DE2118539A1 - Verfahren und Vorrichtung zur Analyse von Flüssigkeitsgemischen - Google Patents
Verfahren und Vorrichtung zur Analyse von FlüssigkeitsgemischenInfo
- Publication number
- DE2118539A1 DE2118539A1 DE19712118539 DE2118539A DE2118539A1 DE 2118539 A1 DE2118539 A1 DE 2118539A1 DE 19712118539 DE19712118539 DE 19712118539 DE 2118539 A DE2118539 A DE 2118539A DE 2118539 A1 DE2118539 A1 DE 2118539A1
- Authority
- DE
- Germany
- Prior art keywords
- component
- mixture
- concentration
- liquid mixture
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000203 mixture Substances 0.000 title claims description 125
- 239000007788 liquid Substances 0.000 title claims description 76
- 238000000034 method Methods 0.000 title claims description 30
- 238000004458 analytical method Methods 0.000 title claims description 19
- 238000006243 chemical reaction Methods 0.000 claims description 34
- 239000000470 constituent Substances 0.000 claims description 30
- 238000004587 chromatography analysis Methods 0.000 claims description 29
- 239000012159 carrier gas Substances 0.000 claims description 10
- 239000003054 catalyst Substances 0.000 claims description 10
- 230000000704 physical effect Effects 0.000 claims description 8
- 238000004817 gas chromatography Methods 0.000 claims description 5
- 238000001179 sorption measurement Methods 0.000 claims description 5
- 229930195733 hydrocarbon Natural products 0.000 claims description 4
- 150000002430 hydrocarbons Chemical class 0.000 claims description 4
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 4
- 238000012360 testing method Methods 0.000 claims description 4
- 229910000831 Steel Inorganic materials 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 230000000737 periodic effect Effects 0.000 claims description 3
- 238000002407 reforming Methods 0.000 claims description 3
- 239000010959 steel Substances 0.000 claims description 3
- 238000004891 communication Methods 0.000 claims description 2
- 229910052697 platinum Inorganic materials 0.000 claims description 2
- 239000000523 sample Substances 0.000 claims 13
- 230000000052 comparative effect Effects 0.000 claims 2
- 239000007789 gas Substances 0.000 claims 2
- 238000006555 catalytic reaction Methods 0.000 claims 1
- 239000012530 fluid Substances 0.000 claims 1
- 239000011261 inert gas Substances 0.000 claims 1
- 238000011835 investigation Methods 0.000 claims 1
- 238000005259 measurement Methods 0.000 claims 1
- 229910000510 noble metal Inorganic materials 0.000 claims 1
- 238000002271 resection Methods 0.000 claims 1
- 230000032258 transport Effects 0.000 claims 1
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 4
- 125000003118 aryl group Chemical group 0.000 description 3
- 238000001833 catalytic reforming Methods 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 239000012188 paraffin wax Substances 0.000 description 3
- 229920006395 saturated elastomer Polymers 0.000 description 3
- 239000006200 vaporizer Substances 0.000 description 3
- 239000004215 Carbon black (E152) Substances 0.000 description 2
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical class S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 150000001336 alkenes Chemical class 0.000 description 2
- 238000010924 continuous production Methods 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000000446 fuel Substances 0.000 description 2
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 2
- NDVLTZFQVDXFAN-UHFFFAOYSA-N 3-(2-cyanoethylsulfanyl)propanenitrile Chemical compound N#CCCSCCC#N NDVLTZFQVDXFAN-UHFFFAOYSA-N 0.000 description 1
- 241000282465 Canis Species 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 238000011001 backwashing Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000011088 calibration curve Methods 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000003889 chemical engineering Methods 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 235000013601 eggs Nutrition 0.000 description 1
- 238000010828 elution Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000004949 mass spectrometry Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 235000019645 odor Nutrition 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000005504 petroleum refining Methods 0.000 description 1
- 238000004886 process control Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229920002379 silicone rubber Polymers 0.000 description 1
- 239000004945 silicone rubber Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000004611 spectroscopical analysis Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/26—Oils; Viscous liquids; Paints; Inks
- G01N33/28—Oils, i.e. hydrocarbon liquids
- G01N33/2835—Specific substances contained in the oils or fuels
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/86—Signal analysis
- G01N30/8603—Signal analysis with integration or differentiation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
- G01N2030/8886—Analysis of industrial production processes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/21—Hydrocarbon
- Y10T436/212—Aromatic
Landscapes
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Physics & Mathematics (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- Pathology (AREA)
- Immunology (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- General Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Food Science & Technology (AREA)
- Molecular Biology (AREA)
- Algebra (AREA)
- Mathematical Analysis (AREA)
- Mathematical Optimization (AREA)
