DE60109188D1 - Auf quaternären borverbindungen basierende polymerisationsinitiatoren und deren verwendungen zur bindung von substraten mit niedriger oberflächenenergie - Google Patents
Auf quaternären borverbindungen basierende polymerisationsinitiatoren und deren verwendungen zur bindung von substraten mit niedriger oberflächenenergieInfo
- Publication number
- DE60109188D1 DE60109188D1 DE60109188T DE60109188T DE60109188D1 DE 60109188 D1 DE60109188 D1 DE 60109188D1 DE 60109188 T DE60109188 T DE 60109188T DE 60109188 T DE60109188 T DE 60109188T DE 60109188 D1 DE60109188 D1 DE 60109188D1
- Authority
- DE
- Germany
- Prior art keywords
- lithium
- alkyl
- butylborohydride
- sec
- triethylborohydride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F4/00—Polymerisation catalysts
- C08F4/42—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors
- C08F4/44—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides
- C08F4/52—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides selected from boron, aluminium, gallium, indium, thallium or rare earths
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J4/00—Adhesives based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; adhesives, based on monomers of macromolecular compounds of groups C09J183/00 - C09J183/16
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31855—Of addition polymer from unsaturated monomers
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31855—Of addition polymer from unsaturated monomers
- Y10T428/31909—Next to second addition polymer from unsaturated monomers
- Y10T428/31928—Ester, halide or nitrile of addition polymer
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31855—Of addition polymer from unsaturated monomers
- Y10T428/31935—Ester, halide or nitrile of addition polymer
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Polymerization Catalysts (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP00650166A EP1201722A1 (de) | 2000-10-23 | 2000-10-23 | Polymerisationsinitiatoren, polymerisierbare Zusammensetzungen und deren Verwendungen |
EP00650166 | 2000-10-23 | ||
PCT/IE2001/000133 WO2002034851A1 (en) | 2000-10-23 | 2001-10-23 | Quaternary boron compound polymerisation initiators, polymerisable compositions, and uses thereof for bonding low surface energy substrates |
Publications (2)
Publication Number | Publication Date |
---|---|
DE60109188D1 true DE60109188D1 (de) | 2005-04-07 |
DE60109188T2 DE60109188T2 (de) | 2006-04-06 |
Family
ID=8174477
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE60109188T Expired - Lifetime DE60109188T2 (de) | 2000-10-23 | 2001-10-23 | Auf quaternären borverbindungen basierende polymerisationsinitiatoren und deren verwendungen zur bindung von substraten mit niedriger oberflächenenergie |
Country Status (8)
Country | Link |
---|---|
US (3) | US7189463B2 (de) |
EP (2) | EP1201722A1 (de) |
AT (1) | ATE290054T1 (de) |
AU (2) | AU2002210857A1 (de) |
DE (1) | DE60109188T2 (de) |
ES (1) | ES2236315T3 (de) |
PT (1) | PT1328597E (de) |
WO (2) | WO2002034851A1 (de) |
Families Citing this family (36)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1201722A1 (de) * | 2000-10-23 | 2002-05-02 | Loctite (R & D) Limited | Polymerisationsinitiatoren, polymerisierbare Zusammensetzungen und deren Verwendungen |
