DK0469014T3 - Emulsifier-free liquid emulsion and method and apparatus for preparing the emulsion - Google Patents

Emulsifier-free liquid emulsion and method and apparatus for preparing the emulsion

Info

Publication number
DK0469014T3
DK0469014T3 DK90906170.7T DK90906170T DK0469014T3 DK 0469014 T3 DK0469014 T3 DK 0469014T3 DK 90906170 T DK90906170 T DK 90906170T DK 0469014 T3 DK0469014 T3 DK 0469014T3
Authority
DK
Denmark
Prior art keywords
emulsion
mixture
chamber portion
chamber
axis
Prior art date
Application number
DK90906170.7T
Other languages
Danish (da)
Inventor
Armando Ulrich
Walter H Ott
Original Assignee
Techno Bio Kk
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE8905075U external-priority patent/DE8905075U1/en
Application filed by Techno Bio Kk filed Critical Techno Bio Kk
Application granted granted Critical
Publication of DK0469014T3 publication Critical patent/DK0469014T3/en

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • B01F23/41Emulsifying
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/10Mixing by creating a vortex flow, e.g. by tangential introduction of flow components
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/10Mixing by creating a vortex flow, e.g. by tangential introduction of flow components
    • B01F25/102Mixing by creating a vortex flow, e.g. by tangential introduction of flow components wherein the vortex is created by two or more jets introduced tangentially in separate mixing chambers or consecutively in the same mixing chamber
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F2025/91Direction of flow or arrangement of feed and discharge openings
    • B01F2025/919Direction of flow or arrangement of feed and discharge openings characterised by the disposition of the feed and discharge openings
    • B01F2025/9191Direction of flow or arrangement of feed and discharge openings characterised by the disposition of the feed and discharge openings characterised by the arrangement of the feed openings for one or more flows, e.g. for the mainflow and the flow of an additional component

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Medicinal Preparation (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Cosmetics (AREA)
  • Polymerisation Methods In General (AREA)
  • Colloid Chemistry (AREA)
  • Processing Of Solid Wastes (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Emulgator-free liquid emulsion and method and device for producing the emulsion. The emulsion consists of at least one hydrophobic liquid phase and at least one hydrophilic liquid phase, one of said phases being a disperse phase of the emulsion, which has a stable colloidal state with a particle size of the disperse phase of 1,000 nm or less, preferably a particle size in the range of 100 to 500 nm. In the method for producing the liquid emulsion in absence of an emulgator, the liquid phases are repeatedly recirculated in the form of their mixture through a mixing chamber which has an axially symmetrical shape and in which the mixture is brought into a rotational flow about the axis with a flow component parallel to the axis and in which the flow pressure of the mixture is reduced in flow direction by gradually increasing the flow velocity of the mixture up to the coaxial discharge of the rotating mixture from the mixing chamber to a minimum pressure being near to the vapor pressure of the mixture without reaching or falling below the vapor pressure. In the device the mixing apparatus (1) comprising a mixing chamber of a rotational symmetrical shape in a hollow element (14) with a plurality of tangential inlet openings (15) opening into a first chamber portion connected to a second chamber portion having a tapering section in flow direction and an axial outlet being coaxial with the axis of the mixing chamber, the first chamber portion has a rotational paraboloid form and the second chamber portion has a rotational inverse hyperboloid form, said axial outlet being a cylindrical duct portion (18), the parabolic wall (14) of said first chamber portion defining a focal line falling in the axis of rotation, said inlet openings (15) being arranged at a wide cross-section of the first chamber portion which is connected to the second chamber portion at the widest cross-section thereof, and the sum of the cross-sections of the inlet openings (15) substantially corresponds to the cross-section of said duct portion (18).
DK90906170.7T 1989-04-21 1990-04-20 Emulsifier-free liquid emulsion and method and apparatus for preparing the emulsion DK0469014T3 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE8905075U DE8905075U1 (en) 1989-04-21 1989-04-21 Mixing device for flow media
JP10326889 1989-04-22

Publications (1)

Publication Number Publication Date
DK0469014T3 true DK0469014T3 (en) 1994-09-19

Family

ID=25954688

Family Applications (1)

