DE60104758D1 - Kontinuierliches Hydrosilylierungsverfahren zur Herstellung einer modifizierten flüssigen Organosiliconverbindung - Google Patents

Kontinuierliches Hydrosilylierungsverfahren zur Herstellung einer modifizierten flüssigen Organosiliconverbindung

Info

Publication number
DE60104758D1
DE60104758D1 DE60104758T DE60104758T DE60104758D1 DE 60104758 D1 DE60104758 D1 DE 60104758D1 DE 60104758 T DE60104758 T DE 60104758T DE 60104758 T DE60104758 T DE 60104758T DE 60104758 D1 DE60104758 D1 DE 60104758D1
Authority
DE
Germany
Prior art keywords
produce
organosilicon compound
modified liquid
liquid organosilicon
hydrosilylation process
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60104758T
Other languages
English (en)
Other versions
DE60104758T2 (de
Inventor
Toshio Okuyama
Naoya Matsui
Takao Takemasa
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
DuPont Toray Specialty Materials KK
Original Assignee
Dow Corning Toray Silicone Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Corning Toray Silicone Co Ltd filed Critical Dow Corning Toray Silicone Co Ltd
Application granted granted Critical
Publication of DE60104758D1 publication Critical patent/DE60104758D1/de
Publication of DE60104758T2 publication Critical patent/DE60104758T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/06—Preparatory processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1862—Stationary reactors having moving elements inside placed in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/20—Stationary reactors having moving elements inside in the form of helices, e.g. screw reactors
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
    • C08L83/04—Polysiloxanes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094—Jackets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761—Details of the reactor
    • B01J2219/00763—Baffles
    • B01J2219/00779—Baffles attached to the stirring means
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18—Details relating to the spatial orientation of the reactor
    • B01J2219/182—Details relating to the spatial orientation of the reactor horizontal
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/12—Polysiloxanes containing silicon bound to hydrogen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/20—Polysiloxanes containing silicon bound to unsaturated aliphatic groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Silicon Polymers (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
DE60104758T 2000-04-13 2001-04-05 Kontinuierliches Hydrosilylierungsverfahren zur Herstellung einer modifizierten flüssigen Organosiliconverbindung Expired - Lifetime DE60104758T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2000112462 2000-04-13
JP2000112462A JP4488582B2 (ja) 2000-04-13 2000-04-13 連続的ヒドロシリル化反応方法、変性された液状有機珪素化合物の連続的製造方法および連続的ヒドロシリル化反応装置

Publications (2)

Publication Number Publication Date
DE60104758D1 true DE60104758D1 (de) 2004-09-16
DE60104758T2 DE60104758T2 (de) 2005-08-25

Family

ID=18624627

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60104758T Expired - Lifetime DE60104758T2 (de) 2000-04-13 2001-04-05 Kontinuierliches Hydrosilylierungsverfahren zur Herstellung einer modifizierten flüssigen Organosiliconverbindung

Country Status (6)

Country Link
US (1) US6410772B2 (de)
EP (1) EP1146064B1 (de)
JP (1) JP4488582B2 (de)
KR (1) KR100698795B1 (de)
CN (1) CN1185237C (de)
DE (1) DE60104758T2 (de)

