DE602004028357D1 - Verfahren zur herstellung von tocyl- und tocopheryl-acylaten - Google Patents
Verfahren zur herstellung von tocyl- und tocopheryl-acylatenInfo
- Publication number
- DE602004028357D1 DE602004028357D1 DE602004028357T DE602004028357T DE602004028357D1 DE 602004028357 D1 DE602004028357 D1 DE 602004028357D1 DE 602004028357 T DE602004028357 T DE 602004028357T DE 602004028357 T DE602004028357 T DE 602004028357T DE 602004028357 D1 DE602004028357 D1 DE 602004028357D1
- Authority
- DE
- Germany
- Prior art keywords
- tocyl
- tocopheryl
- rac
- preparation
- tocopherol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title abstract 3
- ZAKOWWREFLAJOT-ADUHFSDSSA-N [2,5,7,8-tetramethyl-2-[(4R,8R)-4,8,12-trimethyltridecyl]-3,4-dihydrochromen-6-yl] acetate Chemical compound CC(=O)OC1=C(C)C(C)=C2OC(CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-ADUHFSDSSA-N 0.000 title 1
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 abstract 3
- -1 tocopheryl acylate Chemical compound 0.000 abstract 3
- 239000003377 acid catalyst Substances 0.000 abstract 2
- 239000007787 solid Substances 0.000 abstract 2
- 229960001295 tocopherol Drugs 0.000 abstract 2
- 239000011732 tocopherol Substances 0.000 abstract 2
- DFUSDJMZWQVQSF-XLGIIRLISA-N (2r)-2-methyl-2-[(4r,8r)-4,8,12-trimethyltridecyl]-3,4-dihydrochromen-6-ol Chemical compound OC1=CC=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1 DFUSDJMZWQVQSF-XLGIIRLISA-N 0.000 abstract 1
- ODIGIKRIUKFKHP-UHFFFAOYSA-N (n-propan-2-yloxycarbonylanilino) acetate Chemical compound CC(C)OC(=O)N(OC(C)=O)C1=CC=CC=C1 ODIGIKRIUKFKHP-UHFFFAOYSA-N 0.000 abstract 1
- 229930003427 Vitamin E Natural products 0.000 abstract 1
- 230000010933 acylation Effects 0.000 abstract 1
- 238000005917 acylation reaction Methods 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 229920001296 polysiloxane Polymers 0.000 abstract 1
- 239000011148 porous material Substances 0.000 abstract 1
- 229930003799 tocopherol Natural products 0.000 abstract 1
- 235000010384 tocopherol Nutrition 0.000 abstract 1
- 239000011709 vitamin E Substances 0.000 abstract 1
- 229940046009 vitamin E Drugs 0.000 abstract 1
- 235000019165 vitamin E Nutrition 0.000 abstract 1
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
- C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
- C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
- C07D311/58—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4
- C07D311/70—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4 with two hydrocarbon radicals attached in position 2 and elements other than carbon and hydrogen in position 6
- C07D311/72—3,4-Dihydro derivatives having in position 2 at least one methyl radical and in position 6 one oxygen atom, e.g. tocopherols
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Pyrane Compounds (AREA)
- Catalysts (AREA)
- Seasonings (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Medicines Containing Plant Substances (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP03009985 | 2003-05-02 | ||
| PCT/EP2004/004443 WO2004096791A2 (en) | 2003-05-02 | 2004-04-27 | Process for the manufacture of tocyl and tocopheryl acylates |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE602004028357D1 true DE602004028357D1 (de) | 2010-09-09 |
Family
ID=33395781
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE602004028357T Expired - Lifetime DE602004028357D1 (de) | 2003-05-02 | 2004-04-27 | Verfahren zur herstellung von tocyl- und tocopheryl-acylaten |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US7321053B2 (de) |
| EP (2) | EP2206708A1 (de) |
| JP (2) | JP4740834B2 (de) |
| KR (1) | KR101126811B1 (de) |
| CN (2) | CN1780827B (de) |
| AT (1) | ATE475657T1 (de) |
| DE (1) | DE602004028357D1 (de) |
| ES (1) | ES2347653T3 (de) |
| WO (1) | WO2004096791A2 (de) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2007039245A1 (en) * | 2005-09-29 | 2007-04-12 | Dsm Ip Assets B.V. | Cleavage of alkynediols |