AU2003225512A1 (en) * | 2002-04-19 | 2003-11-03 | Loctite (R And D) Limited | Polymerisation initiators based on ammonium tetraalkyl boranes, polymerisable compositions, and uses thereof for bonding low surface energy substrates |
US7166651B2 (en) * | 2003-05-19 | 2007-01-23 | Kerr Corporation | Two-part self-adhering dental compositions |
CN100480279C (zh) * | 2003-06-09 | 2009-04-22 | 陶氏环球技术公司 | 稳定的有机硼烷聚合反应引发剂和可聚合的组合物 |
KR20060064618A (ko) | 2003-08-13 | 2006-06-13 | 다우 글로벌 테크놀로지스 인크. | 배관 시스템과 장비, 설비, 장치, 구조물 및 기구의배관을 접합하는 방법 |
GB0326286D0 (en) | 2003-11-11 | 2003-12-17 | Vantico Gmbh | Initiator systems for polymerisable compositions |
US8501886B2 (en) * | 2003-12-22 | 2013-08-06 | Dow Global Technologies Llc | Accelerated organoborane amine complex initiated polymerizable compositions |
ES2309598T3 (es) | 2003-12-22 | 2008-12-16 | Dow Global Technologies Inc. | Composiciones polimerizables de manera acelerada iniciadas por complejos de organoborano-amina. |
CN1926703A (zh) * | 2004-01-22 | 2007-03-07 | 汉高公司 | 用于粘合及密封燃料电池用低表面能基质的可聚合组合物 |
US8202932B2 (en) | 2004-12-03 | 2012-06-19 | Loctite (R&D) Limited | Adhesive bonding systems having adherence to low energy surfaces |
US7408012B1 (en) | 2005-04-18 | 2008-08-05 | Loctite (R&D) Limited | Adhesive bonding systems having adherence to low energy surfaces |
EP1934296A1 (de) * | 2005-10-07 | 2008-06-25 | Dow Gloval Technologies Inc. | Amido-organoborat-initiatorsysteme |
DE102005049681B4 (de) * | 2005-10-14 | 2011-03-10 | Henkel Ag & Co. Kgaa | Hülsenförmige Etiketten |
US20080103274A1 (en) * | 2006-10-12 | 2008-05-01 | Jialanella Gary L | Accelerated organoborane initiated polymerizable compositions |
US7524907B2 (en) * | 2006-10-12 | 2009-04-28 | Dow Global Technologies, Inc. | Accelerated organoborane initiated polymerizable compositions |
CA2685154C (en) * | 2007-04-25 | 2014-12-23 | Dentsply International Inc. | Self-adhesive dental cement having dual paste components |
US8742050B2 (en) | 2008-03-28 | 2014-06-03 | Henkel US IP LLC | Two part hybrid adhesive |
US20110104508A1 (en) * | 2008-08-29 | 2011-05-05 | Dow Global Technologies Inc. | Adhesive for bonding to flexible polymer surfaces |
US7825202B2 (en) * | 2008-10-09 | 2010-11-02 | The Goodyear Tire & Rubber Company | Potassium based catalyst systems for synthesizing rubbery polymers |
CN102203984A (zh) * | 2008-11-04 | 2011-09-28 | 加州理工学院 | 具有可溶性阳极的混合型电化学发生器 |
GB2491170B (en) | 2011-05-26 | 2013-11-06 | Henkel Ireland Ltd | Two-part polymerisable compositions |
GB2497114B (en) * | 2011-12-01 | 2015-02-18 | Spinnaker Int Ltd | Adhesive composition |
WO2013151680A1 (en) | 2012-04-06 | 2013-10-10 | Ips Corporation | Adhesive composition for bonding low surface energy polyolefin substrates |
US10266726B2 (en) | 2013-12-11 | 2019-04-23 | Sika Technology Ag | Pretreatment of substrates that have unsaturated units |
JP6694823B2 (ja) | 2014-03-27 | 2020-05-20 | スリーエム イノベイティブ プロパティズ カンパニー | 有機ホウ素を含む組成物、及びその使用方法 |
EP3103847A1 (de) | 2015-06-10 | 2016-12-14 | Sika Technology AG | Verbindung von fugenbändern |
GB201709352D0 (en) | 2017-06-13 | 2017-07-26 | Henkel IP & Holding GmbH | Activating surfaces for subsequent bonding |
US11787911B2 (en) | 2017-06-13 | 2023-10-17 | Henkel Ag & Co. Kgaa | Activating surfaces for subsequent bonding |
GB2579608B (en) | 2018-12-06 | 2023-02-15 | Henkel Ag & Co Kgaa | Activating surfaces for subsequent bonding to another substrate |
GB2580162B (en) | 2018-12-21 | 2022-07-13 | Henkel IP & Holding GmbH | One-part photocurable (meth) acrylate compositions |