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US6593436B2 (en) * 2000-11-29 2003-07-15 Crompton Corporation Continuous manufacture of silicone copolymers via static mixing plug flow reactors
JP3530938B2 (ja) * 2001-03-27 2004-05-24 独立行政法人産業技術総合研究所 シルセスキオキサン系ポリマーを含む耐熱性樹脂組成物、該組成物を用いて形成された被膜、及びその被膜の作成方法
JP3786185B2 (ja) * 2001-06-22 2006-06-14 信越化学工業株式会社 固体高分子型燃料電池セパレータシール用ゴム組成物及びこれを用いたシール材並びに固体高分子型燃料電池セパレータ
GB0118858D0 (en) * 2001-08-02 2001-09-26 Dow Corning Hydrosilylation process
US6770708B2 (en) * 2002-08-27 2004-08-03 Dow Corning Corporation Silicone elastomers compositions
US6897280B2 (en) * 2002-09-23 2005-05-24 General Electric Company Continuous manufacture of silicone copolymers via multi-stage blade-mixed plug flow tubular reactor
JP2006307014A (ja) * 2005-04-28 2006-11-09 Kaneka Corp 反応性ケイ素基含有ポリエーテルの製造方法
DE102005029169A1 (de) * 2005-06-23 2006-12-28 Wacker Chemie Ag Kontinuierliche polymeranaloge Umsetzung von reaktiven Silanmonomeren mit funktionalisierten Polymeren
WO2007127004A1 (en) 2006-03-31 2007-11-08 Dow Corning Corporation Process for preparing silicone polyethers
JP5629057B2 (ja) 2006-05-19 2014-11-19 東レ・ダウコーニング株式会社 ポリエーテル変性オルガノポリシロキサン、ジオルガノポリシロキサン・ポリエーテルブロックコポリマー、それらの製造方法および化粧料
US7259220B1 (en) * 2006-07-13 2007-08-21 General Electric Company Selective hydrosilylation method
US20080033136A1 (en) * 2006-07-13 2008-02-07 Rinard Chauncey J Selective hydrosilylation conditions
DE102007023762A1 (de) * 2006-08-10 2008-02-14 Evonik Degussa Gmbh Anlage und Verfahren zur kontinuierlichen industriellen Herstellung von 3-Glycidyloxypropylalkoxysilanen
DE102006038476B4 (de) * 2006-08-17 2010-05-20 Itn Nanovation Ag Kontinuierlich arbeitender Autoklav
US7906581B2 (en) * 2007-09-05 2011-03-15 Xerox Corporation Method, apparatus and system for preparing adhesive-promoter-treated hot melt adhesives in continuous mode
KR20100115765A (ko) 2008-01-15 2010-10-28 다우 코닝 도레이 캄파니 리미티드 메타아크릴옥시기 또는 아크릴옥시기 함유 폴리오가노실록산 및 이의 제조 방법
JP5530429B2 (ja) * 2008-07-01 2014-06-25 モメンティブ パフォーマンス マテリアルズ インコーポレイテッド 気体状の不飽和炭化水素のハイドロシリレーションプロセス
JP5583906B2 (ja) 2008-12-22 2014-09-03 東レ・ダウコーニング株式会社 部分炭化水素基封鎖（ポリ）グリセロール変性ポリシロキサン、その製造方法、及び、当該ポリシロキサンを含む化粧料
JP5430142B2 (ja) 2008-12-22 2014-02-26 東レ・ダウコーニング株式会社 乳化物の製造方法
EP2360205A1 (de) 2010-02-19 2011-08-24 BYK-Chemie GmbH Verfahren zur kontinuierlichen Hydrosilylierung
GB2507488A (en) * 2012-10-30 2014-05-07 Ashe Morris Ltd Rotating flow reactor with extended flow path
GB2507487A (en) * 2012-10-30 2014-05-07 Ashe Morris Ltd Rotating flow reactor
EP3473328A1 (de) * 2014-03-25 2019-04-24 Dow Silicones Corporation Verfahren zur abtrennung von flüchtigem siloxan aus flüssigen feedmischungen
JP6538726B2 (ja) * 2014-06-11 2019-07-03 ダウ シリコーンズ コーポレーション 気体及び液体を反応させる膜接触器を使用して有機ケイ素生成物を生成する方法
JP6327426B2 (ja) * 2014-08-12 2018-05-23 国立大学法人九州大学 ヒドロシリル化反応触媒
CN107129563A (zh) * 2017-03-29 2017-09-05 张燕妮 一种长链烷基改性硅油的连续管式制备方法
JP7180315B2 (ja) * 2018-07-02 2022-11-30 信越化学工業株式会社 カルビノール変性オルガノシロキサンの製造方法
CN110898785A (zh) * 2019-11-29 2020-03-24 湖北新海鸿化工有限公司 一种201甲基硅油的连续生产工艺及装置
CN113801328B (zh) * 2021-09-13 2022-10-11 江西蓝星星火有机硅有限公司 一种利用活性炭纤维固载贵金属催化剂进行硅氢加成反应的方法

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DE2705563C2 (de) * 1977-02-10 1982-10-14 Bayer Ag, 5090 Leverkusen Verfahren zur kontinuierlichen Herstellung von hochviskosen Polydiorganosiloxanen
DE2851456C2 (de) * 1978-11-28 1982-09-23 Wacker-Chemie GmbH, 8000 München Verfahren zur Herstellung von Organosiliciumverbindungen
AU5900880A (en) * 1979-06-18 1981-01-08 General Electric Company Continuous manufacture of siloxane polymers
DE3138236A1 (de) * 1981-09-25 1983-04-07 Wacker-Chemie GmbH, 8000 München "verfahren zur herstellung von tetrafluorethyloxyalkylsilanen"
DE3519411A1 (de) * 1985-05-30 1986-12-04 Wacker-Chemie GmbH, 8000 München Kontinuierliches verfahren zur aenderung des molekulargewichts von organosiliciumverbindungen
US4898961A (en) * 1989-07-17 1990-02-06 Dow Corning Corporation Method for preparing alkenylsilanes
JP2511342B2 (ja) * 1991-04-22 1996-06-26 東レ・ダウコーニング・シリコーン株式会社 複合成形用液状シリコ―ンゴム組成物
US5986022A (en) * 1998-04-01 1999-11-16 Witco Corporation Continuous manufacture of silicone coploymers
DE19816921A1 (de) * 1998-04-16 1999-10-21 Wacker Chemie Gmbh Verfahren für kontinuierliche polymeranaloge Umsetzungen
GB9818541D0 (en) * 1998-08-26 1998-10-21 Dow Corning Continuous process for producing a silicone polymer
US6015920A (en) * 1998-09-11 2000-01-18 Ck Witco Corporation Hydrosilation reaction process with recycle

Also Published As

Publication number Publication date
CN1185237C (zh) 2005-01-19
EP1146064A3 (de) 2003-06-04
EP1146064B1 (de) 2004-08-11
EP1146064A2 (de) 2001-10-17
US20010043893A1 (en) 2001-11-22
DE60104758T2 (de) 2005-08-25
CN1318545A (zh) 2001-10-24
KR20010098531A (ko) 2001-11-08
KR100698795B1 (ko) 2007-03-26
US6410772B2 (en) 2002-06-25
JP2001294666A (ja) 2001-10-23
JP4488582B2 (ja) 2010-06-23

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