| CN101578255B (zh) | 2006-12-27 | 2013-11-06 | 帝斯曼知识产权资产管理有限公司 | 有机羟基化合物的酰化方法 |
| CN102276572B (zh) * | 2011-09-14 | 2013-03-27 | 重庆大学 | 一种制备维生素e乙酸酯的方法 |
| KR101787248B1 (ko) | 2016-04-14 | 2017-10-18 | 라인 가부시키가이샤 | 메신저 서비스를 이용한 키워드 검색 방법 및 시스템 |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2723278A (en) | 1954-01-25 | 1955-11-08 | Hoffmann La Roche | Preparation of alpha-tocopherol |
| US3459773A (en) * | 1966-12-27 | 1969-08-05 | Takasago Perfumery Co Ltd | Process for producing alpha-tocopherol and its esters |
| JPS4955633A (de) | 1972-07-30 | 1974-05-30 | ||
| DE3226093A1 (de) | 1982-07-13 | 1984-01-19 | Degussa Ag, 6000 Frankfurt | Sulfonatgruppen-haltige organopolysiloxane, verfahren zu ihrer herstellung und verwendung |
| DE4012479A1 (de) | 1990-04-19 | 1991-10-24 | Degussa | Titandioxidpresslinge, verfahren zu ihrer herstellung sowie ihre verwendung |
| DE4223539C1 (de) * | 1992-07-17 | 1993-11-25 | Degussa | Geformte Sulfonatgruppen-haltige Organopolysiloxane, Verfahren zu ihrer Herstellung und Verwendung |
| US5587349A (en) * | 1994-02-15 | 1996-12-24 | Mitsubishi Gas Chemical Company, Inc. | Process for preparing silica-titania catalyst |
| JP3712008B2 (ja) * | 1994-02-15 | 2005-11-02 | 三菱瓦斯化学株式会社 | カルボン酸エステル製造用シリカ−チタニア触媒の製造方法 |
| DE19619961A1 (de) | 1996-05-17 | 1997-11-20 | Degussa | Preßlinge auf Basis von pyrogen hergestelltem Siliciumdioxid |
| DE19635769A1 (de) * | 1996-09-04 | 1998-03-05 | Degussa | Verfahren zur Herstellung von Carbonsäureestern und dafür geeignete Katalysatoren |
| MY115474A (en) * | 1996-12-12 | 2003-06-30 | Sasol Tech Pty Ltd | Production of organic carboxylic acid esters. |
| DE19750238A1 (de) | 1997-11-13 | 1999-05-27 | Degussa | Preßlinge auf Basis von pyrogen hergestelltem Siliciumdioxid |
| DE19843845A1 (de) * | 1998-09-24 | 2000-03-30 | Degussa | Formkörper, bestehend aus pyrogenem Mischoxid und deren Verwendung |
| ES2243585T3 (es) * | 2000-11-22 | 2005-12-01 | Basf Aktiengesellschaft | Procedimiento para la acilacion en cintinuo de derivados del ester de cromanol. |
| WO2004096790A1 (en) * | 2003-04-28 | 2004-11-11 | Dsm Ip Assets B.V. | Process for the manufacture of tocyl and tocopheryl acylates |
-
2004
- 2004-04-27 CN CN2004800112783A patent/CN1780827B/zh not_active Expired - Lifetime
- 2004-04-27 ES ES04729614T patent/ES2347653T3/es not_active Expired - Lifetime
- 2004-04-27 JP JP2006505290A patent/JP4740834B2/ja not_active Expired - Fee Related
- 2004-04-27 CN CN201010151061XA patent/CN101899032B/zh not_active Expired - Lifetime
- 2004-04-27 DE DE602004028357T patent/DE602004028357D1/de not_active Expired - Lifetime
- 2004-04-27 EP EP10157639A patent/EP2206708A1/de not_active Withdrawn
- 2004-04-27 AT AT04729614T patent/ATE475657T1/de not_active IP Right Cessation
- 2004-04-27 WO PCT/EP2004/004443 patent/WO2004096791A2/en active Search and Examination
- 2004-04-27 US US10/554,885 patent/US7321053B2/en not_active Expired - Lifetime
- 2004-04-27 KR KR1020057020815A patent/KR101126811B1/ko active IP Right Grant
- 2004-04-27 EP EP04729614A patent/EP1622887B1/de not_active Expired - Lifetime
-
2011
- 2011-01-26 JP JP2011014518A patent/JP5300883B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| JP2006525263A (ja) | 2006-11-09 |
| ATE475657T1 (de) | 2010-08-15 |
| JP4740834B2 (ja) | 2011-08-03 |
| JP5300883B2 (ja) | 2013-09-25 |
| US20060293529A1 (en) | 2006-12-28 |
| KR101126811B1 (ko) | 2012-03-23 |
| US7321053B2 (en) | 2008-01-22 |
| EP1622887A2 (de) | 2006-02-08 |
| CN101899032A (zh) | 2010-12-01 |
| CN1780827A (zh) | 2006-05-31 |
| CN1780827B (zh) | 2010-06-16 |
| EP1622887B1 (de) | 2010-07-28 |
| JP2011105746A (ja) | 2011-06-02 |
| EP2206708A1 (de) | 2010-07-14 |
| CN101899032B (zh) | 2012-05-30 |
| WO2004096791A2 (en) | 2004-11-11 |
| ES2347653T3 (es) | 2010-11-03 |
| WO2004096791A3 (en) | 2005-01-06 |
| KR20060011983A (ko) | 2006-02-06 |
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