DE2232225C3 - Verfahren zur Herstellung von kubischem Bornitrid - Google Patents
Verfahren zur Herstellung von kubischem BornitridInfo
- Publication number
- DE2232225C3 DE2232225C3 DE2232225A DE2232225A DE2232225C3 DE 2232225 C3 DE2232225 C3 DE 2232225C3 DE 2232225 A DE2232225 A DE 2232225A DE 2232225 A DE2232225 A DE 2232225A DE 2232225 C3 DE2232225 C3 DE 2232225C3
- Authority
- DE
- Germany
- Prior art keywords
- boron nitride
- cubic boron
- cemented carbide
- hexagonal boron
- mass
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229910052582 BN Inorganic materials 0.000 title claims description 145
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 title claims description 145
- 238000000034 method Methods 0.000 title claims description 19
- 238000004519 manufacturing process Methods 0.000 title description 8
- 229910052751 metal Inorganic materials 0.000 claims description 49
- 239000002184 metal Substances 0.000 claims description 49
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 38
- 239000000843 powder Substances 0.000 claims description 29
- 229910052782 aluminium Inorganic materials 0.000 claims description 26
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 24
- 229910045601 alloy Inorganic materials 0.000 claims description 20
- 239000000956 alloy Substances 0.000 claims description 20
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 19
- 229910052759 nickel Inorganic materials 0.000 claims description 19
- 239000010941 cobalt Substances 0.000 claims description 18
- 229910017052 cobalt Inorganic materials 0.000 claims description 18
- 239000003054 catalyst Substances 0.000 claims description 17
- 239000011572 manganese Substances 0.000 claims description 10
- 229910052748 manganese Inorganic materials 0.000 claims description 9
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims description 8
- 150000002739 metals Chemical class 0.000 claims description 6
- 238000011065 in-situ storage Methods 0.000 claims description 4
- 238000010586 diagram Methods 0.000 claims 1
- 239000013078 crystal Substances 0.000 description 30
- 239000000203 mixture Substances 0.000 description 25
- 238000011049 filling Methods 0.000 description 20
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 17
- 229910052750 molybdenum Inorganic materials 0.000 description 17
- 239000011733 molybdenum Substances 0.000 description 17
- 239000002245 particle Substances 0.000 description 12
- 238000006243 chemical reaction Methods 0.000 description 9
- 239000000463 material Substances 0.000 description 8
- 231100000241 scar Toxicity 0.000 description 8
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- 150000003839 salts Chemical class 0.000 description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 5
- 238000005520 cutting process Methods 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 239000011159 matrix material Substances 0.000 description 5
- 239000001301 oxygen Substances 0.000 description 5
- 229910052760 oxygen Inorganic materials 0.000 description 5
- UONOETXJSWQNOL-UHFFFAOYSA-N tungsten carbide Chemical compound [W+]#[C-] UONOETXJSWQNOL-UHFFFAOYSA-N 0.000 description 5
- 229910000838 Al alloy Inorganic materials 0.000 description 4
- 229910000943 NiAl Inorganic materials 0.000 description 4
- NPXOKRUENSOPAO-UHFFFAOYSA-N Raney nickel Chemical compound [Al].[Ni] NPXOKRUENSOPAO-UHFFFAOYSA-N 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 4
- 229910052721 tungsten Inorganic materials 0.000 description 4
- 239000010937 tungsten Substances 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 229910052742 iron Inorganic materials 0.000 description 3
- 238000003754 machining Methods 0.000 description 3
- 239000006187 pill Substances 0.000 description 3
- 229910052903 pyrophyllite Inorganic materials 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 210000001787 dendrite Anatomy 0.000 description 2
- 239000010439 graphite Substances 0.000 description 2
- 229910002804 graphite Inorganic materials 0.000 description 2
- 230000001788 irregular Effects 0.000 description 2
- 239000011812 mixed powder Substances 0.000 description 2
- 238000010587 phase diagram Methods 0.000 description 2
- 238000005498 polishing Methods 0.000 description 2
- 229910001088 rené 41 Inorganic materials 0.000 description 2
- 229910000679 solder Inorganic materials 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- 229910000601 superalloy Inorganic materials 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- 229910052715 tantalum Inorganic materials 0.000 description 2
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 description 2
- 239000010936 titanium Substances 0.000 description 2
- 229910052719 titanium Inorganic materials 0.000 description 2
- 229910052726 zirconium Inorganic materials 0.000 description 2
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 1
- 229910018131 Al-Mn Inorganic materials 0.000 description 1
- 229910018461 Al—Mn Inorganic materials 0.000 description 1
- 229910052580 B4C Inorganic materials 0.000 description 1
- 229910000925 Cd alloy Inorganic materials 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 229910002065 alloy metal Inorganic materials 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical group [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- INAHAJYZKVIDIZ-UHFFFAOYSA-N boron carbide Chemical compound B12B3B4C32B41 INAHAJYZKVIDIZ-UHFFFAOYSA-N 0.000 description 1
