DE2150400B2 - Verfahren zur Herstellung von Tetrachlorkohlenstoff - Google Patents
Verfahren zur Herstellung von TetrachlorkohlenstoffInfo
- Publication number
- DE2150400B2 DE2150400B2 DE2150400A DE2150400A DE2150400B2 DE 2150400 B2 DE2150400 B2 DE 2150400B2 DE 2150400 A DE2150400 A DE 2150400A DE 2150400 A DE2150400 A DE 2150400A DE 2150400 B2 DE2150400 B2 DE 2150400B2
- Authority
- DE
- Germany
- Prior art keywords
- volatile
- substances
- reaction
- reaction zone
- chlorine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 title claims description 22
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- 238000000034 method Methods 0.000 title claims 5
- 238000006243 chemical reaction Methods 0.000 claims description 27
- 239000000460 chlorine Substances 0.000 claims description 20
- 229910052801 chlorine Inorganic materials 0.000 claims description 20
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 18
- 239000000203 mixture Substances 0.000 claims description 14
- 238000010438 heat treatment Methods 0.000 claims description 10
- 239000000126 substance Substances 0.000 claims description 10
- CKAPSXZOOQJIBF-UHFFFAOYSA-N hexachlorobenzene Chemical compound ClC1=C(Cl)C(Cl)=C(Cl)C(Cl)=C1Cl CKAPSXZOOQJIBF-UHFFFAOYSA-N 0.000 claims description 5
- 229910052799 carbon Inorganic materials 0.000 claims description 4
- 239000000047 product Substances 0.000 claims description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 3
- 125000001309 chloro group Chemical group Cl* 0.000 claims description 2
- 239000000470 constituent Substances 0.000 claims description 2
- 238000006467 substitution reaction Methods 0.000 claims description 2
- 229930195733 hydrocarbon Natural products 0.000 claims 2
- 150000002430 hydrocarbons Chemical class 0.000 claims 2
- 239000004215 Carbon black (E152) Substances 0.000 claims 1
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 claims 1
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 239000003054 catalyst Substances 0.000 claims 1
- 238000005660 chlorination reaction Methods 0.000 claims 1
- 238000001514 detection method Methods 0.000 claims 1
- 239000000446 fuel Substances 0.000 claims 1
- 239000012535 impurity Substances 0.000 claims 1
- 230000000737 periodic effect Effects 0.000 claims 1
- 238000005070 sampling Methods 0.000 claims 1
- 239000007858 starting material Substances 0.000 claims 1
- HFFLGKNGCAIQMO-UHFFFAOYSA-N trichloroacetaldehyde Chemical compound ClC(Cl)(Cl)C=O HFFLGKNGCAIQMO-UHFFFAOYSA-N 0.000 claims 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 24
- 239000007788 liquid Substances 0.000 description 5
- 239000000523 sample Substances 0.000 description 4
- VHHHONWQHHHLTI-UHFFFAOYSA-N hexachloroethane Chemical compound ClC(Cl)(Cl)C(Cl)(Cl)Cl VHHHONWQHHHLTI-UHFFFAOYSA-N 0.000 description 3
- UBOXGVDOUJQMTN-UHFFFAOYSA-N 1,1,2-trichloroethane Chemical class ClCC(Cl)Cl UBOXGVDOUJQMTN-UHFFFAOYSA-N 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 125000001931 aliphatic group Chemical group 0.000 description 2
- YACLQRRMGMJLJV-UHFFFAOYSA-N chloroprene Chemical compound ClC(=C)C=C YACLQRRMGMJLJV-UHFFFAOYSA-N 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 150000001993 dienes Chemical class 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical compound CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 description 1
- UAZUEJTXWAXSMA-UHFFFAOYSA-N 1,1-dichlorobut-1-ene Chemical class CCC=C(Cl)Cl UAZUEJTXWAXSMA-UHFFFAOYSA-N 0.000 description 1
- MHGNMCJZSOSEJB-UHFFFAOYSA-N 1,2,3,4,5,6-hexachlorobenzene;1,1,1,2,2,2-hexachloroethane Chemical compound ClC(Cl)(Cl)C(Cl)(Cl)Cl.ClC1=C(Cl)C(Cl)=C(Cl)C(Cl)=C1Cl MHGNMCJZSOSEJB-UHFFFAOYSA-N 0.000 description 1
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 1
- KPZGRMZPZLOPBS-UHFFFAOYSA-N 1,3-dichloro-2,2-bis(chloromethyl)propane Chemical compound ClCC(CCl)(CCl)CCl KPZGRMZPZLOPBS-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- CYTYCFOTNPOANT-UHFFFAOYSA-N Perchloroethylene Chemical group ClC(Cl)=C(Cl)Cl CYTYCFOTNPOANT-UHFFFAOYSA-N 0.000 description 1
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 description 1
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 1
- CEDLUJHGAQHWKL-UHFFFAOYSA-N [C].ClC(Cl)(Cl)Cl Chemical compound [C].ClC(Cl)(Cl)Cl CEDLUJHGAQHWKL-UHFFFAOYSA-N 0.000 description 1
- 239000000538 analytical sample Substances 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 description 1
