DE3810681A1 - Verfahren zur herstellung eines natuerlichen suessungsmittels auf der basis von stevia rebaudiana und seine verwendung - Google Patents

Verfahren zur herstellung eines natuerlichen suessungsmittels auf der basis von stevia rebaudiana und seine verwendung

Info

Publication number
DE3810681A1
DE3810681A1 DE3810681A DE3810681A DE3810681A1 DE 3810681 A1 DE3810681 A1 DE 3810681A1 DE 3810681 A DE3810681 A DE 3810681A DE 3810681 A DE3810681 A DE 3810681A DE 3810681 A1 DE3810681 A1 DE 3810681A1
Authority
DE
Germany
Prior art keywords
extraction
extract
sweeteners
carbon dioxide
stevia rebaudiana
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
DE3810681A
Other languages
German (de)
English (en)
Other versions
DE3810681C2 (enExample
Inventor
Udo Kienle
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to DE3810681A priority Critical patent/DE3810681A1/de
Priority to AT89105230T priority patent/ATE143665T1/de
Priority to ES89105230T priority patent/ES2094723T3/es
Priority to DE58909739T priority patent/DE58909739D1/de
Priority to EP89105230A priority patent/EP0335265B1/de
Publication of DE3810681A1 publication Critical patent/DE3810681A1/de
Priority to US07/586,690 priority patent/US5112610A/en
Application granted granted Critical
Publication of DE3810681C2 publication Critical patent/DE3810681C2/de
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
    • C07H15/20—Carbocyclic rings
    • C07H15/24—Condensed ring systems having three or more rings
    • C07H15/256—Polyterpene radicals
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
    • A23L27/11—Natural spices, flavouring agents or condiments; Extracts thereof obtained by solvent extraction
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/30—Artificial sweetening agents
    • A23L27/33—Artificial sweetening agents containing sugars or derivatives
    • A23L27/36—Terpene glycosides
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Nutrition Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Seasonings (AREA)
  • Medicinal Preparation (AREA)
  • Saccharide Compounds (AREA)
DE3810681A 1988-03-29 1988-03-29 Verfahren zur herstellung eines natuerlichen suessungsmittels auf der basis von stevia rebaudiana und seine verwendung Granted DE3810681A1 (de)

Priority Applications (6)

Application Number Priority Date Filing Date Title
DE3810681A DE3810681A1 (de) 1988-03-29 1988-03-29 Verfahren zur herstellung eines natuerlichen suessungsmittels auf der basis von stevia rebaudiana und seine verwendung
AT89105230T ATE143665T1 (de) 1988-03-29 1989-03-23 Verfahren zur herstellung eines natürlichen süssungsmittels auf der basis von stevia rebaudiana
ES89105230T ES2094723T3 (es) 1988-03-29 1989-03-23 Procedimiento de fabricacion y utilizacion del edulcorante natural con estevia rebaudiana.
DE58909739T DE58909739D1 (de) 1988-03-29 1989-03-23 Verfahren zur Herstellung eines natürlichen Süssungsmittels auf der Basis von Stevia rebaudiana
EP89105230A EP0335265B1 (de) 1988-03-29 1989-03-23 Verfahren zur Herstellung eines natürlichen Süssungsmittels auf der Basis von Stevia rebaudiana
US07/586,690 US5112610A (en) 1988-03-29 1990-09-24 Method of making a natural sweetener based on Stevia rebaudiana, and use thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE3810681A DE3810681A1 (de) 1988-03-29 1988-03-29 Verfahren zur herstellung eines natuerlichen suessungsmittels auf der basis von stevia rebaudiana und seine verwendung

Publications (2)

Publication Number Publication Date
DE3810681A1 true DE3810681A1 (de) 1989-10-12
DE3810681C2 DE3810681C2 (enExample) 1993-06-03

Family

ID=6350984

Family Applications (2)

