DE3269530D1 - A method for cleaning gas mixtures which might contain dust from a urea plant - Google Patents

A method for cleaning gas mixtures which might contain dust from a urea plant

Info

Publication number
DE3269530D1
DE3269530D1 DE8282111944T DE3269530T DE3269530D1 DE 3269530 D1 DE3269530 D1 DE 3269530D1 DE 8282111944 T DE8282111944 T DE 8282111944T DE 3269530 T DE3269530 T DE 3269530T DE 3269530 D1 DE3269530 D1 DE 3269530D1
Authority
DE
Germany
Prior art keywords
urea plant
washing solution
gas mixtures
cleaning gas
formaline
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DE8282111944T
Other languages
German (de)
Inventor
Harald Storen
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Norsk Hydro ASA
Original Assignee
Norsk Hydro ASA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Norsk Hydro ASA filed Critical Norsk Hydro ASA
Application granted granted Critical
Publication of DE3269530D1 publication Critical patent/DE3269530D1/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D47/00—Separating dispersed particles from gases, air or vapours by liquid as separating agent
    • B01D47/10—Venturi scrubbers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2247/00—Details relating to the separation of dispersed particles from gases, air or vapours by liquid as separating agent
    • B01D2247/04—Regenerating the washing fluid

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treating Waste Gases (AREA)
  • Gas Separation By Absorption (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Abstract

Gas mixtures from a urea plant, particularly such mixtures containing dust and especially off-gases from prilling towers or granulation units are cleaned. In order to prevent precipitation and accretion in the cleaning unit, there is applied an aqueous washing solution to which formaldehyde is added before it is brought in contact with the gas mixture. Formaldehyde is preferably added in the form of formaline, and the addition of formaline is regulated by pH-measurements in the washing solution such that pH is maintained at pH=6-8.5. The pH of the washing solution is preferably kept at pH=about 7, especially in order to obtain optimal removal of ammonia. The method is carried out during application of standard scrubbers in which aqueous washing solutions can be used.
DE8282111944T 1982-01-07 1982-12-23 A method for cleaning gas mixtures which might contain dust from a urea plant Expired DE3269530D1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
NO820030A NO150667C (en) 1982-01-07 1982-01-07 PROCEDURE FOR CLEANING OF GAS MIXTURES FROM UREA PRODUCTION PLANTS

Publications (1)

Publication Number Publication Date
DE3269530D1 true DE3269530D1 (en) 1986-04-03

Family

ID=19886388

Family Applications (1)

Application Number Title Priority Date Filing Date
DE8282111944T Expired DE3269530D1 (en) 1982-01-07 1982-12-23 A method for cleaning gas mixtures which might contain dust from a urea plant

Country Status (8)

Country Link
US (1) US4507129A (en)
EP (1) EP0084669B1 (en)
AT (1) ATE18202T1 (en)
BR (1) BR8300031A (en)
CA (1) CA1192381A (en)
DE (1) DE3269530D1 (en)
IN (1) IN158998B (en)
NO (1) NO150667C (en)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT1249057B (en) * 1991-05-22 1995-02-11 Agrimont Spa PROCESS FOR BLASTING AMMONIA CONTAINED IN A BREATHER WITH A LIQUID.
DK70693D0 (en) * 1993-06-14 1993-06-14 Niels Ole Vesterager PROCEDURE FOR REMOVAL OF UNUSUAL SUBSTANCES IN A GAS TYPE
FR2740355B1 (en) * 1995-10-27 1998-01-16 Cos Ingenierie PROCESS FOR AMMONIACAL DEPOLLUTION OF LIQUID OR GASEOUS EFFLUENTS
TW201032887A (en) * 2009-01-13 2010-09-16 Saipem Spa Process for the recovery of ammonia from a gaseous stream
EP2662349A1 (en) 2012-05-08 2013-11-13 Uhde Fertilizer Technology B.V. Urea granulation process with scrubbing system
AU2014284776B2 (en) * 2013-07-05 2018-01-18 Stamicarbon B.V. Removal of dust in urea finishing
CN105916838B (en) * 2013-11-15 2019-04-09 斯塔米卡邦有限公司 The method of soluble particles is removed for the device and method from gas stream arrested particles and from gas
US10913025B2 (en) 2014-12-19 2021-02-09 Stamicarbon B.V. Removal of dust in urea finishing
US10730002B2 (en) 2016-05-09 2020-08-04 Stamicarbon B.V. Submicron particle removal from gas streams
EP3652152B1 (en) 2017-07-14 2021-11-17 Stamicarbon B.V. Urea finishing and off-gas treatment plant and process
CN107185332A (en) * 2017-07-19 2017-09-22 郑金风 A kind of new and effective urea recovering-washing tower
CN107854945A (en) * 2017-12-05 2018-03-30 中国华电科工集团有限公司 A kind of flue gas purification system

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE802457C (en) * 1947-07-30 1951-02-12 Basf Ag Process for the preparation of hexamethylenetetramine
US2977386A (en) * 1955-04-08 1961-03-28 Allied Chem Absorption of formaldehyde in alkaline urea solution
DE1128849B (en) * 1959-09-14 1962-05-03 Ici Ltd Process for the production of fine-grain urea
SU504546A1 (en) * 1973-11-14 1976-02-28 Method for automatic control of the absorption process
IT1004432B (en) * 1974-03-28 1976-07-10 Snam Progetti PROCEDURE FOR THE RECOVERY OF POL VER OBTAINED FROM EQUIPMENT FOR THE TREATMENT OF QUID OR SOLID LIQUID MATERIALS
GB1493612A (en) * 1974-07-06 1977-11-30 Fisons Ltd Prilling
JPS5318466A (en) * 1976-08-05 1978-02-20 Mitsubishi Heavy Ind Ltd Charging method for oxygen-containing hydrocarbons and/or their precursors into exhaust gas
US4104041A (en) * 1976-12-08 1978-08-01 Chiyoda Chemical Engineering & Construction Co., Ltd. Apparatus and method for treating waste gas from urea prilling tower
JPS5378974A (en) * 1976-12-22 1978-07-12 Kouriyuu Kougiyou Kk Method of collecting dusts generated in sintering plant

Also Published As

Publication number Publication date
BR8300031A (en) 1983-09-13
EP0084669B1 (en) 1986-02-26
US4507129A (en) 1985-03-26
EP0084669A1 (en) 1983-08-03
ATE18202T1 (en) 1986-03-15
NO150667B (en) 1984-08-20
NO820030L (en) 1983-07-08
CA1192381A (en) 1985-08-27
NO150667C (en) 1984-11-28
IN158998B (en) 1987-03-07

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee