AU2002210857A1 - Metal alkyl borohydride polymerisation initiators, polymerisable compositions, and uses thereof - Google Patents
Metal alkyl borohydride polymerisation initiators, polymerisable compositions, and uses thereofInfo
- Publication number
- AU2002210857A1 AU2002210857A1 AU2002210857A AU1085702A AU2002210857A1 AU 2002210857 A1 AU2002210857 A1 AU 2002210857A1 AU 2002210857 A AU2002210857 A AU 2002210857A AU 1085702 A AU1085702 A AU 1085702A AU 2002210857 A1 AU2002210857 A1 AU 2002210857A1
- Authority
- AU
- Australia
- Prior art keywords
- lithium
- alkyl
- butylborohydride
- sec
- metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F4/00—Polymerisation catalysts
- C08F4/42—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors
- C08F4/44—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides
- C08F4/52—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides selected from boron, aluminium, gallium, indium, thallium or rare earths
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J4/00—Adhesives based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; adhesives, based on monomers of macromolecular compounds of groups C09J183/00 - C09J183/16
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31855—Of addition polymer from unsaturated monomers
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31855—Of addition polymer from unsaturated monomers
- Y10T428/31909—Next to second addition polymer from unsaturated monomers
- Y10T428/31928—Ester, halide or nitrile of addition polymer
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31855—Of addition polymer from unsaturated monomers
- Y10T428/31935—Ester, halide or nitrile of addition polymer
Abstract
Metal alkyl borohydrides are used as initiators of polymerisation, particularly in adhesive compositions for bonding a wide range of substrates including low surface energy substrates such as polyolefins. As described, the metal alkyl borohydrides are of the formula I <CHEM> wherein R<1> is C1 - C10 alkyl, R<2>, R<3> and R<4>, which may be the same or different, are H, D, C1 - C10 alkyl or C1 - C10 cycloalkyl, phenyl, or phenyl-substituted C1 - C10 alkyl or C1 - C10 cycloalkyl, provided that any two of R<1> - R<4> may optionally be part of a carbocyclic ring, and M+ is a metal ion. In particular, alkali metal trialkyl borohydrides are used, the alkali metal salt being selected from the group consisting of: Lithium triethylborohydride, Sodium triethylborohydride, Potassium triethylborohydride, Lithium tri-sec-butylborohydride, Sodium tri-sec-butylborohydride, Potassium tri-sec-butylborohydride, Lithium 9-borabicyclo Ä3.3.1Ü-nonane (9BBN) hydride, Lithium thexylborohydride, Lithium trisiamylborohydride, Potassium trisiamylborohydride and Lithium triethylborodeuteride. A polymerisable composition, particularly a two part adhesive composition. comprises: a) a free-radically polymerisable monomer component, and b) an effective amount of an initiator system for initiating polymerisation of the free-radically polymerisable monomer, said initiator system comprising a metal alkyl borohydride.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP00650166 | 2000-10-23 | ||
EP00650166A EP1201722A1 (en) | 2000-10-23 | 2000-10-23 | Polymerisation initiators, polymerisable compositions, and uses thereof |
PCT/IE2001/000134 WO2002034852A1 (en) | 2000-10-23 | 2001-10-23 | Metal alkyl borohydride polymerisation initiators, polymerisable compositions, and uses thereof |
Publications (1)
Publication Number | Publication Date |
---|---|
AU2002210857A1 true AU2002210857A1 (en) | 2002-05-06 |
Family
ID=8174477
