15
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical class N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 14
- 238000006243 chemical reaction Methods 0.000 description 13
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- 229910052500 inorganic mineral Inorganic materials 0.000 description 11
- 235000010755 mineral Nutrition 0.000 description 11
- 239000011707 mineral Substances 0.000 description 11
- 238000002360 preparation method Methods 0.000 description 11
- 239000007864 aqueous solution Substances 0.000 description 10
- 229940088417 precipitated calcium carbonate Drugs 0.000 description 8
- 150000001412 amines Chemical class 0.000 description 7
- 229910021529 ammonia Inorganic materials 0.000 description 7
- 239000002270 dispersing agent Substances 0.000 description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 6
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 6
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 6
- 239000004793 Polystyrene Substances 0.000 description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 6
- 239000012298 atmosphere Substances 0.000 description 6
- 150000001735 carboxylic acids Chemical class 0.000 description 6
- 229920002223 polystyrene Polymers 0.000 description 6
- 239000002253 acid Substances 0.000 description 5
- 150000001298 alcohols Chemical class 0.000 description 5
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 description 5
- 235000014113 dietary fatty acids Nutrition 0.000 description 5
- 238000009826 distribution Methods 0.000 description 5
- 239000000194 fatty acid Substances 0.000 description 5
- 229930195729 fatty acid Natural products 0.000 description 5
- 150000004665 fatty acids Chemical class 0.000 description 5
- 229910000000 metal hydroxide Inorganic materials 0.000 description 5
- 150000004692 metal hydroxides Chemical class 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 239000003039 volatile agent Substances 0.000 description 5
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 4
- 239000004594 Masterbatch (MB) Substances 0.000 description 4
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 4
- 229920001515 polyalkylene glycol Polymers 0.000 description 4
- 229920000098 polyolefin Polymers 0.000 description 4
- 239000004800 polyvinyl chloride Substances 0.000 description 4
- 229920000915 polyvinyl chloride Polymers 0.000 description 4
- 150000003141 primary amines Chemical class 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 239000002002 slurry Substances 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 239000004743 Polypropylene Substances 0.000 description 3
- 150000007513 acids Chemical class 0.000 description 3
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 3
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 125000004432 carbon atom Chemical group C* 0.000 description 3
- 238000010276 construction Methods 0.000 description 3
- 150000003949 imides Chemical class 0.000 description 3
- 150000002466 imines Chemical class 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 238000010534 nucleophilic substitution reaction Methods 0.000 description 3
- 229920001155 polypropylene Polymers 0.000 description 3
- 239000011343 solid material Substances 0.000 description 3
- ULQISTXYYBZJSJ-UHFFFAOYSA-N 12-hydroxyoctadecanoic acid Chemical compound CCCCCCC(O)CCCCCCCCCCC(O)=O ULQISTXYYBZJSJ-UHFFFAOYSA-N 0.000 description 2
- XDOFQFKRPWOURC-UHFFFAOYSA-N 16-methylheptadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCCCC(O)=O XDOFQFKRPWOURC-UHFFFAOYSA-N 0.000 description 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 238000004438 BET method Methods 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- PXIPVTKHYLBLMZ-UHFFFAOYSA-N Sodium azide Chemical compound [Na+].[N-]=[N+]=[N-] PXIPVTKHYLBLMZ-UHFFFAOYSA-N 0.000 description 2
- 235000021355 Stearic acid Nutrition 0.000 description 2
- 150000007933 aliphatic carboxylic acids Chemical class 0.000 description 2
- 125000001931 aliphatic group Chemical group 0.000 description 2
- 150000001408 amides Chemical class 0.000 description 2
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 2
- 239000000920 calcium hydroxide Substances 0.000 description 2
- 235000011116 calcium hydroxide Nutrition 0.000 description 2
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 2
- GHVNFZFCNZKVNT-UHFFFAOYSA-N decanoic acid Chemical compound CCCCCCCCCC(O)=O GHVNFZFCNZKVNT-UHFFFAOYSA-N 0.000 description 2
- 239000004205 dimethyl polysiloxane Substances 0.000 description 2
- IUNMPGNGSSIWFP-UHFFFAOYSA-N dimethylaminopropylamine Chemical compound CN(C)CCCN IUNMPGNGSSIWFP-UHFFFAOYSA-N 0.000 description 2
- UKMSUNONTOPOIO-UHFFFAOYSA-N docosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCCC(O)=O UKMSUNONTOPOIO-UHFFFAOYSA-N 0.000 description 2
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 2
- 238000001125 extrusion Methods 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