Application Number Title Priority Date Filing Date
DK90906170.7T DK0469014T3 (en) 1989-04-21 1990-04-20 Emulsifier-free liquid emulsion and method and apparatus for preparing the emulsion

Country Status (13)

Country Link
EP (2) EP0469014B1 (en)
AT (1) ATE110001T1 (en)
AU (1) AU5422990A (en)
CA (1) CA2051438A1 (en)
DD (1) DD299620A5 (en)
DE (1) DE69011679T2 (en)
DK (1) DK0469014T3 (en)
ES (1) ES2057555T3 (en)
HU (1) HUT61909A (en)
IL (1) IL94162A (en)
PT (1) PT93846A (en)
RU (1) RU2072891C1 (en)
WO (1) WO1990012639A1 (en)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE9103927U1 (en) * 1991-03-30 1991-07-25 Oswald Bender GmbH, 65779 Kelkheim Device for mixing liquids, especially coloured paint residues
US7810674B2 (en) 2005-07-26 2010-10-12 Millipore Corporation Liquid dispensing system with enhanced mixing
US7950547B2 (en) 2006-01-12 2011-05-31 Millipore Corporation Reservoir for liquid dispensing system with enhanced mixing
DE102007047478A1 (en) * 2007-09-27 2009-04-16 Charité - Universitätsmedizin Berlin Apparatus and method for uniformly distributing microparticles in a liquid
RU2463100C1 (en) * 2011-03-05 2012-10-10 Овченкова Оксана Анатольевна Method of treatment and reactor to this end
RU2486950C1 (en) * 2012-03-27 2013-07-10 Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Пензенская государственная технологическая академия" Method of making solutions in cylindrical vertical vessel heated, mainly, at bottom, for example, for operation of slashing machine

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR844009A (en) * 1938-04-14 1939-07-18 Preparation of emulsions and colloidal suspensions in water, of perfumes, aromatic essences, petrolatum oils and other products used in perfumery, pharmaceuticals and industry
FR2461515A1 (en) * 1979-07-24 1981-02-06 Robert Guerin Emulsification of mutually insol. liquids - by pumping mixt. through passage of narrowing section with wide slowing and diverting sections to give ultra-colloidal emulsion
AU541324B2 (en) * 1979-08-01 1985-01-03 Exxon Research And Engineering Company Emulsifying immiscible liquids
DE3028005A1 (en) * 1980-07-24 1982-02-18 Bayer Ag, 5090 Leverkusen METHOD FOR PRODUCING PHARMACEUTICAL AND COSEMICAL DISPERSIONS
GB2092025A (en) * 1981-01-30 1982-08-11 Ici Plc Spraying emulsions
US4430251A (en) * 1981-09-29 1984-02-07 Hoffert Manufacturing Co., Inc. High energy emulsifier
EP0263443B1 (en) * 1986-10-08 1992-05-20 Zugol AG Method and device for producing a water-in-oil emulsion
EP0312642A1 (en) * 1987-10-23 1989-04-26 "Harrier" Gmbh Gesellschaft Für Den Vertrieb Medizinischer Und Technischer Geräte Method for introducing gas into water in superequilibrum quantity, apparatus for carrying out the method and water produced by the method

Also Published As

Publication number Publication date
EP0469014A1 (en) 1992-02-05
RU2072891C1 (en) 1997-02-10
EP0393715A1 (en) 1990-10-24
DE69011679T2 (en) 1995-02-16
AU5422990A (en) 1990-11-16
IL94162A (en) 1995-08-31
WO1990012639A1 (en) 1990-11-01
ES2057555T3 (en) 1994-10-16
IL94162A0 (en) 1991-01-31
EP0469014B1 (en) 1994-08-17
DD299620A5 (en) 1992-04-30
CA2051438A1 (en) 1990-10-22
HUT61909A (en) 1993-03-29
DE69011679D1 (en) 1994-09-22
PT93846A (en) 1990-11-20
HU903661D0 (en) 1991-12-30
ATE110001T1 (en) 1994-09-15

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