- Pure & Applied Mathematics (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US74648768A | 1968-07-22 | 1968-07-22 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2118539A1 true DE2118539A1 (de) | 1972-10-26 |
Family
ID=25001060
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19712118539 Pending DE2118539A1 (de) | 1968-07-22 | 1971-04-16 | Verfahren und Vorrichtung zur Analyse von Flüssigkeitsgemischen |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US3607073A (enrdf_load_stackoverflow) |
| DE (1) | DE2118539A1 (enrdf_load_stackoverflow) |
| FR (1) | FR2137088B1 (enrdf_load_stackoverflow) |
| GB (1) | GB1304796A (enrdf_load_stackoverflow) |
| NL (1) | NL7106353A (enrdf_load_stackoverflow) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2008067296A3 (en) * | 2006-11-29 | 2008-09-18 | Schlumberger Services Petrol | Microfluidic gas chromatography system architecture |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3753653A (en) * | 1971-03-01 | 1973-08-21 | N Soulages | Method and apparatus for gaseous-phase chemical reaction analysis |
| US3844719A (en) * | 1972-06-01 | 1974-10-29 | Ppg Industries Inc | Mercury metal analyzer |
| DE2243650C3 (de) * | 1972-09-06 | 1980-12-04 | Winfried Dr. Ebing | Gerät zur automatischen Reinigung der Extrakte aus pflanzlichen und tierischen Objekten |
| US4009005A (en) * | 1973-03-19 | 1977-02-22 | Becton, Dickinson And Company | Apparatus for radioimmunoassay with regeneration of immunadsorbent |
| US4229971A (en) * | 1975-04-28 | 1980-10-28 | Phillips Petroleum Company | Liquid sampling system |
| US4113434A (en) * | 1975-07-30 | 1978-09-12 | Yanagimoto Seisakusho Co., Ltd. | Method and apparatus for collectively sampling a plurality of gaseous phases in desired proportions for gas analysis or other purposes |
| US4199545A (en) * | 1975-08-20 | 1980-04-22 | Thagard Technology Company | Fluid-wall reactor for high temperature chemical reaction processes |
| US4119406A (en) * | 1976-05-06 | 1978-10-10 | Miles Laboratories, Inc. | Calibration apparatus |
| DE2621677A1 (de) * | 1976-05-15 | 1977-11-24 | Bayer Ag | Verfahren zur ueberpruefung von gasanalysengeraeten |
| US4234543A (en) * | 1978-10-30 | 1980-11-18 | Thagard Technology Company | Fluid-wall reactor for high temperature chemical reaction processes |
| US4237093A (en) * | 1978-12-27 | 1980-12-02 | Phillips Petroleum Company | Hydrocarbon cracking |
| US4414858A (en) * | 1982-03-22 | 1983-11-15 | Westinghouse Electric Corp. | Steam turbine fluid sampling apparatus |
| US4958295A (en) * | 1986-05-21 | 1990-09-18 | Hercules Incorporated | Analyzing apparatus and method for analysis of liquid samples |
| US4977093A (en) * | 1986-11-03 | 1990-12-11 | Liquid Air Corporation | Process for analyzing carbonyl sulfide in a gas |
| US5080867A (en) * | 1988-04-07 | 1992-01-14 | Liquid Air Corporation | Portable carbonyl sulfide analyzer |
| US5102805A (en) * | 1989-11-16 | 1992-04-07 | Amoco Corporation | Method for detecting the presence and concentration of weak acids and bases in liquids |
| US5110744A (en) * | 1989-11-16 | 1992-05-05 | Amoco Corporation | Method for process control |
| WO2001034290A2 (en) | 1999-11-09 | 2001-05-17 | Sri International | Array for generating combinatorial libraries |
| US7033840B1 (en) | 1999-11-09 | 2006-04-25 | Sri International | Reaction calorimeter and differential scanning calorimeter for the high-throughput synthesis, screening and characterization of combinatorial libraries |
| US9400266B2 (en) * | 2013-03-14 | 2016-07-26 | Rosemount Analytical Inc. | Gas chromatograph with improved operation |
| US9746450B2 (en) * | 2014-04-15 | 2017-08-29 | Rosemount Analytical Inc. | Online gas chromatograph operation with reduced usage of calibration gas |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3172730A (en) * | 1965-03-09 | Method and apparatus for the determination | ||
| US1908202A (en) * | 1930-04-01 | 1933-05-09 | Du Pont | Determination of carbon monoxide in a gas mixture |
| US3226197A (en) * | 1962-07-13 | 1965-12-28 | Martin Sweets Company Inc | Method and apparatus for determining c14 |
| US3304159A (en) * | 1963-01-28 | 1967-02-14 | Hewlett Packard Co | Gas chromatographic analysis method for c, h, and n content in solid organic compounds |
| US3410663A (en) * | 1965-03-29 | 1968-11-12 | Gen Electric | Thermoparticulate detection of explosives |
| US3425807A (en) * | 1965-04-15 | 1969-02-04 | Hewlett Packard Co | Pyrolysis system |
| US3455655A (en) * | 1965-06-01 | 1969-07-15 | Mine Safety Appliances Co | Detection of missile fuels in gas atmosphere |
| US3466228A (en) * | 1967-02-28 | 1969-09-09 | Tennessee Corp | Method for determining minor quantity of strong acid in major quantity of weak acid |
-
1968
- 1968-07-22 US US746487A patent/US3607073A/en not_active Expired - Lifetime
-
1971
- 1971-04-16 DE DE19712118539 patent/DE2118539A1/de active Pending
- 1971-04-24 GB GB1126071*[A patent/GB1304796A/en not_active Expired
- 1971-05-10 NL NL7106353A patent/NL7106353A/xx unknown
- 1971-05-13 FR FR7117289A patent/FR2137088B1/fr not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2008067296A3 (en) * | 2006-11-29 | 2008-09-18 | Schlumberger Services Petrol | Microfluidic gas chromatography system architecture |
Also Published As
| Publication number | Publication date |
|---|---|
| US3607073A (en) | 1971-09-21 |
| FR2137088A1 (enrdf_load_stackoverflow) | 1972-12-29 |
| FR2137088B1 (enrdf_load_stackoverflow) | 1978-06-02 |
| NL7106353A (enrdf_load_stackoverflow) | 1972-11-14 |
| GB1304796A (enrdf_load_stackoverflow) | 1973-01-31 |
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