DE589511C - Process for the preparation of wetting agents, cleaning agents and dispersants - Google Patents

Process for the preparation of wetting agents, cleaning agents and dispersants

Info

Publication number
DE589511C
DE589511C DEI46724D DEI0046724D DE589511C DE 589511 C DE589511 C DE 589511C DE I46724 D DEI46724 D DE I46724D DE I0046724 D DEI0046724 D DE I0046724D DE 589511 C DE589511 C DE 589511C
Authority
DE
Germany
Prior art keywords
agents
dispersants
cleaning
preparation
wetting
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DEI46724D
Other languages
German (de)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IG Farbenindustrie AG
Original Assignee
IG Farbenindustrie AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by IG Farbenindustrie AG filed Critical IG Farbenindustrie AG
Priority to DEI46724D priority Critical patent/DE589511C/en
Application granted granted Critical
Publication of DE589511C publication Critical patent/DE589511C/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)

Description

Verfahren zur Darstellung von Netz-, Reinigungs- und Dispergiermitteln In dem Hauptpatent 577 428 ist ein Verfahren zur Herstellung von Netz-, Reinigungs-und Dispergiermitteln beschrieben, bei dem die nach Patent 524 354 durch unvollständige Oxydation von Kohlenwasserstoffen erhaltenen Kondensationsprodukte mit konzentrierter Schwefelsäure sulfoniert werden.Process for the preparation of wetting, cleaning and dispersing agents In the main patent 577 428 is a method for the production of network, cleaning and Dispersants described in which the patent 524 354 by incomplete Oxidation of hydrocarbons obtained with concentrated condensation products Sulfuric acid are sulfonated.

Es wurde nun gefunden, daß man ebenfalls vorzügliche Netz-, Reinigungs- und Dispergiermittel erhält, wenn man die nach Patent 524 354 gewonnenen Oxydationsprodukte mit anderen sulfonierend wirkenden Mitteln als konzentrierter Schwefelsäure behandelt. Die Sulfonierung verläuft sehr glatt und liefert in Wasser leicht lösliche Produkte von vorzüglichem Netz-, Reinigungs- und Dispergiervermögen.It has now been found that excellent network, cleaning and dispersants are obtained by using the oxidation products obtained in accordance with patent 524,354 treated with other sulfonating agents than concentrated sulfuric acid. The sulfonation proceeds very smoothly and produces products that are easily soluble in water of excellent wetting, cleaning and dispersing properties.

Beispiel Ein durch unvollständige Oxydation von Paraffinöl oder Hartparaffin erhaltenes Pro-Bukt wird durch Extraktion mit Methylalkohol vom unangegriffenen Ausgangsmaterial befreit und mit einem Drittel seiner Gewichtsmenge an 3o°/oigem Oleum bei 30° 2 Stunden lang verrührt. Hierauf wird noch vorhandene überschüssige Säure unter Kühlen durch Auswaschen mit Natriumsulfatlösung entfernt. Das Produkt, das mit alkalischen Mitteln neutralisiert wird, zeigt ausgezeichnete Netz-, Reinigungs- und Dispergiereigenschaften. Statt des Oleums können auch entsprechende Mengen Chlorsulfonsäure verwendet werden.Example one due to incomplete oxidation of paraffin oil or hard paraffin Pro-Bukt obtained is unaffected by extraction with methyl alcohol Starting material freed and with a third of its weight of 30% Stirred oleum at 30 ° for 2 hours. Thereupon still existing excess Acid removed by washing with sodium sulfate solution while cooling. The product, which is neutralized with alkaline agents shows excellent wetting, cleaning properties and dispersing properties. Corresponding amounts of chlorosulfonic acid can also be used instead of the oleum be used.

Claims (1)

PATENTANSPRUCH: Weiterbildung des Verfahrens des Hauptpatents 577 428 zur Herstellung von Netz-, Reinigungs- und Dispergiermitteln, dadurch gekennzeichnet, daß man andere sulfonierende Mittel verwendet. PATENT CLAIM: Further development of the process of main patent 577 428 for the production of wetting, cleaning and dispersing agents, characterized in that other sulfonating agents are used.
DEI46724D 1928-01-02 1928-01-02 Process for the preparation of wetting agents, cleaning agents and dispersants Expired DE589511C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DEI46724D DE589511C (en) 1928-01-02 1928-01-02 Process for the preparation of wetting agents, cleaning agents and dispersants

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEI46724D DE589511C (en) 1928-01-02 1928-01-02 Process for the preparation of wetting agents, cleaning agents and dispersants

Publications (1)

Publication Number Publication Date
DE589511C true DE589511C (en) 1933-12-08

Family

ID=7191817

Family Applications (1)

Application Number Title Priority Date Filing Date
DEI46724D Expired DE589511C (en) 1928-01-02 1928-01-02 Process for the preparation of wetting agents, cleaning agents and dispersants

Country Status (1)

Country Link
DE (1) DE589511C (en)

Similar Documents

Publication Publication Date Title
DE589511C (en) Process for the preparation of wetting agents, cleaning agents and dispersants
DE550572C (en) Process for the production of ethionic acid or carbyl sulfate and their homologues
DE705179C (en) Process for the manufacture of sulphonation products
DE540218C (en) Process for the decomposition of the emulsions formed during fat splitting
DE931768C (en) Process for the production of detergents and wetting agents through the action of ethylene oxide on non-uniform technical mixtures of oxaethylatable substances
DE566453C (en) Process for the production of wetting agents, detergents, dispersants, plasticizers and the like. like
DE454458C (en) Process for the production of monomolecular aliphatic sulfuric acid compounds in addition to polymeric sulfuric acid compounds
DE539625C (en) Process for the production of water-soluble products from wool fatty acids
DE644131C (en) Process for the production of sulfonated condensation products from higher molecular weight fatty acid esters and aromatic hydrocarbons
DE630679C (en) Process for the production of emulsifying, cleaning, wetting agents u. like
DE514080C (en) Process for the preparation of agents for increasing the wetting and emulsifying capacity of aqueous solutions
DE531296C (en) Process for the production of water-soluble, in acidic and alkaline solutions soluble products from wool fatty acids
DE717384C (en) Process for the production of sulfonated fatty acids or their derivatives
DE478332C (en) Process for the preparation of aromatic sulphonic acids
DE691229C (en) Process for the preparation of water-soluble sulfonated phosphatides
DE555311C (en) Process for the production of wetting and emulsifying agents
DE428789C (en) Thicken thin sulfuric acid
DE550780C (en) Process for preserving solutions and jellies of organic colloid substances
DE604255C (en) Process for the production of capillary-active sulfonation products from uncleaved waxes
DE573719C (en) Process for carrying out reactions with elimination of water
DE631910C (en) Process for the production of water-soluble oils which are not or only very slightly split from fatty acid esters containing more solidifying fatty acids
DE764950C (en) Process for the manufacture of sulphonation products
DE456855C (en) Process for the production of sulphonic acids from naphtha distillates
AT160550B (en) Process for the manufacture of detergents.
DE577428C (en) Process for the production of wetting, cleaning and dispersing agents