Application Number Title Priority Date Filing Date
DE3810681A Granted DE3810681A1 (de) 1988-03-29 1988-03-29 Verfahren zur herstellung eines natuerlichen suessungsmittels auf der basis von stevia rebaudiana und seine verwendung
DE58909739T Expired - Fee Related DE58909739D1 (de) 1988-03-29 1989-03-23 Verfahren zur Herstellung eines natürlichen Süssungsmittels auf der Basis von Stevia rebaudiana

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE58909739T Expired - Fee Related DE58909739D1 (de) 1988-03-29 1989-03-23 Verfahren zur Herstellung eines natürlichen Süssungsmittels auf der Basis von Stevia rebaudiana

Country Status (5)

Country Link
US (1) US5112610A (enExample)
EP (1) EP0335265B1 (enExample)
AT (1) ATE143665T1 (enExample)
DE (2) DE3810681A1 (enExample)
ES (1) ES2094723T3 (enExample)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4342874A1 (de) * 1993-12-16 1995-06-22 Barth Raiser Hopfenextraktion Verfahren zur Entfernung von unpolaren Inhaltsstoffen aus Ginseng
US5822726A (en) * 1995-01-31 1998-10-13 Motorola, Inc. Speech presence detector based on sparse time-random signal samples
AT513907A1 (de) * 2013-02-07 2014-08-15 Natex Prozesstech Gmbh Verfahren zur Anreicherung von Wertstoffen aus einem flüssigen Rohstoff