- 229920001477 hydrophilic polymer Polymers 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- UTOPWMOLSKOLTQ-UHFFFAOYSA-N octacosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCCC(O)=O UTOPWMOLSKOLTQ-UHFFFAOYSA-N 0.000 description 2
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 2
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 2
- 125000001190 organyl group Chemical group 0.000 description 2
- 239000011236 particulate material Substances 0.000 description 2
- 229920000233 poly(alkylene oxides) Polymers 0.000 description 2
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 2
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 description 2
- 229920000058 polyacrylate Polymers 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 238000007873 sieving Methods 0.000 description 2
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical class [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 description 2
- 238000001694 spray drying Methods 0.000 description 2
- 239000008117 stearic acid Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 238000001757 thermogravimetry curve Methods 0.000 description 2
- 238000001238 wet grinding Methods 0.000 description 2
- 229940114072 12-hydroxystearic acid Drugs 0.000 description 1
- 235000021357 Behenic acid Nutrition 0.000 description 1
- FGUUSXIOTUKUDN-IBGZPJMESA-N C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 Chemical compound C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 FGUUSXIOTUKUDN-IBGZPJMESA-N 0.000 description 1
- 229910021532 Calcite Inorganic materials 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 239000005632 Capric acid (CAS 334-48-5) Substances 0.000 description 1
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 1
- 239000005639 Lauric acid Substances 0.000 description 1
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 235000021314 Palmitic acid Nutrition 0.000 description 1
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical class OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 description 1
- 229920002845 Poly(methacrylic acid) Polymers 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 229920002873 Polyethylenimine Polymers 0.000 description 1
- 229920002125 Sokalan® Polymers 0.000 description 1
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 229940116226 behenic acid Drugs 0.000 description 1
- 229920001400 block copolymer Polymers 0.000 description 1
- 238000000071 blow moulding Methods 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 238000011088 calibration curve Methods 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 150000005323 carbonate salts Chemical class 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 150000007942 carboxylates Chemical group 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- HNEGQIOMVPPMNR-IHWYPQMZSA-N citraconic acid Chemical class OC(=O)C(/C)=C\C(O)=O HNEGQIOMVPPMNR-IHWYPQMZSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000000748 compression moulding Methods 0.000 description 1
- 238000012937 correction Methods 0.000 description 1
- 238000005443 coulometric titration Methods 0.000 description 1
- 238000003869 coulometry Methods 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 150000005690 diesters Chemical group 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 239000000806 elastomer Substances 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 125000004185 ester group Chemical group 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 125000000816 ethylene group Chemical group [H]C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 150000004673 fluoride salts Chemical class 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 239000011888 foil Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- WOLATMHLPFJRGC-UHFFFAOYSA-N furan-2,5-dione;styrene Chemical compound O=C1OC(=O)C=C1.C=CC1=CC=CC=C1 WOLATMHLPFJRGC-UHFFFAOYSA-N 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000001746 injection moulding Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 239000003879 lubricant additive Substances 0.000 description 1
- 239000003550 marker Substances 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 1
- 239000005445 natural material Substances 0.000 description 1
- 229920005615 natural polymer Polymers 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 150000003891 oxalate salts Chemical class 0.000 description 1
- JTJMJGYZQZDUJJ-UHFFFAOYSA-N phencyclidine Chemical class C1CCCCN1C1(C=2C=CC=CC=2)CCCCC1 JTJMJGYZQZDUJJ-UHFFFAOYSA-N 0.000 description 1
- 235000021317 phosphate Nutrition 0.000 description 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920000223 polyglycerol Polymers 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 229920005604 random copolymer Polymers 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000000518 rheometry Methods 0.000 description 1
- 238000001175 rotational moulding Methods 0.000 description 1
