DK0625578T4 - Sweetener, method of manufacture thereof, and use thereof - Google Patents

Sweetener, method of manufacture thereof, and use thereof

Info

Publication number
DK0625578T4
DK0625578T4 DK93120934T DK93120934T DK0625578T4 DK 0625578 T4 DK0625578 T4 DK 0625578T4 DK 93120934 T DK93120934 T DK 93120934T DK 93120934 T DK93120934 T DK 93120934T DK 0625578 T4 DK0625578 T4 DK 0625578T4
Authority
DK
Denmark
Prior art keywords
weight
glucopyranosyl
alpha
sorbitol
gps
Prior art date
Application number
DK93120934T
Other languages
Danish (da)
Other versions
DK0625578T3 (en
Inventor
Markwart Kunz
Mohammad Munir
Hanspeter Degelmann
Joerg Kowalczyk
Wolfgang Wach
Manfred Vogel
Original Assignee
Suedzucker Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=6487304&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=DK0625578(T4) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Suedzucker Ag filed Critical Suedzucker Ag
Publication of DK0625578T3 publication Critical patent/DK0625578T3/en
Application granted granted Critical
Publication of DK0625578T4 publication Critical patent/DK0625578T4/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P19/00Preparation of compounds containing saccharide radicals
    • C12P19/24Preparation of compounds containing saccharide radicals produced by the action of an isomerase, e.g. fructose
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/30Artificial sweetening agents
    • A23L27/33Artificial sweetening agents containing sugars or derivatives
    • A23L27/34Sugar alcohols
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P19/00Preparation of compounds containing saccharide radicals
    • C12P19/12Disaccharides

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Health & Medical Sciences (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Microbiology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Nutrition Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Seasonings (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Saccharide Compounds (AREA)
  • Jellies, Jams, And Syrups (AREA)
  • Confectionery (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Medicinal Preparation (AREA)

Abstract

The invention relates firstly to a process for the preparation of a sweetener in which sucrose is converted enzymatically into a saccharide mixture which is called "isomerised sucrose" and has a disaccharide content of more than 85% by weight, then non-isomerised remaining sucrose is removed from the latter by enzymatic and/or H<+> ion-catalysed cleavage, and this product is catalytically hydrogenated, the resulting mixture being subjected, preferably either before or after the catalytic hydrogenation, to a chromatographic separation. It also relates to sweeteners which have preferably been prepared by this process and which contain either a mixture of 10 to 50% by weight of 6-O- alpha -D-glucopyranosyl-D-sorbitol (= 1.6 GPS) 2 to 20% by weight of 1-O- alpha -D-glucopyranosyl-D-sorbitol (= 1.1 GPS) 30 to 70% by weight of 1-O- alpha -D-glucopyranosyl-D-mannitol (= 1.1 GPM) or of 5 to 10% by weight of 6-O- alpha -D-glucopyranosyl-D-sorbitol (= 1.6 GPS) 30 to 40% by weight of 1-O- alpha -D-glucopyranosyl-D-sorbitol (= 1.1 GPS) 45 to 60% by weight of 1-O- alpha -D-glucopyranosyl-D-mannitol (= 1.1 GPM)
DK93120934T 1993-05-06 1993-12-27 Sweetener, method of manufacture thereof, and use thereof DK0625578T4 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE4314961 1993-05-06

Publications (2)

Publication Number Publication Date
DK0625578T3 DK0625578T3 (en) 1996-11-11
DK0625578T4 true DK0625578T4 (en) 2004-08-02

Family

ID=6487304

Family Applications (1)

Application Number Title Priority Date Filing Date
DK93120934T DK0625578T4 (en) 1993-05-06 1993-12-27 Sweetener, method of manufacture thereof, and use thereof

Country Status (7)

Country Link
EP (1) EP0625578B2 (en)
JP (1) JP4446005B2 (en)
AT (1) ATE140032T1 (en)
DE (1) DE59303142D1 (en)
DK (1) DK0625578T4 (en)
ES (1) ES2089691T5 (en)
GR (1) GR3020742T3 (en)