- NSAODVHAXBZWGW-UHFFFAOYSA-N cadmium silver Chemical compound [Ag].[Cd] NSAODVHAXBZWGW-UHFFFAOYSA-N 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- -1 cicronium Chemical compound 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 238000003384 imaging method Methods 0.000 description 1
- 229910001026 inconel Inorganic materials 0.000 description 1
- 229910000816 inconels 718 Inorganic materials 0.000 description 1
- 239000011872 intimate mixture Substances 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- NFFIWVVINABMKP-UHFFFAOYSA-N methylidynetantalum Chemical compound [Ta]#C NFFIWVVINABMKP-UHFFFAOYSA-N 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000000284 resting effect Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- 229910003468 tantalcarbide Inorganic materials 0.000 description 1
- PMTRSEDNJGMXLN-UHFFFAOYSA-N titanium zirconium Chemical compound [Ti].[Zr] PMTRSEDNJGMXLN-UHFFFAOYSA-N 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- MTPVUVINMAGMJL-UHFFFAOYSA-N trimethyl(1,1,2,2,2-pentafluoroethyl)silane Chemical compound C[Si](C)(C)C(F)(F)C(F)(F)F MTPVUVINMAGMJL-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/58—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides
- C04B35/583—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides based on boron nitride
- C04B35/5831—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides based on boron nitride based on cubic boron nitrides or Wurtzitic boron nitrides, including crystal structure transformation of powder
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Crystallography & Structural Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Powder Metallurgy (AREA)
- Ceramic Products (AREA)
- Catalysts (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US15871071A | 1971-07-01 | 1971-07-01 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2232225A1 DE2232225A1 (de) | 1973-01-18 |
| DE2232225B2 DE2232225B2 (de) | 1981-04-16 |
| DE2232225C3 true DE2232225C3 (de) | 1982-02-04 |
Family
ID=22569359
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2232225A Expired DE2232225C3 (de) | 1971-07-01 | 1972-06-30 | Verfahren zur Herstellung von kubischem Bornitrid |
Country Status (13)
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE805525A (fr) * | 1972-10-02 | 1974-04-01 | Vnii Abrazivov | Materiau composite extra-dur a base de nitrure cubique de bore et procede d'obtention de ce materiau |
| IN150013B (enrdf_load_stackoverflow) * | 1977-07-01 | 1982-06-26 | Gen Electric | |
| JPS5860604A (ja) * | 1981-10-01 | 1983-04-11 | Komatsu Ltd | 立方晶窒化硼素の合成法 |
| US5043120A (en) * | 1988-11-10 | 1991-08-27 | The General Electric Company | Process for preparing polycrystalline CBN ceramic masses |
| US9808544B2 (en) | 2005-08-31 | 2017-11-07 | Ultraviolet Sciences, Inc. | Ultraviolet light treatment chamber |
| JP5613970B2 (ja) * | 2011-03-30 | 2014-10-29 | 三菱マテリアル株式会社 | 立方晶窒化ホウ素の合成方法および立方晶窒化ホウ素焼結体の製造方法 |
| WO2020096038A1 (ja) * | 2018-11-08 | 2020-05-14 | 国立大学法人群馬大学 | 粒子群計測装置 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3192015A (en) | 1963-04-01 | 1965-06-29 | Gen Electric | Growth of large cubic form of boron nitride crystals |
-
1972
- 1972-06-13 ZA ZA724056A patent/ZA724056B/xx unknown
- 1972-06-22 GB GB2936372A patent/GB1391665A/en not_active Expired
- 1972-06-27 CA CA145,768A patent/CA982541A/en not_active Expired
- 1972-06-27 NL NLAANVRAGE7208866,A patent/NL174714C/xx not_active IP Right Cessation
- 1972-06-28 IT IT26341/72A patent/IT956917B/it active
- 1972-06-29 JP JP6539272A patent/JPS5517000B2/ja not_active Expired
- 1972-06-30 CH CH981872A patent/CH573867A5/xx not_active IP Right Cessation
- 1972-06-30 DK DK327472A patent/DK144415C/da not_active IP Right Cessation
- 1972-06-30 FR FR7223865A patent/FR2143954B1/fr not_active Expired
- 1972-06-30 SE SE7208676A patent/SE393588B/xx unknown
- 1972-06-30 DE DE2232225A patent/DE2232225C3/de not_active Expired
- 1972-07-03 AT AT571272A patent/AT352078B/de active
- 1972-07-03 BE BE785770A patent/BE785770A/xx not_active IP Right Cessation
-
1976
- 1976-01-08 SE SE7600140A patent/SE418962B/xx not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| SE393588B (sv) | 1977-05-16 |
| NL174714C (nl) | 1984-08-01 |
| JPS5517000B2 (enrdf_load_stackoverflow) | 1980-05-08 |
| GB1391665A (en) | 1975-04-23 |
| FR2143954B1 (enrdf_load_stackoverflow) | 1977-08-26 |
| ZA724056B (en) | 1973-03-28 |
| DE2232225B2 (de) | 1981-04-16 |
| AT352078B (de) | 1979-08-27 |
| SE418962B (sv) | 1981-07-06 |
| IT956917B (it) | 1973-10-10 |
| FR2143954A1 (enrdf_load_stackoverflow) | 1973-02-09 |
| DK144415B (da) | 1982-03-08 |
| NL7208866A (enrdf_load_stackoverflow) | 1973-01-03 |
| JPS4818200A (enrdf_load_stackoverflow) | 1973-03-07 |
| CA982541A (en) | 1976-01-27 |
| ATA571272A (de) | 1979-02-15 |
| BE785770A (fr) | 1972-11-03 |
| DE2232225A1 (de) | 1973-01-18 |
| DK144415C (da) | 1982-08-16 |
| SE7600140L (sv) | 1976-01-08 |
| CH573867A5 (enrdf_load_stackoverflow) | 1976-03-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OD | Request for examination | ||
| C3 | Grant after two publication steps (3rd publication) | ||
| 8328 | Change in the person/name/address of the agent |
Free format text: SCHUELER, H., DIPL.-CHEM. DR.RER.NAT., PAT.-ANW., 6000 FRANKFURT |
|
| AH | Division in |
Ref country code: DE Ref document number: 2248539 Format of ref document f/p: P |
|
| 8339 | Ceased/non-payment of the annual fee |