GB2583920B (en) | 2019-05-10 | 2023-09-27 | Henkel Ag & Co Kgaa | Method for bonding three-dimensional articles made by additive manufacturing |
FR3098815B1 (fr) * | 2019-07-18 | 2021-06-25 | Bostik Sa | Procédé de polymérisation avec un complexe de borane-amine |
GB2593752B (en) | 2020-04-01 | 2023-06-14 | Henkel Ag & Co Kgaa | Anaerobically curable compositions |
GB2593754B (en) | 2020-04-01 | 2022-12-28 | Henkel Ag & Co Kgaa | Redox curable compositions and methods of manufacture thereof |
GB2606002B (en) | 2021-04-21 | 2023-06-14 | Henkel Ag & Co Kgaa | Anaerobically curable compositions |
GB2622079A (en) | 2022-09-01 | 2024-03-06 | Henkel Ag & Co Kgaa | Anaerobically curable compositions |
Family Cites Families (54)
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BE599646A (de) | 1960-02-02 | |||
US3275611A (en) * | 1960-12-30 | 1966-09-27 | Monsanto Co | Process for polymerizing unsaturated monomers with a catalyst comprising an organoboron compound, a peroxygen compound and an amine |
US3661744A (en) * | 1966-07-26 | 1972-05-09 | Grace W R & Co | Photocurable liquid polyene-polythiol polymer compositions |
US3898349A (en) * | 1966-07-26 | 1975-08-05 | Grace W R & Co | Polyene/polythiol paint vehicle |
US4008340A (en) * | 1973-05-21 | 1977-02-15 | General Foods Corporation | Method for stabilizing coffee grinder gas aroma |
US3996308A (en) * | 1974-02-19 | 1976-12-07 | Avery Products Corporation | Anaerobic pressure sensitive adhesive composition |
JPS5313382B2 (de) * | 1974-07-10 | 1978-05-10 | ||
US4295909A (en) * | 1975-02-03 | 1981-10-20 | Loctite Corporation | Curable polybutadiene-based resins having improved properties |
US4018851A (en) * | 1975-03-12 | 1977-04-19 | Loctite Corporation | Curable poly(alkylene) ether polyol-based grafted resins having improved properties |
US4215209A (en) | 1979-06-22 | 1980-07-29 | National Starch And Chemical Corporation | Anaerobic curing composition and process for preparing same |
DE3143945A1 (de) * | 1981-11-05 | 1983-05-11 | Henkel KGaA, 4000 Düsseldorf | 2-komponentige no-mix-klebstoffe, verfahren zu ihrer herstellung und ihre verwendung |
DE3201731A1 (de) * | 1982-01-21 | 1983-07-28 | Henkel KGaA, 4000 Düsseldorf | "aerob haertende kunststoffmassen" |
DE3201780A1 (de) * | 1982-01-21 | 1983-08-25 | Henkel KGaA, 4000 Düsseldorf | Neue polymere organo-borverbindungen und ihre verwendung |
DE3207264A1 (de) * | 1982-03-01 | 1983-09-08 | Henkel KGaA, 4000 Düsseldorf | Neue boralkylverbindungen, verfahren zu ihrer herstellung und ihre verwendung |
US4536546A (en) | 1983-09-22 | 1985-08-20 | Illinois Tool Works Inc. | (Meth)acrylate-based compositions |
DE3518965A1 (de) * | 1985-05-25 | 1986-11-27 | Henkel KGaA, 40589 Düsseldorf | Schmelzbare und dabei aerob aushaertende kunststoffmassen und verfahren zu ihrer herstellung |
US4772530A (en) | 1986-05-06 | 1988-09-20 | The Mead Corporation | Photosensitive materials containing ionic dye compounds as initiators |
US5151520A (en) * | 1985-11-20 | 1992-09-29 | The Mead Corporation | Cationic dye-triarylmonoalkylorate anion complexes |
US4772541A (en) * | 1985-11-20 | 1988-09-20 | The Mead Corporation | Photohardenable compositions containing a dye borate complex and photosensitive materials employing the same |
US4808638A (en) | 1986-10-14 | 1989-02-28 | Loctite Corporation | Thiolene compositions on based bicyclic 'ene compounds |