Families Citing this family (41)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19532396C2 (en) * 1995-09-02 1997-08-21 Suedzucker Ag Sugar-free products and process for their preparation
DE19549645C5 (en) * 1995-09-02 2005-08-25 Südzucker AG Mannheim/Ochsenfurt Sugar-free coated products with layers of mixt. of glucopyranosyl-sorbitol and -mannitol derivs. - over core, also the mixt. and other products contg. it, useful in confectionery, baked goods, pharmaceuticals etc.
DE19549825B4 (en) * 1995-09-02 2010-11-04 Südzucker AG Mannheim/Ochsenfurt Sugar-free hard caramels
DE19606968C2 (en) * 1996-02-24 1998-07-09 Suedzucker Ag Use of 1,1-GPS in hard caramels
DE19639343C2 (en) * 1996-09-25 1998-10-08 Suedzucker Ag Comprimate containing a sweetener mixture
DE19639342C2 (en) 1996-09-25 1998-07-16 Suedzucker Ag Chewing gum containing a sweetener
DE19701439C2 (en) * 1997-01-17 2001-01-25 Suedzucker Ag Process for the hydrogenation of sugars
DE19758788B4 (en) * 1997-01-17 2007-12-13 Südzucker Aktiengesellschaft Mannheim/Ochsenfurt Stereo-selective hydrogenation of sugars to sugar alcohols with good purity - in aqueous solution, at high temperature and pressure, uses catalyst mixture of Raney metal and its alloy with inert core and active shell
DE19702609C1 (en) 1997-01-24 1998-06-25 Suedzucker Ag Coated, sugar-free chewing sweets with good consistency
DE19705664B4 (en) * 1997-02-14 2004-01-22 Südzucker AG Mannheim/Ochsenfurt Process for the preparation of phases enriched in 1,1-GPM with over 75% by weight of TS up to over 99% by weight of TS 1,1-GPM and 1,6-GPS-enriched phases with more than 80% by weight a.TS up to over 99% by weight a.TS 1.6 GPS
DE19709304C2 (en) * 1997-03-07 2002-08-14 Suedzucker Ag Process for the production of hard caramels and tablets
FI105048B (en) * 1997-05-22 2000-05-31 Xyrofin Oy Process for the preparation of isomaltulose and other products
DE19747642B4 (en) * 1997-10-29 2004-12-23 Südzucker AG Mannheim/Ochsenfurt Process for the production of sweeteners containing isomelecitosis, isomelecitosis and isomaltulose
DE19749820C1 (en) * 1997-11-11 1999-04-15 Suedzucker Ag Production of coated gelling agent with pectin core useful for making preserve and jelly
DE19818842C1 (en) * 1998-04-28 2000-01-05 Suedzucker Ag Cold remedy containing sugar alcohol mixture such as Isomalt, having immunostimulant and antimicrobial activity
DE19943496C1 (en) * 1999-09-10 2001-05-17 Suedzucker Ag Directly compressible raw material for compressed air
DE19943491B4 (en) 1999-09-10 2010-04-01 Südzucker AG Mannheim/Ochsenfurt Improved compressed
DE19945481A1 (en) * 1999-09-22 2001-04-05 Suedzucker Ag Hard caramels with improved storage stability
ATE454048T1 (en) 2000-05-22 2010-01-15 Ueno Fine Chemical Ind SOLID CRYSTALLINE MIXTURE AND PRODUCTION PROCESS
DE10221559B4 (en) * 2002-05-15 2009-04-30 Henkel Ag & Co. Kgaa Detergent and detergent tablets with active phase
JP4482336B2 (en) * 2004-01-05 2010-06-16 上野製薬株式会社 Method for producing isomaltulose crystals and reduced isomaltulose
DE102004013736A1 (en) * 2004-03-18 2005-10-06 Basf Ag Process for the enrichment of trehalose using aluminosilicates
DE102004038689A1 (en) * 2004-08-10 2006-03-02 Südzucker AG Mannheim/Ochsenfurt Organoleptically improved particularly storage-stable hard caramels
EP1804591B1 (en) 2004-10-15 2010-08-25 Südzucker Aktiengesellschaft Mannheim/Ochsenfurt Improved pan coating process
DE102005010833B4 (en) * 2005-03-07 2015-04-09 Südzucker Aktiengesellschaft Mannheim/Ochsenfurt A method of making a glazed or frosted cereal product having a core of cereals and a coating
WO2008025809A1 (en) * 2006-09-01 2008-03-06 Cargill, Incorporated Polyol syrups useful in the manufacture of sugar-free chewable confectionery
US20100267658A1 (en) 2009-04-15 2010-10-21 Sudzucker Aktiengesellschaft Mannheim/Ochsenfurt Trehalulose-containing composition, its preparation and use
EP2361255B1 (en) 2009-12-23 2014-06-11 Evonik Degussa GmbH Sweetener and method for the production thereof
DE102009060934A1 (en) 2009-12-23 2011-06-30 Südzucker AG Mannheim/Ochsenfurt, 68165 Improved pickle excipients
DE102011100772A1 (en) 2011-05-05 2012-11-08 Evonik Degussa Gmbh Process for the preparation of isomaltulose from plant juices
DE102011083030A1 (en) 2011-09-20 2013-03-21 Evonik Degussa Gmbh Mixture composition and its use as a sweetener
DE102013011977A1 (en) 2013-07-18 2015-01-22 Südzucker Aktiengesellschaft Mannheim/Ochsenfurt Optimized process for preparing an isomaltulose-containing composition
DE102014203964A1 (en) 2014-03-05 2015-09-10 Evonik Degussa Gmbh Granules containing isomaltulose synthase
EP3363909A1 (en) 2017-02-15 2018-08-22 Evonik Degussa GmbH Process for production of a solid material containing isomaltulose crystals and trehalulose
JP2020529846A (en) * 2017-08-02 2020-10-15 エボニック オペレーションズ ゲーエムベーハー Isomaltulose sweetener
DE102018201916A1 (en) * 2018-02-07 2019-08-08 Südzucker AG Solid functionally improved isomalt
DE102018201920A1 (en) 2018-02-07 2019-08-08 Südzucker AG Liquid functionally improved isomalt
US20220119436A1 (en) 2018-09-11 2022-04-21 Südzucker AG Method for improved production of isomalt
EP3653708A1 (en) 2018-11-14 2020-05-20 Evonik Operations GmbH Isomaltulose production
WO2022219094A1 (en) 2021-04-15 2022-10-20 Südzucker AG Process for producing 1,1-gpm- and/or 1,6-gps-enriched isomalt compositions
CN115029396B (en) * 2022-01-05 2024-09-10 山东天力药业有限公司 Method for effectively shortening one-step fermentation reaction period of vitamin C

