DE69625989D1 - Herstellungsverfahren für Sucrose-6-Ester - Google Patents

Herstellungsverfahren für Sucrose-6-Ester

Info

Publication number
DE69625989D1
DE69625989D1 DE69625989T DE69625989T DE69625989D1 DE 69625989 D1 DE69625989 D1 DE 69625989D1 DE 69625989 T DE69625989 T DE 69625989T DE 69625989 T DE69625989 T DE 69625989T DE 69625989 D1 DE69625989 D1 DE 69625989D1
Authority
DE
Germany
Prior art keywords
reaction mixture
sucrose
codistillation
water
solvent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69625989T
Other languages
English (en)
Other versions
DE69625989T2 (de
Inventor
James A White
Billy A Bradford
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tate and Lyle Technology Ltd
Original Assignee
McNeil PPC Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by McNeil PPC Inc filed Critical McNeil PPC Inc
Application granted granted Critical
Publication of DE69625989D1 publication Critical patent/DE69625989D1/de
Publication of DE69625989T2 publication Critical patent/DE69625989T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
    • C07H13/06—Fatty acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/08—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals directly attached to carbocyclic rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Saccharide Compounds (AREA)
  • Catalysts (AREA)
  • Silicon Polymers (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE69625989T 1995-11-28 1996-11-27 Herstellungsverfahren für Sucrose-6-Ester Expired - Lifetime DE69625989T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US766095P 1995-11-28 1995-11-28

Publications (2)

Publication Number Publication Date
DE69625989D1 true DE69625989D1 (de) 2003-03-06
DE69625989T2 DE69625989T2 (de) 2003-11-13

Family

ID=21727452

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69625989T Expired - Lifetime DE69625989T2 (de) 1995-11-28 1996-11-27 Herstellungsverfahren für Sucrose-6-Ester

Country Status (9)

Country Link
EP (1) EP0776903B1 (de)
JP (1) JP4168168B2 (de)
AT (1) ATE231876T1 (de)
CA (1) CA2191412C (de)
DE (1) DE69625989T2 (de)
DK (1) DK0776903T3 (de)
ES (1) ES2191745T3 (de)
NO (1) NO307381B1 (de)
RU (1) RU2159773C2 (de)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2365424B (en) * 2000-07-31 2002-06-26 Tate & Lyle Plc An improved method for the synthesis of sucrose-6-esters
CN100418976C (zh) 2006-04-03 2008-09-17 广州科宏食品添加物有限公司 一种三氯蔗糖的制备方法
GB0702854D0 (en) * 2007-01-09 2007-03-28 Tate & Lyle Plc Method for the synthesis of sucrose-6-esters
US8476424B2 (en) * 2008-03-20 2013-07-02 Tate & Lyle Technology Limited Removal of acids from tertiary amide solvents
GB2468936B (en) * 2009-03-27 2011-09-07 Mohamad Rami Radwan Jaber Chlorination of sucrose-6-esters
GB2469158B (en) 2009-03-31 2011-09-28 Peter J Seaberg Base-assisted formation of tin-sucrose adducts
GB2474310B (en) 2009-10-12 2012-02-29 Tate & Lyle Technology Ltd Process for the production of sucrose-6-ester
GB2474311B (en) 2009-10-12 2012-10-17 Tate & Lyle Technology Ltd Low temperature, single solvent process for the production of sucrose-6-ester
GB201110520D0 (en) 2011-05-10 2011-08-03 Tate & Lyle Technology Ltd Extraction of carboxylic acids with tin compounds
CN105111246B (zh) * 2015-08-22 2017-11-17 安徽金禾实业股份有限公司 三氯蔗糖生产中有机锡的回收方法
CN106349300B (zh) * 2016-08-30 2019-02-26 安徽金禾实业股份有限公司 三氯蔗糖酯化单溶剂反应方法
CN112480164A (zh) * 2020-12-11 2021-03-12 安徽金禾实业股份有限公司 一种蔗糖-6-乙酯生产中回收制备有机锡催化剂的方法
EP4163000B1 (de) * 2021-02-19 2024-04-10 Anhui Jinhe Industrial Co., Ltd. Vorrichtung und verfahren zur herstellung von saccharose-6-ester
WO2022174382A1 (zh) * 2021-02-19 2022-08-25 安徽金禾实业股份有限公司 蔗糖-6-酯的生产设备及生产方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6287248A (ja) * 1985-10-11 1987-04-21 Kuraray Co Ltd エステル化触媒
US4950746A (en) * 1988-07-18 1990-08-21 Noramco, Inc. Process for synthesizing sucrose derivatives by regioselective reaction
US5089608A (en) 1990-03-23 1992-02-18 Mcneil-Ppc, Inc. Selective 6-acylation of sucrose mediated by cyclic adducts of dialkyltin oxides and diols
US5023329A (en) 1990-04-23 1991-06-11 Noramco, Inc. Sucrose-6-ester production process
US5034551A (en) 1990-04-23 1991-07-23 Noramco, Inc. Process for recovery of organotin esters from reaction mixtures containing the same and re-use of the recovered organotin compounds
GR910100356A (el) 1990-08-27 1992-08-31 Mcneil Ppc Inc Καταλυόμενη μέ?οδος εστέρος-6-σακχαρόζης.
US5470969A (en) 1990-08-27 1995-11-28 Mcneil-Ppc, Inc. Catalyzed sucrose-6-ester process

Also Published As

Publication number Publication date
JPH09309894A (ja) 1997-12-02
CA2191412C (en) 2005-10-11
NO965048L (no) 1997-05-29
EP0776903A1 (de) 1997-06-04
ES2191745T3 (es) 2003-09-16
EP0776903B1 (de) 2003-01-29
NO307381B1 (no) 2000-03-27
NO965048D0 (no) 1996-11-27
CA2191412A1 (en) 1997-05-29
DE69625989T2 (de) 2003-11-13
ATE231876T1 (de) 2003-02-15
DK0776903T3 (da) 2003-05-12
RU2159773C2 (ru) 2000-11-27
JP4168168B2 (ja) 2008-10-22

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8327 Change in the person/name/address of the patent owner

Owner name: TATE & LYLE PUBLIC LIMITED COMPANY, LONDON, GB

8328 Change in the person/name/address of the agent

Representative=s name: MARKS & CLERK, LUXEMBOURG, LU

8327 Change in the person/name/address of the patent owner

Owner name: TATE & LYLE TECHNOLOGY LTD., LONDON, GB

8328 Change in the person/name/address of the agent

Representative=s name: MOSELPATENT TRIERPATENT, 54290 TRIER

8328 Change in the person/name/address of the agent

Representative=s name: PATENTANWAELTE SERWE & DR. WAGNER, 54290 TRIER