DE117009C - - Google Patents
Info
- Publication number
- DE117009C DE117009C DENDAT117009D DE117009DA DE117009C DE 117009 C DE117009 C DE 117009C DE NDAT117009 D DENDAT117009 D DE NDAT117009D DE 117009D A DE117009D A DE 117009DA DE 117009 C DE117009 C DE 117009C
- Authority
- DE
- Germany
- Prior art keywords
- lead
- carbonate
- sugar
- saturated
- carbonic acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 229910000003 Lead carbonate Inorganic materials 0.000 claims description 10
- BVKZGUZCCUSVTD-UHFFFAOYSA-N Carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 claims description 5
- DSLZVSRJTYRBFB-LLEIAEIESA-L D-glucarate(2-) Chemical compound [O-]C(=O)[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O DSLZVSRJTYRBFB-LLEIAEIESA-L 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims description 2
- 238000000746 purification Methods 0.000 claims description 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims 4
- 238000000034 method Methods 0.000 claims 3
- 229960003563 Calcium Carbonate Drugs 0.000 claims 2
- 229910000019 calcium carbonate Inorganic materials 0.000 claims 2
- 150000007513 acids Chemical class 0.000 claims 1
- 230000008929 regeneration Effects 0.000 claims 1
- 238000011069 regeneration method Methods 0.000 claims 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate dianion Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 3
- 239000003513 alkali Substances 0.000 description 3
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 235000015450 Tilia cordata Nutrition 0.000 description 2
- 235000011941 Tilia x europaea Nutrition 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 239000004571 lime Substances 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N carbon dioxide Chemical class O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B35/00—Extraction of sucrose from molasses
- C13B35/02—Extraction of sucrose from molasses by chemical means
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Description
KAISERLICHESIMPERIAL
PATENTAMT.PATENT OFFICE.
PATENTSCHRIFTPATENT LETTERING
M 117009 KLASSE 89 h. M 117009 CLASS 89 h.
Patentirt im Deutschen Reiche vom 27. März 1900 ab.Patented in the German Empire on March 27, 1900.
Beim "Bleisaccharat-Verfahren auf nassem Wege mittelst Bleicarbonat und Alkali ist es von Vortheil, das Bleicarbonat möglichst mit Kohlensäure gesättigt anzuwenden.With the "lead saccharate method on wet By means of lead carbonate and alkali, it is advantageous to use lead carbonate as well as possible Use saturated carbon dioxide.
Wird Bleisaccharat . mit Kohlensäure behandelt, so wird zuerst der Zucker frei gemacht und ist lange schon vollständig in Lösung, bevor das Bleicarbonat gesättigt ist. Bei dem letzten Theil der Saturation gehen dann nach dem Zucker organische und anorganische Verunreinigungen heraus, welche das Filtriren des Carbonats und die Verarbeitung der erhaltenen Zuckerlösung erschweren.Becomes lead saccharate. Treated with carbonic acid, the sugar is first released and is completely in solution long before the lead carbonate is saturated. In the last part of saturation, organic and inorganic follow the sugar Impurities, which the filtration of the carbonate and the processing complicate the obtained sugar solution.
Wir haben gefunden, dafs sich der Vortheil . eines hochgesättigten Bleicarbonats erzielen läfst, ohne die Reinheit der erhaltenen Zuckerlösung zu beeinträchtigen, wenn man die Saturation theilt, also zunächst, wie früher (vgl. Patentschrift 85024, Seite 3) beschrieben, gerade bis zum vollständigen Freiwerden des Zuckers saturirt, das Carbonat durch Filtriren und Auswaschen vom Zucker befreit, mit viel Wasser aufrührt und — am besten in der Wärme — mit Kohlensäure bis zur Sättigung behandelt. Dabei werden auch die durch Wasser allein nicht völlig zersetzlichen Doppelverbindungen des Bleicarbonats mit Alkali zersetzt und das Alkali in Lösung übergeführt, was insbesondere für die Wiederbenutzung des aus der Lauge gefällten Bleicarbonats in Betracht kommt.We have found the advantage. of a highly saturated lead carbonate runs without affecting the purity of the sugar solution obtained, if one has the saturation divides, so initially, as described earlier (see patent specification 85024, page 3), straight until the sugar is completely free, the carbonate is saturated by filtration and washing, freed from the sugar, stirred up with plenty of water and - ideally in the Heat - carbonated to saturation. The Water alone does not decompose completely decomposable double compounds of lead carbonate with alkali and the alkali converted into solution, which is particularly important for the reuse of the lead carbonate precipitated from the liquor comes into consideration.
Mit dieser Nachsaturation läfst sich zweckmäfsig eine Reinigung des Bleicarbonats von aufgenommenem kohlensaurem Kalk verbinden, indem man allmählich während der Zuführung der Kohlensäure einen Ueberschufs der auf den vorhandenen kohlensauren Kalk berechneten Menge Salzsäure oder einer anderen Säure verdünnt zugiebt; dabei geht Blei, nur spurenweise in Lösung.This post-saturation can be expedient Connect a purification of the lead carbonate of ingested carbonate of lime by gradually increasing during the feeding the carbonic acid an excess of that calculated on the existing carbonic acid lime Diluted amount of hydrochloric acid or another acid is added; this goes lead, only traces in solution.
Claims (2)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE117009C true DE117009C (en) |
Family
ID=386310
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT117009D Active DE117009C (en) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE117009C (en) |
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0
- DE DENDAT117009D patent/DE117009C/de active Active
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