- 238000007665 sagging Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 150000003335 secondary amines Chemical class 0.000 description 1
- 150000004756 silanes Chemical class 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Inorganic materials [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 229910052712 strontium Inorganic materials 0.000 description 1
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 150000003890 succinate salts Chemical class 0.000 description 1
- 229940014800 succinic anhydride Drugs 0.000 description 1
- 150000003460 sulfonic acids Chemical class 0.000 description 1
- 239000012756 surface treatment agent Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 229920001059 synthetic polymer Polymers 0.000 description 1
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical class CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
- 238000003856 thermoforming Methods 0.000 description 1
- 238000002411 thermogravimetry Methods 0.000 description 1
- 229920001169 thermoplastic Polymers 0.000 description 1
- 229920005992 thermoplastic resin Polymers 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/02—Compounds of alkaline earth metals or magnesium
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/02—Compounds of alkaline earth metals or magnesium
- C09C1/021—Calcium carbonates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C19/00—Other disintegrating devices or methods
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F11/00—Compounds of calcium, strontium, or barium
- C01F11/18—Carbonates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
- C09C3/10—Treatment with macromolecular organic compounds
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
- C01P2002/88—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by thermal analysis data, e.g. TGA, DTA, DSC
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
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- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
- C01P2006/82—Compositional purity water content
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
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- Polymers & Plastics (AREA)
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- Food Science & Technology (AREA)
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Claims (15)
1. Fremgangsmåde til fremstilling af et mineralfyldstofprodukt, hvilken fremgangsmåde omfatter trinnene: a) at tilvejebringe et calciumcarbonat-holdigt materiale; b) at tilvejebringe mindst et formalingsmiddel; c) at tørformale det calciumcarbonat-holdige materiale i en blanding opnået ved at bringe i kontakt: i) det calciumcarbonat-holdige materiale tilvejebragt i trin a), med ii) det mindst ene formalingsmiddel tilvejebragt i trin b) i mindst en formalingsenhed til at opnå et tørformalet mineralfyldstof; d) at klassificere det tørformalede mineralfyldstof fra trin c) til at opnå en grov fraktion og en fin fraktion, hvor den grove fraktion fjernes eller underkastes et tørformalingstrin c) og den fine fraktion udgør et fint mineralfyldstof; og e) eventuelt at tørre det fine mineralfyldstof fra trin d) til at opnå et tørret mineralfyldstof med en samlet fugtindhold på mindre end 1,0 vægtprocent, baseret på den samlede vægt af det tørrede mineralfyldstof; hvor det samlede fugtindhold i blandingen fra trin c) er mindre end eller lig med 10.0 vægtprocent, baseret på blandingens samlede vægt; mængden af det mindst ene formalingsmiddel tilvejebragt i trin b) er i området fra 0,05 til 150 mg/m2, baseret på det specifikke overfladeareal af det calciumcarbonat-holdige materiale som målt med BET-nitrogenmetoden; temperaturen i trin c) er i området fra 55 °C til 200 °C; og det mindst ene formalingsmiddel er valgt fra gruppen bestående af styren- maleinsyreanhydrid-copolymerer og derivativer af styrenmaleinsyreanhydrid- copolymerer, og har et monomerenhedsforhold (styrenenheder : maleinsyreanhydrid-enheder, S:MA) på fra 1:2 til 15:1 og en molekylevægt Mw på fra 500 til 40Ό00 g/mol.
2. Fremgangsmåde ifølge krav 1, hvor det calciumcarbonat-holdige materiale tilvejebragt i trin a) er valgt fra naturlige calciumcarbonatkilder og er fortrinsvis valgt fra gruppen bestående af marmor, kalksten, kridt, dolomit og blandinger deraf.
3. Fremgangsmåde ifølge et hvilket som helst af kravene 1 eller 2, hvor mængden af det mindst ene formalingsmiddel tilvejebragt i trin b) er i området fra 0,1 til 100,0 mg/m2, fortrinsvis fra 0,2 til 75,0 mg/m2, og mere fortrinsvis 0,2 til 50,0 mg/m2 fra baseret på det specifikke overfladeareal af det calciumcarbonat-holdige materiale som målt med BET-nitrogenmetoden.
4. Fremgangsmåde ifølge et hvilket som helst af kravene 1 til 3, hvor det mindst ene formalingsmiddel tilvejebragt i trin b) har et monomerenhedsforhold (S:MA) på fra 1:1 til 5:1, fortrinsvis fra 1:1 til 4:1, og mere fortrinsvis fra 1:1 til 3:1.
