DE253706C - - Google Patents
Info
- Publication number
- DE253706C DE253706C DENDAT253706D DE253706DA DE253706C DE 253706 C DE253706 C DE 253706C DE NDAT253706 D DENDAT253706 D DE NDAT253706D DE 253706D A DE253706D A DE 253706DA DE 253706 C DE253706 C DE 253706C
- Authority
- DE
- Germany
- Prior art keywords
- carbon oxide
- hydrogen
- evaporator
- water gas
- condenser
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/06—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by partial condensation
Landscapes
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Mechanical Engineering (AREA)
- Thermal Sciences (AREA)
- General Engineering & Computer Science (AREA)
- Separation By Low-Temperature Treatments (AREA)
Description
KAISERLICHESIMPERIAL
PATENTAMT.PATENT OFFICE.
PATENTSCHRIFTPATENT LETTERING
- M 253706 KLASSE 12«. GRUPPE- M 253706 CLASS 12 «. GROUP
Patentiert im Deutschen Reiche vom 10. November 1911 ab.Patented in the German Empire on November 10, 1911.
Der den Gegenstand der Erfindung bildende Apparat dient zur Trennung von Wasserstoff und Kohlenoxyd aus Wassergas durch Abscheidung des Kohlenoxyds in flüssiger Form.The apparatus forming the subject of the invention serves to separate hydrogen and carbon oxide from water gas by separating the carbon oxide in liquid form.
Der Apparat ist in der beiliegenden Zeichnung veranschaulicht. Er besteht aus einem Kondensator h und Verdampfer d, die durch ein Uberströmrohr verbunden sind. Das Wesen der Erfindung besteht darin, daß zum ZweckeThe apparatus is illustrated in the accompanying drawing. It consists of a condenser h and evaporator d, which are connected by an overflow pipe. The essence of the invention is that for the purpose
ίο der vollständigen Trennung des Wasserstoffes vom Kohlenoxyd an dem Kondensator und an dem Verdampfer schachtförmige Verlängerungen vorgesehen sind, so daß der gasförmig gebliebene Wasserstoff ,in dem in dem Kondensator angeschlossenen Schacht nach oben steigt und ebenso der aus dem Kondensator mit dem verflüssigten Kohlenoxyd in den Verdampfer noch mitgerissene Wasserstoff sich in dem Schacht des Verdampfers sammelt.ίο the complete separation of the hydrogen from the carbon dioxide on the condenser and on the evaporator shaft-shaped extensions are provided so that the gaseous hydrogen remaining in the in the condenser connected shaft rises upwards and so does the one from the condenser with the liquefied carbon oxide into the evaporator Any hydrogen that is still entrained collects in the shaft of the evaporator.
In einem Generator wird Wassergas erzeugt und in einem Kompressor auf jenen Druck gebracht, der für die Verflüssigung des im Wassergas enthaltenen Kohlenoxyds nötig ist.Water gas is produced in a generator and at this pressure in a compressor brought, which is necessary for the liquefaction of the carbon dioxide contained in the water gas.
• Verunreinigungen des Wassergases, wie z. B.• Impurities in the water gas, such as B.