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2217628C2 (en) 1972-04-12 1974-06-06 Sueddeutsche Zucker Ag Process for the production of alpha-D-glucopyranosido square bracket on 1-6 square bracket to sorbitol (isomaltite)
CH592141A5 (en) * 1972-04-12 1977-10-14 Sueddeutsche Zucker Ag
DE3241788A1 (en) * 1982-11-11 1984-05-17 Süddeutsche Zucker AG, 6800 Mannheim METHOD FOR PRODUCING 1-0- (ALPHA) -D-GLUCOPYRANOSIDO-D-FRUCTOSE AND USE AS A SWEETENER
JPS59162953A (en) * 1983-03-05 1984-09-13 Showa Denko Kk Cation-exchange resin, and separation of saccharide and sugar-alcohol using said resin
DE3403973A1 (en) * 1984-02-04 1985-08-14 Bayer Ag, 5090 Leverkusen METHOD FOR PRODUCING A MIXTURE OF (ALPHA) -D-GLUCOPYRANOSIDO-1,6-MANNITE AND (ALPHA) -D-GLUCOPYRANOSIDO-1,6-SORBITE FROM (ALPHA) -D-GLUCOPYRANOSIDO-1,6-FRUCTOSE
US5229276A (en) * 1990-10-31 1993-07-20 Mitsui Sugar Co., Ltd. Process for preparing trehalulose and isomaltulose
JP2756360B2 (en) * 1990-10-31 1998-05-25 三井製糖株式会社 Method for producing trehalulose and palatinose

Also Published As

Publication number Publication date
JP2008245650A (en) 2008-10-16
EP0625578B2 (en) 2004-04-28
ATE140032T1 (en) 1996-07-15
DE59303142D1 (en) 1996-08-08
EP0625578A1 (en) 1994-11-23
EP0625578B1 (en) 1996-07-03
DK0625578T3 (en) 1996-11-11
JP4446005B2 (en) 2010-04-07
ES2089691T3 (en) 1996-10-01
GR3020742T3 (en) 1996-11-30
ES2089691T5 (en) 2004-12-01

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