DE3066353D1 - A method of purifying phosphoric acid of heavy metal - Google Patents
A method of purifying phosphoric acid of heavy metalInfo
- Publication number
- DE3066353D1 DE3066353D1 DE8080850070T DE3066353T DE3066353D1 DE 3066353 D1 DE3066353 D1 DE 3066353D1 DE 8080850070 T DE8080850070 T DE 8080850070T DE 3066353 T DE3066353 T DE 3066353T DE 3066353 D1 DE3066353 D1 DE 3066353D1
- Authority
- DE
- Germany
- Prior art keywords
- phosphoric acid
- alkali
- heavy metals
- sulphide
- heavy metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/18—Phosphoric acid
- C01B25/234—Purification; Stabilisation; Concentration
- C01B25/237—Selective elimination of impurities
- C01B25/238—Cationic impurities, e.g. arsenic compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Removal Of Specific Substances (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Processing Of Solid Wastes (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE7904135A SE418845B (sv) | 1979-05-10 | 1979-05-10 | Forfarande for rening av vatprocessfosforsyra |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE3066353D1 true DE3066353D1 (en) | 1984-03-08 |
Family
ID=20338025
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE8080850070T Expired DE3066353D1 (en) | 1979-05-10 | 1980-05-08 | A method of purifying phosphoric acid of heavy metal |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US4378340A (OSRAM) |
| EP (1) | EP0023195B2 (OSRAM) |
| JP (1) | JPH021086B2 (OSRAM) |
| AT (1) | ATE6050T1 (OSRAM) |
| DE (1) | DE3066353D1 (OSRAM) |
| DK (1) | DK151216C (OSRAM) |
| FI (1) | FI66162C (OSRAM) |
| NO (1) | NO152505C (OSRAM) |
| SE (1) | SE418845B (OSRAM) |
| WO (1) | WO1980002418A1 (OSRAM) |
Families Citing this family (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3134847A1 (de) * | 1981-09-03 | 1983-03-17 | Hoechst Ag, 6000 Frankfurt | "verfahren zur gewinnung cadmium-freier rohphosphorsaeure" |
| FR2520342A1 (fr) * | 1982-01-25 | 1983-07-29 | Rhone Poulenc Chim Base | Procede de purification d'acide phosphorique de voie humide |
| DE3202658A1 (de) * | 1982-01-28 | 1983-08-04 | Hoechst Ag, 6230 Frankfurt | Verfahren zur entfernung von schwermetallionen aus nassverfahrensphosphorsaeure |
| EP0087065B1 (de) * | 1982-02-12 | 1985-09-25 | Hoechst Aktiengesellschaft | Verfahren zur Verminderung des Schwermetallgehaltes im Rohphosphat |
| DE3218599A1 (de) * | 1982-05-18 | 1983-12-01 | Chemische Fabrik Budenheim Rudolf A. Oetker, 6501 Budenheim | Verfahren zum entfernen von cadmium aus sauren, insbesondere p(pfeil abwaerts)2(pfeil abwaerts)0(pfeil abwaerts)5(pfeil abwaerts)-haltigen loesungen |
| DE3604483A1 (de) * | 1986-02-13 | 1987-08-20 | Hoechst Ag | Verfahren zum entfernen von schwermetallen aus mineralsaeuren |
| DE3604920A1 (de) * | 1986-02-17 | 1987-08-20 | Hoechst Ag | Verfahren zur herstellung von rohphosphorsaeure |
| DE3622597A1 (de) * | 1986-07-04 | 1988-01-07 | Budenheim Rud A Oetker Chemie | Verfahren zur faellung und abtrennung von cadmiumsulfid aus den raffinaten der phosphorsaeurereinigung |
| NL8601846A (nl) * | 1986-07-15 | 1988-02-01 | Stamicarbon | Werkwijze voor het verwijderen van zware metalen uit zure fosfaathoudende waterige media. |
| DE3631290A1 (de) * | 1986-09-13 | 1988-03-24 | Budenheim Rud A Oetker Chemie | Verfahren zur behandlung von nassverfahrensphosphorsaeure |