US4950581A (en) | 1987-07-06 | 1990-08-21 | Fuji Photo Film Co., Ltd. | Photopolymerizable composition |
US4963220A (en) | 1988-01-22 | 1990-10-16 | Dymax Corporation | Adhesive system utilizing metal ion-containing activator |
US4942201A (en) * | 1988-08-29 | 1990-07-17 | Illinois Tool Works, Inc. | Adhesive for low temperature applications |
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US5143884A (en) | 1991-04-29 | 1992-09-01 | National Starch And Chemical Investment Holding Corporation | Acrylic adhesive composition and organoboron initiator system |
US5106928A (en) | 1991-04-29 | 1992-04-21 | National Starch And Chemical Investment Holding Corporation | Acrylic adhesive composition and organoboron initiator system |
US5286821A (en) * | 1992-03-17 | 1994-02-15 | National Starch And Chemical Investment Holding Corporation | Acrylic adhesive composition and organoboron initiator system |
US5310835A (en) * | 1993-09-30 | 1994-05-10 | National Starch And Chemical Investment Holding Corporation | Transparent two-part acrylic adhesive composition and the method of use thereof |
DE69427411T2 (de) * | 1994-02-22 | 2002-06-06 | Minnesota Mining & Mfg | Polymerisierbare zusammensetzung die polymerisationsinitiatorsysteme auf basis von organoboran-amin-komplexen enthält |
US5621143A (en) | 1995-04-14 | 1997-04-15 | Minnesota Mining And Manufacturing Company | Organoborane polyoxyalkylenepolyamine complexes and adhesive compositions made therewith |
US5616796A (en) | 1995-04-14 | 1997-04-01 | Minnesota Mining And Manufacturing Company | Organoborane polyamine complexes and adhesive composition made therewith |
AU6177796A (en) | 1995-08-11 | 1997-03-12 | Minnesota Mining And Manufacturing Company | Initiator system and adhesive composition made therewith |
US5686544A (en) * | 1995-08-11 | 1997-11-11 | Minnesota Mining And Manufacturing Company | Organoborane polyamine complex initiator systems and polymerizable compositions made therewith |
JP2000500172A (ja) * | 1995-11-07 | 2000-01-11 | ミネソタ・マイニング・アンド・マニュファクチャリング・カンパニー | 開始剤系とそれを用いて製造した接着剤組成物 |
US5866631A (en) * | 1995-12-22 | 1999-02-02 | Tokuyama Corporation | Dental primer composition and polymerization catalyst |
JP3431782B2 (ja) | 1996-03-08 | 2003-07-28 | 昭和高分子株式会社 | 硬化性複合材料組成物及びその硬化方法 |
JPH1081838A (ja) * | 1996-07-16 | 1998-03-31 | Showa Denko Kk | 光硬化性材料及びその硬化方法 |
US5935711A (en) * | 1996-10-23 | 1999-08-10 | 3M Innovative Properties Company | Organoborane amine complex initiator systems and polymerizable compositions made therewith |
EP1098943B1 (de) | 1998-06-12 | 2004-01-21 | Minnesota Mining And Manufacturing Company | Geruchsarme polymerisierbare zusammensetzungen zum binden von substraten mit niedriger oberflächenenergie |
US6252023B1 (en) | 1999-03-19 | 2001-06-26 | 3M Innovative Properties Company | Organoborane amine complex inatator systems and polymerizable compositions made therewith |
JP2000327683A (ja) | 1999-05-24 | 2000-11-28 | Fuji Photo Film Co Ltd | ボレート化合物、それを含む光重合性組成物及び記録材料 |
US6486090B1 (en) | 1999-11-04 | 2002-11-26 | 3M Innovative Properties Company | Initiator/hydroxide and initiator/alkoxide complexes, systems comprising the complexes, and polymerized compositions made therewith |
US6410667B1 (en) | 1999-11-04 | 2002-06-25 | 3M Innovative Properties Company | Initiator/amidine complexes, systems comprising the complexes, and polymerized compositions made therewith |