Families Citing this family (78)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3810681A1 (de) * 1988-03-29 1989-10-12 Udo Kienle Verfahren zur herstellung eines natuerlichen suessungsmittels auf der basis von stevia rebaudiana und seine verwendung
US5120558A (en) * 1991-05-01 1992-06-09 Norac Technologies Inc. Process for the supercritical extraction and fractionation of spices
EP0675754A4 (en) * 1992-11-27 1996-01-10 Napro Biotherapeutics Inc TREATMENT OF TAXANE SOLUTS USING MEMBRANES.
US6156318A (en) * 1997-03-31 2000-12-05 Naohiko Sato Method of counteracting harmful effects of histamine
US5958419A (en) * 1997-03-31 1999-09-28 Naohiko Sato Antihistaminic substance of stevia origin
CN1078217C (zh) * 1998-02-18 2002-01-23 南开大学 吸附树脂法从甜菊糖中富集、分离菜鲍迪甙a
US6811793B2 (en) 2002-03-11 2004-11-02 Amerilab Technologies, Inc. Effervescent composition including stevia
US7507396B2 (en) * 2003-10-17 2009-03-24 Amerilab Technologies, Inc. Effervescent composition and method of making an effervescent composition including a viscous component
US9107436B2 (en) 2011-02-17 2015-08-18 Purecircle Sdn Bhd Glucosylated steviol glycoside as a flavor modifier
US9392799B2 (en) 2011-02-17 2016-07-19 Purecircle Sdn Bhd Glucosyl stevia composition
US9386797B2 (en) 2011-02-17 2016-07-12 Purecircle Sdn Bhd Glucosyl stevia composition
US8790730B2 (en) 2005-10-11 2014-07-29 Purecircle Usa Process for manufacturing a sweetener and use thereof
US8337927B2 (en) * 2005-10-11 2012-12-25 Purecircle Sdn Bhd Process for manufacturing a sweetener and use thereof
US8318459B2 (en) 2011-02-17 2012-11-27 Purecircle Usa Glucosyl stevia composition
US8257948B1 (en) 2011-02-17 2012-09-04 Purecircle Usa Method of preparing alpha-glucosyl Stevia composition
US8334006B2 (en) * 2005-10-11 2012-12-18 Purecircle Sdn Bhd Process for manufacturing a sweetener and use thereof
US9101160B2 (en) 2005-11-23 2015-08-11 The Coca-Cola Company Condiments with high-potency sweetener
US8791253B2 (en) * 2006-06-19 2014-07-29 The Coca-Cola Company Rebaudioside A composition and method for purifying rebaudioside A
US9012626B2 (en) * 2006-06-19 2015-04-21 The Coca-Cola Company Rebaudioside a composition and method for purifying rebaudioside a
US8017168B2 (en) 2006-11-02 2011-09-13 The Coca-Cola Company High-potency sweetener composition with rubisco protein, rubiscolin, rubiscolin derivatives, ace inhibitory peptides, and combinations thereof, and compositions sweetened therewith
CN101200480B (zh) * 2006-12-15 2011-03-30 成都华高药业有限公司 莱鲍迪甙a的提取方法
ATE547953T1 (de) * 2007-01-22 2012-03-15 Cargill Inc Verfahren zur herstellung gereinigter rebaudiosid-a-zusammensetzungen durch solvent/antisolvent- kristallisation
US8030481B2 (en) 2007-05-21 2011-10-04 The Coca-Cola Company Stevioside polymorphic and amorphous forms, methods for their formulation, and uses
WO2010021001A2 (en) * 2008-08-19 2010-02-25 Kaushik Ramakrishnan S Process for preparing sweetener from stevia rebaudiana
KR20120027363A (ko) * 2009-06-16 2012-03-21 이피씨 (베이징) 내추럴 프로덕츠 컴퍼니, 리미티드 뒷맛을 감소시키거나 제거하기 위한 레바우디오사이드 ｄ를 포함하는 조성물 및 그의 제조 방법
US8574656B2 (en) * 2009-10-15 2013-11-05 Purecircle Sdn Bhd High-purity Rebaudioside D and low-calorie fruit juice containing the same
US8568818B2 (en) * 2009-10-15 2013-10-29 Pure Circle Sdn Bhd High-purity Rebaudioside D and low-calorie carbonated drink containing the same
US8414950B2 (en) * 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie table top tablet containing the same
US8299224B2 (en) * 2009-10-15 2012-10-30 Purecircle Sdn Bhd High-purity Rebaudioside D
MX2012003686A (es) 2009-10-15 2012-07-25 Purecircle Sdn Bhd Rebaudiosido d de alta pureza y aplicaciones.
US8420147B2 (en) * 2009-10-15 2013-04-16 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie cake containing the same
US8414952B2 (en) * 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie diet cookies containing the same
US8414948B2 (en) * 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie ice cream containing the same
US8507022B2 (en) * 2009-10-15 2013-08-13 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie carbonated lemon-flavored beverage containing the same
US8414949B2 (en) * 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie yogurt containing the same
US8420146B2 (en) * 2009-10-15 2013-04-16 Purecircle Sdn Bhd High-purity Rebaudioside D and low-calorie bread containing the same
US8916138B2 (en) * 2009-10-15 2014-12-23 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie tooth paste composition containing the same