| NO164768C (no) * | 1988-03-04 | 1990-11-14 | Norsk Hydro As | Fremgangsmaate for fjerning av tungmetaller, spesielt kadmium, fra fosforsyreholdige loesninger. |
| DE4327401A1 (de) * | 1993-08-14 | 1995-02-16 | Hoechst Ag | Verfahren zur Entfernung von Blei und Cadmium aus Phosphorsäure |
| US20040179984A1 (en) * | 2003-03-13 | 2004-09-16 | Nagaraj D. R. | Process for removing metal impurities from wet process phosphoric acid and compositions thereof |
| TW200944535A (en) * | 2008-03-20 | 2009-11-01 | Sigma Aldrich Co | Purification and preparation of phosphorus-containing compounds |
| JP6099737B2 (ja) * | 2012-06-21 | 2017-03-22 | オウトテック(フィンランド)オーワイ | リン含有出発原料から重金属を分離するためのプロセス及びプラント |
| DE102014006278B3 (de) * | 2014-05-02 | 2015-02-26 | Remondis Aqua Gmbh & Co. Kg | Verfahren zur Reinigung von Roh-Phosphorsäure (z.B. MGA-Säure) durch Zugabe von Aschen aus Abfall-Verbrennungsanlagen umfassend die Gewinnung von reiner Phosphorsäure, Kalziumsulfat, wasserlöslichen Kalziumhydrogenphosphaten und Metallsalz-Lösung |
| FR3039830B1 (fr) | 2015-08-03 | 2018-09-07 | Ocp Sa | Procede de fabrication d'un engrais a base de phosphate d'ammonium presentant une teneur reduite en cadmium |
| PL3691992T3 (pl) | 2017-10-08 | 2022-10-24 | Cytec Industries Inc. | Sposoby usuwania metali ciężkich z roztworów kwasu fosforowego |
| MY207665A (en) | 2020-06-16 | 2025-03-11 | Yara Int Asa | Process for the removal of heavy metals from a phosphoric acid containing composition using an ionic polymeric surfactant and use of said surfactant in the precipitation of heavy metals in a phosphoric acid containing composition |
| AU2021294256B2 (en) | 2020-06-16 | 2024-01-04 | Yara International Asa | Process for the removal of heavy metals from a phosphoric acid containing composition |
| AU2021294255A1 (en) | 2020-06-16 | 2023-02-02 | Yara International Asa | Process for the removal of heavy metals from a phosphoric acid containing composition using a flocculating agent |
| EP3964477A1 (en) | 2020-09-08 | 2022-03-09 | Yara International ASA | Process for the removal of heavy metals from a phosphoric acid containing composition using an ionic polymeric surfactant |
| EP3964476A1 (en) | 2020-09-08 | 2022-03-09 | Yara International ASA | Process for the removal of heavy metals from a phosphoric acid containing composition using a flocculating agent |
| EP3964478A1 (en) | 2020-09-08 | 2022-03-09 | Yara International ASA | Process for the removal of heavy metals from a phosphoric acid containing composition |
| EP4015452A1 (en) | 2020-12-21 | 2022-06-22 | Técnicas Reunidas, S.A. | Process for producing technical grade phosphoric acid from sewage sludge ash |
| AU2023332203A1 (en) | 2022-09-02 | 2025-03-06 | Cytec Industries Inc. | Reagents and processes for removing heavy metals from phosphoric acid solutions |
| PL442462A1 (pl) * | 2022-10-07 | 2024-04-08 | Politechnika Wrocławska | Sposób oczyszczania surowców fosforowych przez kalcynację z dodatkiem soli nieorganicznych |
| CN120322408A (zh) | 2022-11-17 | 2025-07-15 | 塞特工业公司 | 用于从含磷酸的流中去除重金属的组合物和方法 |
| WO2024256668A1 (en) | 2023-06-15 | 2024-12-19 | Cytec Industries Inc. | Heavy metals removal from phosphoric acid containing streams |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SE37857C1 (OSRAM) | 1914-11-18 | |||
| SE190035C1 (OSRAM) | 1964-01-01 | |||
| US935337A (en) * | 1908-07-08 | 1909-09-28 | John Herbert Thwaites | Wet method of separating metallic compounds. |