US6806330B1 (en) | 1999-12-17 | 2004-10-19 | Dow Global Technologies Inc. | Amine organoborane complex polymerization initiators and polymerizable compositions |
US6660784B2 (en) * | 2000-09-26 | 2003-12-09 | Tokuyama Corporation | Dental catalyst for chemical polymerization and use thereof |
EP1201722A1 (de) * | 2000-10-23 | 2002-05-02 | Loctite (R & D) Limited | Polymerisationsinitiatoren, polymerisierbare Zusammensetzungen und deren Verwendungen |
US20020195453A1 (en) | 2001-05-02 | 2002-12-26 | Mcleod David G. | Fuel tanks and fuel transport lines |
US20030044553A1 (en) | 2001-08-23 | 2003-03-06 | Ravi Ramanathan | Fuel tanks |
US20030047268A1 (en) | 2001-08-23 | 2003-03-13 | Korchnak Gregory J. | Method for repairing fuel tanks |
IE20020293A1 (en) * | 2002-04-23 | 2003-10-29 | Loctite R & D Ltd | Initiator systems, polymerisable compositions, and uses thereof for bonding low surface energy substrates |
US6630555B2 (en) | 2001-11-06 | 2003-10-07 | Lord Corporation | Internally blocked organoborate initiators and adhesives therefrom |
US6734268B2 (en) * | 2001-12-31 | 2004-05-11 | 3M Innovative Properties Company | Metal salt modifiers for bonding compositions |
AU2003225512A1 (en) * | 2002-04-19 | 2003-11-03 | Loctite (R And D) Limited | Polymerisation initiators based on ammonium tetraalkyl boranes, polymerisable compositions, and uses thereof for bonding low surface energy substrates |
US7098279B2 (en) * | 2002-10-22 | 2006-08-29 | Loctite (R&D) Limited | Non-flammable and non-combustible adhesive bonding systems having adherence to low energy surfaces |
-
2000
- 2000-10-23 EP EP00650166A patent/EP1201722A1/de not_active Withdrawn
-
2001
- 2001-10-23 AT AT01976581T patent/ATE290054T1/de not_active IP Right Cessation
- 2001-10-23 WO PCT/IE2001/000133 patent/WO2002034851A1/en active IP Right Grant
- 2001-10-23 AU AU2002210857A patent/AU2002210857A1/en not_active Abandoned
- 2001-10-23 US US10/399,230 patent/US7189463B2/en not_active Expired - Fee Related
- 2001-10-23 DE DE60109188T patent/DE60109188T2/de not_active Expired - Lifetime
- 2001-10-23 AU AU2001295845A patent/AU2001295845A1/en not_active Abandoned
- 2001-10-23 PT PT01976581T patent/PT1328597E/pt unknown
- 2001-10-23 EP EP01976581A patent/EP1328597B1/de not_active Expired - Lifetime
- 2001-10-23 WO PCT/IE2001/000134 patent/WO2002034852A1/en active Application Filing
- 2001-10-23 ES ES01976581T patent/ES2236315T3/es not_active Expired - Lifetime
- 2001-10-23 US US10/399,229 patent/US6844080B2/en not_active Expired - Fee Related
-
2004
- 2004-12-03 US US11/003,959 patent/US7267886B2/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
US7189463B2 (en) | 2007-03-13 |
US7267886B2 (en) | 2007-09-11 |
US20050154160A1 (en) | 2005-07-14 |
EP1201722A1 (de) | 2002-05-02 |
US20040068067A1 (en) | 2004-04-08 |
ES2236315T3 (es) | 2005-07-16 |
DE60109188T2 (de) | 2006-04-06 |
IE20010937A1 (en) | 2003-04-16 |
AU2001295845A1 (en) | 2002-05-06 |
AU2002210857A1 (en) | 2002-05-06 |
US6844080B2 (en) | 2005-01-18 |
IE20010980A1 (en) | 2003-04-02 |
US20040097673A1 (en) | 2004-05-20 |
WO2002034851A1 (en) | 2002-05-02 |
EP1328597B1 (de) | 2005-03-02 |
EP1328597A1 (de) | 2003-07-23 |
ATE290054T1 (de) | 2005-03-15 |
WO2002034852A1 (en) | 2002-05-02 |
PT1328597E (pt) | 2005-06-30 |
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