5. Fremgangsmåde ifølge et hvilket som helst af kravene 1 til 4, hvor det mindst ene formalingsmiddel tilvejebragt i trin b) har en molekylevægt Mw på fra 2Ό00 til 30Ό00 g/mol og fortrinsvis fra 3Ό00 til 25Ό00 g/mol.
6. Fremgangsmåde ifølge et hvilket som helst af kravene 1 til 5, hvor det mindst ene formalingsmiddel tilvejebragt i trin b) er delvist eller helt neutraliseret med kationer valgt fra lithium, natrium, kalium, calcium, magnesium, ammonium, iminium og blandinger deraf.
7. Fremgangsmåde ifølge et hvilket som helst af kravene 1 til 6, hvor det samlede fugtindhold i blandingen fra trin c) er mindre end eller lig med 5,0 vægtprocent, fortrinsvis mindre end eller lig med 2,0 vægtprocent, og mere fortrinsvis mindre end eller lig med 1,0 vægtprocent, baseret på blandingens samlede vægt.
8. Fremgangsmåde ifølge et hvilket som helst af kravene 1 til 7, hvor temperaturen in trin c) er i området fra 70 °C til 180 °C, fortrinsvis fra 75 °C til 160 °C, og mere fortrinsvis fra 80 °C til 150 °C.
9. Fremgangsmåde ifølge et hvilket som helst af kravene 1 til 8, hvor det fine mineralfyldstof fra trin d) haren vægtgennemsnitlig partikelstørrelse dso i området fra 0,4 til 40,0 pm, fortrinsvis fra 0,6 til 20,0 pm, og mere fortrinsvis fra 0,7 til 10,0 pm.
10. Fremgangsmåde ifølge et hvilket som helst af kravene 1 til 9, hvor fremgangsmåden omfatter et yderligere trin til behandling af det fine mineralfyldstof fra trin d) og/eller det tørrede mineralfyldstof fra trin e) med et hydrofobiseringsmiddel til at opnå et overfladebehandlet produkt med et behandlingslag på mindst en del af produktets overflade.
11. Mineralfyldstofprodukt opnået med en fremgangsmåde ifølge et hvilket som helst af kravene 1 til 10, hvor produktet har en flygtig starttemperatur på mindst eller lig med 200 °C.
12. Mineralfyldstofprodukt opnået med fremgangsmåden ifølge krav 10, hvor produktet har en fugtopsamlingssusceptibilitet på mindre end eller lig med 0,9 mg/g, fortrinsvis mindre end eller lig med 0,8 mg/g, mere fortrinsvis mindre end eller lig med 0,7 mg/g, og mest fortrinsvis fra 0,2 til 0,6 mg/g.
13. Mineralfyldstofprodukt ifølge et hvilket som helst af kravene 11 eller 12, hvor produktet har en flygtig starttemperatur på mindst eller lig med 230 °C, fortrinsvis mindst eller lig med 250 °C.
14. Anvendelse af et mineralfyldstofproduct ifølge et hvilket som helst af kravene 11 til 13 i en polymersammensætning, til papirfremstilling, papircoatings, landbrugsmæssige produkter, maling, klæbemidler, tætningsmidler, bygningsprodukter, og/eller kosmetikprodukter, fortrinsvis anvendes mineralfyldstofproduktet i en polymersammensætning.
