DE498138C - Process for the preparation of a dry fertilizer - Google Patents

Process for the preparation of a dry fertilizer

Info

Publication number
DE498138C
DE498138C DEK105995D DEK0105995D DE498138C DE 498138 C DE498138 C DE 498138C DE K105995 D DEK105995 D DE K105995D DE K0105995 D DEK0105995 D DE K0105995D DE 498138 C DE498138 C DE 498138C
Authority
DE
Germany
Prior art keywords
dry fertilizer
preparation
act
fine
temperatures
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DEK105995D
Other languages
German (de)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
WLADIMIR KYBER DIPL ING
Original Assignee
WLADIMIR KYBER DIPL ING
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by WLADIMIR KYBER DIPL ING filed Critical WLADIMIR KYBER DIPL ING
Priority to DEK105995D priority Critical patent/DE498138C/en
Application granted granted Critical
Publication of DE498138C publication Critical patent/DE498138C/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05B—PHOSPHATIC FERTILISERS
    • C05B1/00—Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
    • C05B1/04—Double-superphosphate; Triple-superphosphate; Other fertilisers based essentially on monocalcium phosphate

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Fertilizers (AREA)

Description

Verfahren zur Darstellung eines trockenen Düngemittels Es ist bekannt, Phosphorsäure mit Salzen in wässeriger Lösung zu kuppeln.Method of preparing a dry fertilizer It is known Coupling phosphoric acid with salts in aqueous solution.

Demgegenüber wurde gefunden, daß, wenn man nebelförmige Phosphorsäuren bei der hierbei notwendigen Menge Wasserdampf in einem geeigneten Apparat (Turm oder drehbare Trommel) auf sehr feinkörnige Kreide einwirken läßt und hierbei die Temperatur auf etwa iio bis 12o° C hält, folgende Umsetzungen stattfinden: CaCO3 + 2 HP03= Ca(P03)2 + H20 -f- C02 (z) Ca(PO3)2 -;- z H20 = (2) Wenn, wie beschrieben, .verfahre. wird, erhält man ein trockenes, streubares Produkt, das bis zu 6o °/o P"0, enthalten kann. Dieses Salz ist bis zu go °/o wasserlöslich rund nur ro°io davon sind citratlös.lichePhosphorsäure.On the other hand, it has been found that if nebulous phosphoric acids are allowed to act on very fine-grained chalk with the required amount of steam in a suitable apparatus (tower or rotating drum) and the temperature is kept at about 110 to 120 ° C., the following reactions take place: CaCO3 + 2 HP03 = Ca (P03) 2 + H20 -f- C02 (z) Ca (PO3) 2 -; - z H20 = (2) If, as described, proceed. a dry, scatterable product is obtained which can contain up to 60% P "0. This salt is up to 100% water-soluble, around only 100% of which are citrate-soluble phosphoric acid.

Wird die Reaktion jedoch bei .4oo bis 6oo° C durchgeführt, so geht die Umsetzung nach Reaktion i. Das so erhaltene Produkt muß nachträglich mit Wasserdampf behandelt werden, gibt dann aber ebenfalls ein gut streubares Produkt.However, if the reaction is carried out at .400 to 600 ° C., it works the implementation after reaction i. The product obtained in this way must subsequently be steamed are treated, but then also gives a product that is easy to spread.

Das Düngemittel ist leicht herstellbar und enthält keine den Boden schädigende Bestandteile.The fertilizer is easy to manufacture and does not contain the soil harmful components.

Claims (2)

PATENTANSPRÜCHE: i. Verfahren zur Darstellung eines trockenen Düngemittels, dadurch gekennzeichnet, daß man nebelförmige Phosphorsäuren bei Gegenwart von Wasserdampf und bei Temperaturen von ioo bis 1200 C auf sehr feinkörnige Kreide einwirken läßt. PATENT CLAIMS: i. Method of preparing a dry fertilizer, characterized in that mist-shaped phosphoric acids are used in the presence of water vapor and lets it act on very fine-grained chalk at temperatures of 100 to 1200 C. 2. Verfahren zur Erzeugung eines streubaren, trockenen Düngemittels, dadurch gekennzeichnet, daß man dampfförmige Phosphorsäuren bei Temperaturen von 400 bis 6oo° C auf sehr feinkörnige Kreide einwirken läßt und das erhaltene Produkt dann nachträglich mit Wasserdampf behandelt.2. A method for producing a spreadable, dry fertilizer, characterized in that that you vaporous phosphoric acids at temperatures of 400 to 6oo ° C to very Fine-grained chalk can act and the product obtained is then added later Steam treated.
DEK105995D 1927-09-22 1927-09-22 Process for the preparation of a dry fertilizer Expired DE498138C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DEK105995D DE498138C (en) 1927-09-22 1927-09-22 Process for the preparation of a dry fertilizer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEK105995D DE498138C (en) 1927-09-22 1927-09-22 Process for the preparation of a dry fertilizer

Publications (1)

Publication Number Publication Date
DE498138C true DE498138C (en) 1930-05-19

Family

ID=7240819

Family Applications (1)

Application Number Title Priority Date Filing Date
DEK105995D Expired DE498138C (en) 1927-09-22 1927-09-22 Process for the preparation of a dry fertilizer

Country Status (1)

Country Link
DE (1) DE498138C (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE742197C (en) * 1940-02-13 1943-11-24 Chem Fab Joh A Benckiser G M B Production of dry, water-soluble salts of phosphoric acids, which are lower in constitutional water than orthophosphoric acid
DE1206293B (en) * 1960-01-16 1965-12-02 Knapsack Ag Process for the production of a mineral feed consisting essentially of dicalcium phosphate
US3273960A (en) * 1961-10-17 1966-09-20 Monsanto Co Caking resistant monocalcium phosphate, monohydrate and process for its manufacture
DE2643683A1 (en) * 1975-10-10 1977-04-21 Dansk Ind Syndikat PROCESS FOR PRODUCING A POWDER OR GRANULATE, NON-DUSTING MINERAL MIXTURE

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE742197C (en) * 1940-02-13 1943-11-24 Chem Fab Joh A Benckiser G M B Production of dry, water-soluble salts of phosphoric acids, which are lower in constitutional water than orthophosphoric acid
DE1206293B (en) * 1960-01-16 1965-12-02 Knapsack Ag Process for the production of a mineral feed consisting essentially of dicalcium phosphate
US3273960A (en) * 1961-10-17 1966-09-20 Monsanto Co Caking resistant monocalcium phosphate, monohydrate and process for its manufacture
DE2643683A1 (en) * 1975-10-10 1977-04-21 Dansk Ind Syndikat PROCESS FOR PRODUCING A POWDER OR GRANULATE, NON-DUSTING MINERAL MIXTURE

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