| US1473641A (en) * | 1921-08-24 | 1923-11-13 | Pohl Otto | Process of dry distilling and carbonizing crude peat |
| US1783757A (en) * | 1927-12-14 | 1930-12-02 | Ig Farbenindustrie Ag | Dehydration of moist fuels |
| US1787192A (en) * | 1928-08-11 | 1930-12-30 | Rumford Chemical Works | Method of purifying phosphoric acid and the like |
| US2183924A (en) * | 1938-04-13 | 1939-12-19 | Eugene P Schoch | Lignite and process of producing the same |
| DE817590C (de) | 1948-10-02 | 1951-10-18 | Paul Hoppe | Verfahren zum Herstellen von hochwertigem Brennstoff |
| US3124419A (en) * | 1961-04-20 | 1964-03-10 | Purification of phosphoric acid | |
| US3205589A (en) * | 1961-09-27 | 1965-09-14 | West Wood Proc Corp | Process of drying wood by oil immersion and vacuum treatment to selected moisture content with oil recovery |
| US3685964A (en) * | 1970-12-09 | 1972-08-22 | Fmc Corp | Purification of alkali phosphate solution |
| SE393676B (sv) | 1972-02-22 | 1977-05-16 | B O Heger | Forfarande for torkning av tre och andra liknande fiberprodukter |
| JPS5018388A (OSRAM) | 1973-06-21 | 1975-02-26 | ||
| JPS5651123B2 (OSRAM) * | 1973-11-07 | 1981-12-03 | ||
| DE2447390C3 (de) | 1974-10-04 | 1983-11-17 | Hoechst Ag, 6230 Frankfurt | Verfahren zur Reinigung von Naßphosphorsäure |
| DE2608029C2 (de) * | 1976-02-27 | 1984-02-23 | Hoechst Ag, 6230 Frankfurt | Verfahren zur Herstellung einer Alkaliphosphatlösung aus Naßverfahrensphosphorsäuren |
| JPS5375196A (en) * | 1976-12-15 | 1978-07-04 | Central Glass Co Ltd | Removing method for heavy metals from phosphoric acid solution |
-
1979
- 1979-05-10 SE SE7904135A patent/SE418845B/sv not_active IP Right Cessation
-
1980
- 1980-05-08 JP JP55501082A patent/JPH021086B2/ja not_active Expired - Lifetime
- 1980-05-08 AT AT80850070T patent/ATE6050T1/de not_active IP Right Cessation
- 1980-05-08 EP EP80850070A patent/EP0023195B2/en not_active Expired
- 1980-05-08 DE DE8080850070T patent/DE3066353D1/de not_active Expired
- 1980-05-08 WO PCT/SE1980/000134 patent/WO1980002418A1/en unknown
- 1980-05-08 US US06/220,060 patent/US4378340A/en not_active Expired - Fee Related
- 1980-05-09 FI FI801521A patent/FI66162C/fi not_active IP Right Cessation
- 1980-12-22 DK DK547780A patent/DK151216C/da not_active IP Right Cessation
-
1981
- 1981-01-07 NO NO810039A patent/NO152505C/no unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP0023195B2 (en) | 1988-09-21 |
| NO152505B (no) | 1985-07-01 |
| SE7904135L (sv) | 1980-11-11 |
| DK547780A (da) | 1980-12-22 |
| US4378340A (en) | 1983-03-29 |
| EP0023195A2 (en) | 1981-01-28 |
| NO810039L (no) | 1981-01-07 |
| EP0023195B1 (en) | 1984-02-01 |
| EP0023195A3 (en) | 1981-09-09 |
| DK151216C (da) | 1988-07-18 |
| DK151216B (da) | 1987-11-16 |
| FI66162C (fi) | 1984-09-10 |
| FI801521A7 (fi) | 1980-11-11 |
| FI66162B (fi) | 1984-05-31 |
| JPS56500492A (OSRAM) | 1981-04-16 |
| ATE6050T1 (de) | 1984-02-15 |
| JPH021086B2 (OSRAM) | 1990-01-10 |
| SE418845B (sv) | 1981-06-29 |
| WO1980002418A1 (en) | 1980-11-13 |
| NO152505C (no) | 1985-10-09 |
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| FR2319576A1 (fr) | Procede de production d'acide phosphorique a partir de minerai de phosphate de calcium | |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8366 | Restricted maintained after opposition proceedings | ||
| 8339 | Ceased/non-payment of the annual fee |