15. Anvendelse ifølge krav 14, hvor polymersammensætningen omfatter: a) mindst en polymerresin; og b) fra 0,1 til 90,0 vægtprocent, fortrinsvis fra 1,0 til 85,0 vægtprocent, og mere fortrinsvis fra 2,0 til 45,0 vægtprocent, baseret den samlede vægt af polymersammensætningen, af mineralfyldstofproduktet ifølge krav 11 til 13.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP14156165.4A EP2910610B1 (en) | 2014-02-21 | 2014-02-21 | Process for the preparation of a calcium carbonate filler product |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DK2910610T3 true DK2910610T3 (da) | 2017-09-25 |
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|---|---|---|---|
| DK14156165.4T DK2910610T3 (da) | 2014-02-21 | 2014-02-21 | Fremgangsmåde til fremstilling af et calciumcarbonatfyldstofprodukt |
Country Status (19)
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|---|---|
| US (2) | US10316193B2 (da) |
| EP (2) | EP2910610B1 (da) |
| JP (1) | JP6310089B2 (da) |
| KR (1) | KR20160124202A (da) |
| CN (1) | CN106029792B (da) |
| AU (1) | AU2015220955B2 (da) |
| CA (1) | CA2939144A1 (da) |
| CL (1) | CL2016002095A1 (da) |
| DK (1) | DK2910610T3 (da) |
| ES (1) | ES2640099T3 (da) |
| HR (1) | HRP20171368T1 (da) |
| HU (1) | HUE034671T2 (da) |
| MX (1) | MX2016010842A (da) |
| PL (1) | PL2910610T3 (da) |
| PT (1) | PT2910610T (da) |
| RU (1) | RU2647026C1 (da) |
| SI (1) | SI2910610T1 (da) |
| TW (1) | TWI530536B (da) |
| WO (1) | WO2015124494A1 (da) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3017872B1 (fr) * | 2014-02-21 | 2016-05-20 | Coatex Sas | Utilisation de copolymeres de styrene et d'anhydride maleique pour preparer des particules de matiere minerale |
| EP3133127B1 (en) | 2015-08-21 | 2018-08-08 | Omya International AG | Process for the preparation of a mineral filler product |
| EP3156369B1 (en) * | 2015-10-16 | 2018-07-11 | Omya International AG | High solids pcc with copolymeric additive |
| EP3192838A1 (en) * | 2016-01-14 | 2017-07-19 | Omya International AG | Treatment of surface-reacted calcium carbonate |
| ES2702459T3 (es) | 2016-01-14 | 2019-03-01 | Omya Int Ag | Uso de un carbonato de calcio tratado en superficie como secuestrante de oxígeno |
| EP3467050A1 (en) * | 2017-10-04 | 2019-04-10 | Omya International AG | Coating compositions comprising ground natural calcium carbonate (gcc) |
| EP3537428A1 (en) * | 2018-03-05 | 2019-09-11 | Omya International AG | Noise and/or sound reducing multilayer unit |
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| US4136830A (en) * | 1976-05-19 | 1979-01-30 | The Dow Chemical Company | Ore grinding process containing copolymer grinding aids |
| JPS532557A (en) * | 1976-06-28 | 1978-01-11 | Shiraishi Chuo Kenkiyuushiyo K | Calcium carbonateewater dispersion substance |
| JPS5389839A (en) * | 1977-01-18 | 1978-08-08 | Kyodo Yushi | Component of protective agent of metal pipe |
| SU854940A1 (ru) * | 1978-11-20 | 1981-08-15 | Ордена Трудового Красного Знамени Институт Физической Химии Ан Ссср | Способ получени привитых сополимеров |
| JPS56120742A (en) | 1980-02-29 | 1981-09-22 | Idemitsu Petrochem Co Ltd | Polypropylene composition |
| JPS6272762A (ja) * | 1985-09-26 | 1987-04-03 | Idemitsu Petrochem Co Ltd | 無機顔料スラリ−用添加剤 |
| JPS62132730A (ja) * | 1985-12-02 | 1987-06-16 | Kuraray Co Ltd | 炭酸カルシウム用分散剤 |
| DE3801649C2 (de) | 1988-01-21 | 1996-09-19 | Solvay Werke Gmbh | Unterbodenschutzmasse, Verfahren zu deren Herstellung sowie Verwendung eines gegebenenfalls synthetischen Calciumcarbonats zur Rheologiesteuerung von Unterbodenschutzmassen |
| JPH02150462A (ja) | 1988-12-02 | 1990-06-08 | Nippon Soda Co Ltd | 表面処理剤 |
| JP3177616B2 (ja) * | 1991-05-09 | 2001-06-18 | 東ソー株式会社 | 炭酸カルシウム用分散剤 |
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| GB9602084D0 (en) * | 1996-02-02 | 1996-04-03 | Sandoz Ltd | Improvements in or relating to organic compounds |
| CA2303812A1 (en) | 1998-05-22 | 1999-12-02 | Dickey S. Shurling | Particulate carbonates and their preparation and use in thermoplastic film compositions |
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| DE10138490A1 (de) * | 2001-08-04 | 2003-02-13 | Degussa | Hydrophobe Fällungskieselsäure mit hohem Weißgrad und extrem niedriger Feuchtigkeitsaufnahme |
| GB2383046A (en) * | 2001-12-12 | 2003-06-18 | Imerys Minerals Ltd | Calcium carbonate filler in stretched polyolefin film |
| DE10247744A1 (de) * | 2002-10-10 | 2004-04-22 | Oskar Hauke | Material zur Errichtung oder Sanierung von Deichen |
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| FR2901491B1 (fr) | 2006-05-24 | 2009-03-20 | Coatex Sas | Procede de broyage a sec de materiaux contenant un minerai carbonate |
| AR061138A1 (es) * | 2006-06-09 | 2008-08-06 | Omya Development Ag | Compuestos de microparticulas inorganicas y/u organicas y nanoparticulas de dolomita |
| FR2913427B1 (fr) * | 2007-03-05 | 2011-10-07 | Omya Development Ag | Procede de broyage a sec d'un ou plusieurs materiaux comprenant au moins un carbonate de calcium |
| CN100436530C (zh) * | 2007-03-15 | 2008-11-26 | 上海交通大学 | 聚乙烯-醋酸乙烯酯基热可塑性木塑复合材料的制备方法 |
| FR2954715B1 (fr) | 2009-12-24 | 2014-12-26 | Coatex Sas | Utilisation de glycerol comme agent ameliorant le caractere autodispersant d'une matiere minerale destinee a une composition aqueuse |
| DK2371766T3 (da) | 2010-04-01 | 2013-05-06 | Omya Development Ag | Fremgangsmåde til at opnå præcipiteret calciumcarbonat |
| PT2558529T (pt) * | 2010-04-12 | 2016-08-19 | Omya Int Ag | Composição para moldagem por sopro |
| ES2540248T3 (es) | 2010-10-26 | 2015-07-09 | Omya Development Ag | Producción de carbonato de calcio precipitado de alta pureza |
| PL2447328T3 (pl) * | 2010-10-29 | 2015-05-29 | Omya Int Ag | Sposób polepszania właściwości materiałów zawierających węglan wapnia związanych z manipulowaniem |
| SI2524898T1 (sl) | 2011-05-16 | 2015-10-30 | Omya International Ag | Postopek za proizvodnjo oborjenega kalcijevega karbonata iz odpadne mlete papirne kaše |
| EP2626388B1 (en) * | 2012-02-09 | 2016-05-04 | Omya International AG | A composition and method for controlling the wettability of surfaces |
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- 2015-02-12 WO PCT/EP2015/053000 patent/WO2015124494A1/en active Application Filing
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- 2015-02-12 EP EP15705568.2A patent/EP3107967A1/en not_active Withdrawn
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- 2015-02-12 KR KR1020167025858A patent/KR20160124202A/ko active IP Right Grant
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Also Published As
| Publication number | Publication date |
|---|---|
| TW201544555A (zh) | 2015-12-01 |
| MX2016010842A (es) | 2016-11-17 |
| HRP20171368T1 (hr) | 2017-11-03 |
| US20170009076A1 (en) | 2017-01-12 |
| JP2017512849A (ja) | 2017-05-25 |
| US20190136066A1 (en) | 2019-05-09 |
| CN106029792A (zh) | 2016-10-12 |
| CA2939144A1 (en) | 2015-08-27 |
| US10619051B2 (en) | 2020-04-14 |
| CL2016002095A1 (es) | 2017-02-24 |
| HUE034671T2 (hu) | 2018-02-28 |
| JP6310089B2 (ja) | 2018-04-11 |
| KR20160124202A (ko) | 2016-10-26 |
| TWI530536B (zh) | 2016-04-21 |
| PL2910610T3 (pl) | 2017-12-29 |
| EP3107967A1 (en) | 2016-12-28 |
| AU2015220955B2 (en) | 2017-04-13 |
| EP2910610B1 (en) | 2017-07-05 |
| CN106029792B (zh) | 2018-09-11 |
| EP2910610A1 (en) | 2015-08-26 |
| AU2015220955A1 (en) | 2016-08-25 |
| RU2647026C1 (ru) | 2018-03-13 |
| US10316193B2 (en) | 2019-06-11 |
| SI2910610T1 (sl) | 2017-10-30 |
| ES2640099T3 (es) | 2017-10-31 |
| PT2910610T (pt) | 2017-09-15 |
| WO2015124494A1 (en) | 2015-08-27 |
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