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AU2002210857A Abandoned AU2002210857A1 (en) | 2000-10-23 | 2001-10-23 | Metal alkyl borohydride polymerisation initiators, polymerisable compositions, and uses thereof |
AU2001295845A Abandoned AU2001295845A1 (en) | 2000-10-23 | 2001-10-23 | Quaternary boron compound polymerisation initiators, polymerisable compositions,and uses thereof for bonding low surface energy substrates |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AU2001295845A Abandoned AU2001295845A1 (en) | 2000-10-23 | 2001-10-23 | Quaternary boron compound polymerisation initiators, polymerisable compositions,and uses thereof for bonding low surface energy substrates |
Country Status (8)
Country | Link |
---|---|
US (3) | US7189463B2 (en) |
EP (2) | EP1201722A1 (en) |
AT (1) | ATE290054T1 (en) |
AU (2) | AU2002210857A1 (en) |
DE (1) | DE60109188T2 (en) |
ES (1) | ES2236315T3 (en) |
PT (1) | PT1328597E (en) |
WO (2) | WO2002034851A1 (en) |
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EP1201722A1 (en) * | 2000-10-23 | 2002-05-02 | Loctite (R & D) Limited | Polymerisation initiators, polymerisable compositions, and uses thereof |
WO2003089536A2 (en) * | 2002-04-19 | 2003-10-30 | Loctite (R & D) Limited | Polymerisation initiators based on ammonium tetraalkyl boranes, polymerisable compositions, and uses thereof for bonding low surface energy substrates |
US7166651B2 (en) * | 2003-05-19 | 2007-01-23 | Kerr Corporation | Two-part self-adhering dental compositions |
EP1648944A1 (en) * | 2003-06-09 | 2006-04-26 | The Dow Global Technologies Inc. | Stabilized organoborane polymerization initiators and polymerizable compositions |
WO2005017006A1 (en) | 2003-08-13 | 2005-02-24 | Dow Global Technologies Inc. | Method for joining piping systems and piping to equipment, fixtures, devices, structures, and appliances |
GB0326286D0 (en) | 2003-11-11 | 2003-12-17 | Vantico Gmbh | Initiator systems for polymerisable compositions |
KR20060118559A (en) | 2003-12-22 | 2006-11-23 | 다우 글로벌 테크놀로지스 인크. | Accelerated organoborane amine complex initiated polymerizable compositions |
US8501886B2 (en) * | 2003-12-22 | 2013-08-06 | Dow Global Technologies Llc | Accelerated organoborane amine complex initiated polymerizable compositions |
WO2005074060A1 (en) * | 2004-01-22 | 2005-08-11 | Henkel Corporation | Polymerizable compositions for bonding and sealing low surface energy substrates for fuel cells |
US8202932B2 (en) | 2004-12-03 | 2012-06-19 | Loctite (R&D) Limited | Adhesive bonding systems having adherence to low energy surfaces |
US7408012B1 (en) | 2005-04-18 | 2008-08-05 | Loctite (R&D) Limited | Adhesive bonding systems having adherence to low energy surfaces |
US7737241B2 (en) | 2005-10-07 | 2010-06-15 | Dow Global Technologies Inc. | Amido-organoborate initiator systems |
DE102005049681B4 (en) * | 2005-10-14 | 2011-03-10 | Henkel Ag & Co. Kgaa | Sleeve-shaped labels |
US7524907B2 (en) * | 2006-10-12 | 2009-04-28 | Dow Global Technologies, Inc. | Accelerated organoborane initiated polymerizable compositions |
US20080103274A1 (en) * | 2006-10-12 | 2008-05-01 | Jialanella Gary L | Accelerated organoborane initiated polymerizable compositions |
US8198343B2 (en) * | 2007-04-25 | 2012-06-12 | Dentsply International Inc. | Self-adhesive dental cement |
US8742050B2 (en) | 2008-03-28 | 2014-06-03 | Henkel US IP LLC | Two part hybrid adhesive |
WO2010025086A1 (en) * | 2008-08-29 | 2010-03-04 | Dow Global Technologies Inc. | Adhesive for bonding to flexible polymer surfaces |
US7825202B2 (en) * | 2008-10-09 | 2010-11-02 | The Goodyear Tire & Rubber Company | Potassium based catalyst systems for synthesizing rubbery polymers |