US8414951B2 (en) 2009-10-15 2013-04-09 Purecircle Sdn Bhd High-purity Rebaudioside D and low-calorie soy sauce containing the same
US8512790B2 (en) 2009-10-15 2013-08-20 Purecircle Sdn Bhd High-purity rebaudioside D and low-calorie chocolate containing the same
US20110111115A1 (en) * 2009-11-06 2011-05-12 Jingang Shi Rebaudioside a polymorphs and methods to prepare them
PL2498625T3 (pl) 2009-11-12 2019-07-31 Purecircle Usa Inc. Granulacja słodzika stewia
US20150344512A1 (en) 2011-12-19 2015-12-03 Purecircle Usa Inc. Methods of purifying steviol glycosides and uses of the same
EP4108668A1 (en) 2010-03-12 2022-12-28 PureCircle USA Inc. High-purity steviol glycosides
US10696706B2 (en) 2010-03-12 2020-06-30 Purecircle Usa Inc. Methods of preparing steviol glycosides and uses of the same
US20120070533A1 (en) * 2010-08-23 2012-03-22 Jingang Shi Superfine powdered stevia
US9578895B2 (en) 2010-08-23 2017-02-28 Epc (Beijing) Natural Products Co., Ltd. Rebaudioside A and stevioside compositions
MX346137B (es) 2010-12-13 2017-03-08 Purecircle Usa Inc Rebaudiosido d altamente soluble.
US9510611B2 (en) 2010-12-13 2016-12-06 Purecircle Sdn Bhd Stevia composition to improve sweetness and flavor profile
ES2385559B2 (es) * 2010-12-30 2013-04-02 Universidad De Granada Procedimiento de obtencion de steviosidos organicos a partir de stevia
MX362676B (es) 2011-02-10 2019-01-31 Purecircle Usa Composición de estevia.
US11690391B2 (en) 2011-02-17 2023-07-04 Purecircle Sdn Bhd Glucosylated steviol glycoside as a flavor modifier
US9474296B2 (en) 2011-02-17 2016-10-25 Purecircle Sdn Bhd Glucosyl stevia composition
US9603373B2 (en) 2011-02-17 2017-03-28 Purecircle Sdn Bhd Glucosyl stevia composition
US9795156B2 (en) 2011-03-17 2017-10-24 E.P.C (Beijing) Plant Pharmaceutical Technology Co., Ltd Rebaudioside B and derivatives
US9894922B2 (en) 2011-05-18 2018-02-20 Purecircle Sdn Bhd Glucosyl rebaudioside C
WO2012166163A1 (en) 2011-05-31 2012-12-06 Purecircle Usa Stevia composition
EP2713762B1 (en) 2011-06-03 2016-03-30 Purecircle USA Stevia composition
ES2713573T3 (es) 2011-06-20 2019-05-22 Purecircle Usa Inc Composición de estevia
US9771434B2 (en) 2011-06-23 2017-09-26 Purecircle Sdn Bhd Products from stevia rebaudiana
US10480019B2 (en) 2011-08-10 2019-11-19 Purecircle Sdn Bhd Process for producing high-purity rubusoside
BR112014004581B1 (pt) 2011-09-07 2020-03-17 Purecircle Usa Inc. Adoçante de stevia alta solubilidade, método de produção, pó, composições de adoçante e de sabor, ingrediente alimentar, alimento, bebida e produto cosmético ou farmacêutico do referido adoçante
EP3345490B1 (en) 2011-12-19 2023-11-08 The Coca-Cola Company Beverage comprising rebaudioside x
US9752174B2 (en) 2013-05-28 2017-09-05 Purecircle Sdn Bhd High-purity steviol glycosides
CN110358795B (zh) 2012-05-22 2024-12-03 谱赛科有限责任公司 高纯度的甜菊醇糖苷
US20140082768A1 (en) * 2012-09-17 2014-03-20 Mcneil Nutritionals, Llc. Enhanced natural sweetener
US20140079858A1 (en) * 2012-09-17 2014-03-20 Mcneil Nutritionals, Llc. Enhanced natural sweetener
DK3714699T3 (da) 2013-06-07 2025-01-20 Purecircle Usa Inc Stevia-ekstrakt indeholdende udvalgte steviolglycosider som aroma-, salt- og sødmeprofilmodifikator
US10952458B2 (en) 2013-06-07 2021-03-23 Purecircle Usa Inc Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier
US10264811B2 (en) 2014-05-19 2019-04-23 Epc Natural Products Co., Ltd. Stevia sweetener with improved solubility
US10357052B2 (en) 2014-06-16 2019-07-23 Sweet Green Fields USA LLC Rebaudioside A and stevioside with improved solubilities
US10485256B2 (en) 2014-06-20 2019-11-26 Sweet Green Fields International Co., Limited Stevia sweetener with improved solubility with a cyclodextrin
CN114794444A (zh) 2014-09-02 2022-07-29 谱赛科美国股份有限公司 富含莱鲍迪苷d、e、n和/或o的甜菊提取物及其制备方法
PL3367816T3 (pl) 2015-10-26 2024-05-06 Purecircle Usa Inc. Kompozycje glikozydów stewiolowych
WO2017106577A1 (en) 2015-12-15 2017-06-22 Purecircle Usa Inc. Steviol glycoside compositions
US10577248B2 (en) 2016-05-24 2020-03-03 Harper Biotech LLC Methods and systems for large scale carbon dioxide utilization from Lake Kivu via a CO2 industrial utilization hub integrated with electric power production and optional cryo-energy storage
CN109704966B (zh) * 2018-12-25 2021-08-20 中化健康产业发展有限公司 一种超临界萃取技术分离甜菊叶中组份的方法
CN110959863A (zh) * 2019-12-13 2020-04-07 徐明德 一种甜菊叶混合营养料糖浆及其制备方法和应用
US12446605B2 (en) 2022-03-23 2025-10-21 Sweegen, Inc. Sweeteners

