DE266300C - - Google Patents

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Publication number
DE266300C
DE266300C DENDAT266300D DE266300DA DE266300C DE 266300 C DE266300 C DE 266300C DE NDAT266300 D DENDAT266300 D DE NDAT266300D DE 266300D A DE266300D A DE 266300DA DE 266300 C DE266300 C DE 266300C
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DE
Germany
Prior art keywords
phosphoric acid
heated
increased
oils
mineral
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
DENDAT266300D
Other languages
German (de)
Publication of DE266300C publication Critical patent/DE266300C/de
Active legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G17/00Refining of hydrocarbon oils in the absence of hydrogen, with acids, acid-forming compounds or acid-containing liquids, e.g. acid sludge
    • C10G17/02Refining of hydrocarbon oils in the absence of hydrogen, with acids, acid-forming compounds or acid-containing liquids, e.g. acid sludge with acids or acid-containing liquids, e.g. acid sludge
    • C10G17/04Liquid-liquid treatment forming two immiscible phases
    • C10G17/07Liquid-liquid treatment forming two immiscible phases using halogen acids or oxyacids of halogen
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10CWORKING-UP PITCH, ASPHALT, BITUMEN, TAR; PYROLIGNEOUS ACID
    • C10C1/00Working-up tar
    • C10C1/20Refining by chemical means inorganic or organic compounds
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G17/00Refining of hydrocarbon oils in the absence of hydrogen, with acids, acid-forming compounds or acid-containing liquids, e.g. acid sludge
    • C10G17/02Refining of hydrocarbon oils in the absence of hydrogen, with acids, acid-forming compounds or acid-containing liquids, e.g. acid sludge with acids or acid-containing liquids, e.g. acid sludge

Landscapes

  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Fats And Perfumes (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Description

DEUTSCHES REICHGERMAN EMPIRE

REICHSPATENTAMTREICH PATENT OFFICE

PATENTSCHRIFTPATENT LETTERING

KLASSE'230. GRUPPEl.CLASS '230. GROUP

Verfahren zur Gewinnung von reinen Mineral- und Teerölen.Process for the extraction of pure mineral and tar oils.

Zusatz zum Patent 264811.Addendum to patent 264811.

Patentiert im Deutschen Reiche vom 22. August 1912 ab. Längste Dauer: 21.August 1927.Patented in the German Empire on August 22, 1912. Longest duration: August 21, 1927.

In dem Hatiptpatent ist' ein Verfahren zur Reinigung yon Mineralölen, ζ. Β. Erdölen, oder von Teerölen u. dgl. mit Phosphorsäure beschrieben worden. . Es hat sich nun gezeigt, - 5 daß man auch brauchbare und marktfähige Produkte erhält, wenn man jenes Verfahren derart abändert,. daß man z. ü; zur Abarbeitung von rohem Erdöl, aus welchem die leichten Kohlenwasserstoffe noch nicht abdestilliert In the Hatipt patent there is a method for Cleaning of mineral oils, ζ. Β. Petroleum, or tar oils and the like with phosphoric acid has been described. . It has now been shown - 5 that one can also use useful and marketable Products obtained by modifying that process in such a way. that one z. ü; for processing crude petroleum from which the light hydrocarbons have not yet distilled off

10. sind — was beim Erhitzen auf etwa 3000 C. und darüber viele Schwierigkeiten bietet -—, andere Oxydationsprodukte des Phosphors bei niedriger Temperatur anwendet, z.B. bei 150 bis 2oo° C. Diese Temperatur kann dann gesteigert werden, falls es noch nötig ist.10 are - which, when heated to about 300 0 C. and above has many problems - other oxidation products of phosphorus applies at low temperature, for example, can then at 150 to 2oo ° C. This temperature can be increased if it is still necessary .

A u s f ü h run g S'b e i s ρ i e 1.D o u tio n S'b e i s ρ i e 1.

20 kg Meta-Phosphorsäure, - 20 kg Pyro-Phosphorsäure urd 2 kg phosphorige Säure werden in einer Lösung von '5 kg technischer Phosphorsäure gelöst, so daß das Ganze eine sirupöse Flüssigkeit bildet; zu dieser'Flüssigkeit werden 1000 kg leichtsiedendes Mineralöl gegeben, ..und es wird auf etwa- 150 bis 200° C. erhitzt.20 kg meta-phosphoric acid, - 20 kg pyro-phosphoric acid urd 2 kg of phosphorous acid become more technical in a solution of 5 kg Phosphoric acid dissolved so that the whole forms a syrupy liquid; to this' liquid 1000 kg of low-boiling mineral oil are added, ... and it is increased to about 150 to Heated to 200 ° C.

Claims (1)

Patent-Anspruch:Patent claim: Verfahren zur Gewinnung von reinen Mineral- und Teerölen nach Patent 264811, dadurch gekennzeichnet, daß die rohen Öle anstatt mit Phosphorsäure auf hohe Temperatur mit den anderen Sauerstoffverbindungen des Phosphors auf niedrigere 35' Temperatur (etwa 150 bis 2009C.) erhitzt werden, die später auf etwa 3000 C. und darüber gesteigert werden kanu.Process for the production of pure mineral and tar oils according to patent 264811, characterized in that the crude oils are heated to a lower temperature (about 150 to 200 9 C.) with the other oxygen compounds of phosphorus instead of with phosphoric acid to a high temperature later be increased to about 300 0 C. and about canoe.
DENDAT266300D Active DE266300C (en)

Publications (1)

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DE266300C true DE266300C (en)

Family

ID=523441

Family Applications (1)

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Country Status (1)

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DE (1) DE266300C (en)

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