CN102203984A (en) * | 2008-11-04 | 2011-09-28 | 加州理工学院 | Hybrid electrochemical generator with a soluble anode |
GB2491170B (en) | 2011-05-26 | 2013-11-06 | Henkel Ireland Ltd | Two-part polymerisable compositions |
GB2497114B (en) * | 2011-12-01 | 2015-02-18 | Spinnaker Int Ltd | Adhesive composition |
US9018326B2 (en) | 2012-04-06 | 2015-04-28 | Ips Corporation | Adhesive composition for bonding low surface energy polyolefin substrates |
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WO2015148319A1 (en) | 2014-03-27 | 2015-10-01 | 3M Innovative Properties Company | Organoborane-containing compositions, and methods of using same |
EP3103847A1 (en) | 2015-06-10 | 2016-12-14 | Sika Technology AG | Connection of joining strips |
GB201709352D0 (en) | 2017-06-13 | 2017-07-26 | Henkel IP & Holding GmbH | Activating surfaces for subsequent bonding |
US11787911B2 (en) | 2017-06-13 | 2023-10-17 | Henkel Ag & Co. Kgaa | Activating surfaces for subsequent bonding |
GB2579608B (en) | 2018-12-06 | 2023-02-15 | Henkel Ag & Co Kgaa | Activating surfaces for subsequent bonding to another substrate |
GB2580162B (en) | 2018-12-21 | 2022-07-13 | Henkel IP & Holding GmbH | One-part photocurable (meth) acrylate compositions |
GB2583920B (en) | 2019-05-10 | 2023-09-27 | Henkel Ag & Co Kgaa | Method for bonding three-dimensional articles made by additive manufacturing |
FR3098815B1 (en) * | 2019-07-18 | 2021-06-25 | Bostik Sa | Polymerization process with a borane-amine complex |
GB2593752B (en) | 2020-04-01 | 2023-06-14 | Henkel Ag & Co Kgaa | Anaerobically curable compositions |
GB2593754B (en) | 2020-04-01 | 2022-12-28 | Henkel Ag & Co Kgaa | Redox curable compositions and methods of manufacture thereof |
GB2606002B (en) | 2021-04-21 | 2023-06-14 | Henkel Ag & Co Kgaa | Anaerobically curable compositions |
GB2622079A (en) | 2022-09-01 | 2024-03-06 | Henkel Ag & Co Kgaa | Anaerobically curable compositions |
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-
2000
- 2000-10-23 EP EP00650166A patent/EP1201722A1/en not_active Withdrawn
-
2001
- 2001-10-23 PT PT01976581T patent/PT1328597E/en unknown
- 2001-10-23 WO PCT/IE2001/000133 patent/WO2002034851A1/en active IP Right Grant
- 2001-10-23 US US10/399,230 patent/US7189463B2/en not_active Expired - Fee Related
- 2001-10-23 DE DE60109188T patent/DE60109188T2/en not_active Expired - Lifetime
- 2001-10-23 ES ES01976581T patent/ES2236315T3/en not_active Expired - Lifetime
- 2001-10-23 AU AU2002210857A patent/AU2002210857A1/en not_active Abandoned
- 2001-10-23 EP EP01976581A patent/EP1328597B1/en not_active Expired - Lifetime
- 2001-10-23 US US10/399,229 patent/US6844080B2/en not_active Expired - Fee Related
- 2001-10-23 AU AU2001295845A patent/AU2001295845A1/en not_active Abandoned
- 2001-10-23 AT AT01976581T patent/ATE290054T1/en not_active IP Right Cessation
- 2001-10-23 WO PCT/IE2001/000134 patent/WO2002034852A1/en active Application Filing
-
2004
- 2004-12-03 US US11/003,959 patent/US7267886B2/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
US20040068067A1 (en) | 2004-04-08 |
AU2001295845A1 (en) | 2002-05-06 |
IE20010980A1 (en) | 2003-04-02 |
IE20010937A1 (en) | 2003-04-16 |
US7267886B2 (en) | 2007-09-11 |
ES2236315T3 (en) | 2005-07-16 |
US6844080B2 (en) | 2005-01-18 |
WO2002034851A1 (en) | 2002-05-02 |
EP1328597B1 (en) | 2005-03-02 |
DE60109188D1 (en) | 2005-04-07 |
ATE290054T1 (en) | 2005-03-15 |
EP1201722A1 (en) | 2002-05-02 |
PT1328597E (en) | 2005-06-30 |
US20050154160A1 (en) | 2005-07-14 |
US20040097673A1 (en) | 2004-05-20 |
US7189463B2 (en) | 2007-03-13 |
EP1328597A1 (en) | 2003-07-23 |
DE60109188T2 (en) | 2006-04-06 |
WO2002034852A1 (en) | 2002-05-02 |
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