Citations (3)

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Publication number Priority date Publication date Assignee Title
US4082858A (en) * 1975-06-04 1978-04-04 F. K. Suzuki International, Inc. Sweetening compound, method of recovery, and use thereof
US4219571A (en) * 1978-06-15 1980-08-26 Kabushiki Kaisha Hayashibara Seibutsu Kagaku Kenkyujo Process for producing a sweetener
JPS62496A (ja) * 1985-06-27 1987-01-06 Mitsui Petrochem Ind Ltd 配糖体の抽出方法

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AU497159B2 (en) * 1974-02-21 1978-12-07 Commonwealth Scientific And Industrial Research Organization Removing limonin from citrus fruit juice
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BE896610A (fr) * 1982-05-06 1983-08-16 Hop Developments Ltd Extraction d'une matiere vegetale en utilisant de l'anhydride carbonique
GB8327756D0 (en) * 1983-10-17 1983-11-16 Ici Plc Extraction process
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Patent Citations (3)

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Publication number Priority date Publication date Assignee Title
US4082858A (en) * 1975-06-04 1978-04-04 F. K. Suzuki International, Inc. Sweetening compound, method of recovery, and use thereof
US4219571A (en) * 1978-06-15 1980-08-26 Kabushiki Kaisha Hayashibara Seibutsu Kagaku Kenkyujo Process for producing a sweetener
JPS62496A (ja) * 1985-06-27 1987-01-06 Mitsui Petrochem Ind Ltd 配糖体の抽出方法

Non-Patent Citations (4)

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Title
"Stevioside" in Alternative Sweeteners, S. 295-307, Marcel Dekker Inc., New York, 1986 *
CA 107 : 151 504 *
Derwent 87-40955/06 *
STAHL, E. et.al.: "Verdichtete Gase zur Extraktion und Raffination", Springer-Verlag, 1987 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4342874A1 (de) * 1993-12-16 1995-06-22 Barth Raiser Hopfenextraktion Verfahren zur Entfernung von unpolaren Inhaltsstoffen aus Ginseng
US5822726A (en) * 1995-01-31 1998-10-13 Motorola, Inc. Speech presence detector based on sparse time-random signal samples
AT513907A1 (de) * 2013-02-07 2014-08-15 Natex Prozesstech Gmbh Verfahren zur Anreicherung von Wertstoffen aus einem flüssigen Rohstoff
AT513907B1 (de) * 2013-02-07 2015-01-15 Natex Prozesstech Gmbh Verfahren zur Anreicherung von Wertstoffen aus einem flüssigen Rohstoff

Also Published As

Publication number Publication date
EP0335265B1 (de) 1996-10-02
ATE143665T1 (de) 1996-10-15
EP0335265A3 (de) 1991-09-11
DE58909739D1 (de) 1996-11-07
ES2094723T3 (es) 1997-02-01
US5112610A (en) 1992-05-12
DE3810681C2 (enExample) 1993-06-03
EP0335265A2 (de) 1989-10-04

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