- -1 chloroprene Chemical class 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- BNIXVQGCZULYKV-UHFFFAOYSA-N pentachloroethane Chemical compound ClC(Cl)C(Cl)(Cl)Cl BNIXVQGCZULYKV-UHFFFAOYSA-N 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000000859 sublimation Methods 0.000 description 1
- 230000008022 sublimation Effects 0.000 description 1
- 229950011008 tetrachloroethylene Drugs 0.000 description 1
- 238000013022 venting Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/361—Preparation of halogenated hydrocarbons by reactions involving a decrease in the number of carbon atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (9)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2150400A DE2150400B2 (de) | 1971-10-09 | 1971-10-09 | Verfahren zur Herstellung von Tetrachlorkohlenstoff |
| CA152,489A CA988540A (en) | 1971-10-09 | 1972-09-25 | Process for the manufacture of carbon tetrachloride |
| NL7213425A NL7213425A (enExample) | 1971-10-09 | 1972-10-04 | |
| GB4604572A GB1396752A (en) | 1971-10-09 | 1972-10-05 | Halogenation of organic materials |
| US00295715A US3845148A (en) | 1971-10-09 | 1972-10-06 | Process for the manufacture of carbon tetrachloride |
| FR7235482A FR2156115B1 (enExample) | 1971-10-09 | 1972-10-06 | |
| IT30227/72A IT968744B (it) | 1971-10-09 | 1972-10-06 | Procedimento per la preparazione di tetracloruro di carbonio |
| JP47099952A JPS4844206A (enExample) | 1971-10-09 | 1972-10-06 | |
| BE122905A BE789854A (fr) | 1971-10-09 | 1972-10-09 | Procede de preparation du tetrachlorure de carbone |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2150400A DE2150400B2 (de) | 1971-10-09 | 1971-10-09 | Verfahren zur Herstellung von Tetrachlorkohlenstoff |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2150400A1 DE2150400A1 (de) | 1973-04-12 |
| DE2150400B2 true DE2150400B2 (de) | 1974-02-28 |
| DE2150400C3 DE2150400C3 (enExample) | 1974-10-03 |
Family
ID=5821897
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2150400A Granted DE2150400B2 (de) | 1971-10-09 | 1971-10-09 | Verfahren zur Herstellung von Tetrachlorkohlenstoff |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US3845148A (enExample) |
| JP (1) | JPS4844206A (enExample) |
| BE (1) | BE789854A (enExample) |
| CA (1) | CA988540A (enExample) |
| DE (1) | DE2150400B2 (enExample) |
| FR (1) | FR2156115B1 (enExample) |
| GB (1) | GB1396752A (enExample) |
| IT (1) | IT968744B (enExample) |
| NL (1) | NL7213425A (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0051236A1 (de) * | 1980-10-30 | 1982-05-12 | Hoechst Aktiengesellschaft | Verfahren zur Herstellung von Tetrachlorkohlenstoff |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5259333A (en) * | 1975-11-11 | 1977-05-16 | Yuukichi Asakawa | Combustion device |
| JPS5337573A (en) * | 1976-09-20 | 1978-04-06 | Japan Steel Works Ltd:The | Method and apparatus for cleaning waste gas |
| JPS5392563A (en) * | 1977-01-21 | 1978-08-14 | Yuukichi Asakawa | Garbage incinerator |
| JPH04358761A (ja) * | 1991-06-06 | 1992-12-11 | Masamichi Higashiyama | 波動静電気イオン化による、不完全燃焼改善装置。 |
-
1971
- 1971-10-09 DE DE2150400A patent/DE2150400B2/de active Granted
-
1972
- 1972-09-25 CA CA152,489A patent/CA988540A/en not_active Expired
- 1972-10-04 NL NL7213425A patent/NL7213425A/xx not_active Application Discontinuation
- 1972-10-05 GB GB4604572A patent/GB1396752A/en not_active Expired
- 1972-10-06 JP JP47099952A patent/JPS4844206A/ja active Pending
- 1972-10-06 US US00295715A patent/US3845148A/en not_active Expired - Lifetime
- 1972-10-06 FR FR7235482A patent/FR2156115B1/fr not_active Expired
- 1972-10-06 IT IT30227/72A patent/IT968744B/it active
- 1972-10-09 BE BE122905A patent/BE789854A/xx unknown
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0051236A1 (de) * | 1980-10-30 | 1982-05-12 | Hoechst Aktiengesellschaft | Verfahren zur Herstellung von Tetrachlorkohlenstoff |
Also Published As
| Publication number | Publication date |
|---|---|
| CA988540A (en) | 1976-05-04 |
| BE789854A (fr) | 1973-04-09 |
| US3845148A (en) | 1974-10-29 |
| NL7213425A (enExample) | 1973-04-11 |
| FR2156115B1 (enExample) | 1976-03-26 |
| JPS4844206A (enExample) | 1973-06-26 |
| DE2150400C3 (enExample) | 1974-10-03 |
| FR2156115A1 (enExample) | 1973-05-25 |
| IT968744B (it) | 1974-03-20 |
| DE2150400A1 (de) | 1973-04-12 |
| GB1396752A (en) | 1975-06-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| E77 | Valid patent as to the heymanns-index 1977 | ||
| EHJ | Ceased/non-payment of the annual fee |