Kohlensäure, können sowohl vor als auch nach der Kompression in bekannter Weise ausgeschieden werden. Das Wassergas tritt hierauf in den Trennungsapparat a, durchströmt im Gegenstrom zu kaltem Wasserstoff ein Rohrbündel b, gelangt aus diesem in eine Rohrschlange c, die in dem teilweise mit flüssigem Kohlenoxyd gefüllten Verdampfer d liegt, wird bei e entspannt und tritt durch eine Düse mit einstellbarem Eintrittsquerschnitt in den Kondensator h. In diesem sammelt sich nun das verflüssigte Kohlenoxyd, während der gasförmig bleibende Wasserstoff in der schachtförmigen Verlängerung i des Kondensatorraumes nach oben steigt. In i werden die mitgerissenen Kohlenoxyddämpfe von dem bekanntlich sehr leichten Wasserstoff getrennt, indem sie infolge ihres größeren spezifischen Gewichtes nach unten sinken. Der von Kohlenoxyd gereinigte Wasserstoff tritt nun durch das Überströmrohr k in das Rohrbündel b, im Gegenstrom an das verdichtete Wassergas seine Kälte abgebend, und entweicht bei / aus dem Trennungsapparat.Carbonic acid can be excreted in a known manner both before and after compression. The water gas then enters the separation apparatus a, flows through a tube bundle b in countercurrent to the cold hydrogen, passes from this into a tube coil c, which is located in the evaporator d , which is partially filled with liquid carbon oxide, is expanded at e and passes through a nozzle with adjustable Entry cross-section into the condenser h. The liquefied carbon oxide collects in this, while the hydrogen, which remains in gaseous form , rises upwards in the shaft-shaped extension i of the condenser space. In i the entrained carbon oxide vapors are separated from the hydrogen, which is known to be very light, in that they sink downwards as a result of their greater specific weight. The hydrogen, which has been purified of carbon oxide, now passes through the overflow pipe k into the pipe bundle b, releasing its coldness in countercurrent to the compressed water gas, and escapes at / from the separation apparatus.
Das in h gesammelte flüssige Kohlenoxyd fließt durch das Überströmrohr m in den schachtförmigen Aufsatz η des Verdampfers d. Der Schacht η dient dazu, das Kohlenoxyd von mitgerissenem Wasserstoff zu befreien; dieser sammelt sich im oberen Teil von η und wird von dort durch eine Reguliervorrichtung abgelassen. Das ist besonders dann von Bedeutung, wenn es sich um die Gewinnung von sehr reinem Kohlenoxyd handelt.The liquid carbon oxide collected in h flows through the overflow pipe m into the shaft-shaped attachment η of the evaporator d. The shaft η serves to free the carbon oxide from entrained hydrogen; this collects in the upper part of η and is drained from there by a regulating device. This is particularly important when it comes to the extraction of very pure carbon monoxide.
Zur Regelung des Überströmens dient das Ventil 0. Das durch m austretende flüssige Kohlenoxyd sammelt sich am Boden von d, wobei es durch die Rohrschlange c geheizt wird und wieder verdampft. Die Kohlenoxyddämpfe entweichen durch das Rohr p, durchströmen das Rohrbündel b, im Gegenstrom an das Wassergas Kälte abgebend, und treten bei I aus dem Apparat.Valve 0 is used to regulate the overflow. The liquid carbon oxide exiting through m collects at the bottom of d, where it is heated by the coil c and evaporates again. The carbon oxide vapors escape through tube p, flow through tube bundle b, releasing cold in countercurrent to the water gas, and emerge from the apparatus at I.
Durch entsprechend gewählte Höhe der Schächte i und η kann man beide Gase in beliebiger Reinheit erhalten.By appropriately choosing the height of the shafts i and η , both gases can be obtained in any purity.
Zur Vorkühlung des Wassergases auf—80 ° kann eine Rohrschlange y dienen, in der flüssige Kohlensäure oder ein anderes Kältemittel verdampft und im Gegenstrom Kälte an das Wassergas abgibt. A pipe coil y can be used to precool the water gas to -80 °, in which liquid carbonic acid or another refrigerant evaporates and releases cold to the water gas in countercurrent.
Claims (1)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE253706T |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE253706C true DE253706C (en) | 1912-11-14 |
Family
ID=5954412
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT253706D Expired DE253706C (en) |
Country Status (2)
| Country | Link |
|---|---|
| DE (1) | DE253706C (en) |
| FR (1) | FR445883A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5314843A (en) * | 1992-03-27 | 1994-05-24 | Micron Technology, Inc. | Integrated circuit polishing method |
-
0
- DE DENDAT253706D patent/DE253706C/de not_active Expired
-
1912
- 1912-07-08 FR FR445883A patent/FR445883A/en not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5314843A (en) * | 1992-03-27 | 1994-05-24 | Micron Technology, Inc. | Integrated circuit polishing method |
Also Published As
| Publication number | Publication date |
|---|---|
| FR445883A (en) | 1912-11-21 |
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