DE102006010075B4 - Verfahren zur Herstellung von im Dentalbereich einsetzbaren Kunststoffformteilen - Google Patents
Verfahren zur Herstellung von im Dentalbereich einsetzbaren Kunststoffformteilen Download PDFInfo
- Publication number
- DE102006010075B4 DE102006010075B4 DE102006010075A DE102006010075A DE102006010075B4 DE 102006010075 B4 DE102006010075 B4 DE 102006010075B4 DE 102006010075 A DE102006010075 A DE 102006010075A DE 102006010075 A DE102006010075 A DE 102006010075A DE 102006010075 B4 DE102006010075 B4 DE 102006010075B4
- Authority
- DE
- Germany
- Prior art keywords
- initiator
- component
- polymerization
- cuvette
- injection
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000000034 method Methods 0.000 title claims abstract description 47
- 230000008569 process Effects 0.000 title claims abstract description 19
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- 238000010137 moulding (plastic) Methods 0.000 title description 4
- 239000003999 initiator Substances 0.000 claims abstract description 51
- 238000002347 injection Methods 0.000 claims abstract description 18
- 239000007924 injection Substances 0.000 claims abstract description 18
- 239000004033 plastic Substances 0.000 claims abstract description 11
- 229920003023 plastic Polymers 0.000 claims abstract description 11
- 238000005204 segregation Methods 0.000 claims abstract description 4
- 239000000463 material Substances 0.000 claims description 28
- 229920000642 polymer Polymers 0.000 claims description 25
- 239000012190 activator Substances 0.000 claims description 12
- 239000011324 bead Substances 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 9
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 8
- 238000005538 encapsulation Methods 0.000 claims description 4
- 239000003112 inhibitor Substances 0.000 claims 1
- 238000002360 preparation method Methods 0.000 abstract description 4
- 239000000306 component Substances 0.000 description 40
- 238000006116 polymerization reaction Methods 0.000 description 38
- 239000000178 monomer Substances 0.000 description 23
- 239000000203 mixture Substances 0.000 description 20
- 238000001723 curing Methods 0.000 description 12
- 230000008901 benefit Effects 0.000 description 7
- 239000000945 filler Substances 0.000 description 7
- 150000002978 peroxides Chemical class 0.000 description 7
- 238000001816 cooling Methods 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 238000003860 storage Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 230000000977 initiatory effect Effects 0.000 description 3
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 3
- 230000008961 swelling Effects 0.000 description 3
- VNQXSTWCDUXYEZ-UHFFFAOYSA-N 1,7,7-trimethylbicyclo[2.2.1]heptane-2,3-dione Chemical compound C1CC2(C)C(=O)C(=O)C1C2(C)C VNQXSTWCDUXYEZ-UHFFFAOYSA-N 0.000 description 2
- OZAIFHULBGXAKX-UHFFFAOYSA-N 2-(2-cyanopropan-2-yldiazenyl)-2-methylpropanenitrile Chemical compound N#CC(C)(C)N=NC(C)(C)C#N OZAIFHULBGXAKX-UHFFFAOYSA-N 0.000 description 2
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- OMPJBNCRMGITSC-UHFFFAOYSA-N Benzoylperoxide Chemical compound C=1C=CC=CC=1C(=O)OOC(=O)C1=CC=CC=C1 OMPJBNCRMGITSC-UHFFFAOYSA-N 0.000 description 2
- 239000004908 Emulsion polymer Substances 0.000 description 2
- YIVJZNGAASQVEM-UHFFFAOYSA-N Lauroyl peroxide Chemical compound CCCCCCCCCCCC(=O)OOC(=O)CCCCCCCCCCC YIVJZNGAASQVEM-UHFFFAOYSA-N 0.000 description 2
- 235000019400 benzoyl peroxide Nutrition 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 229930006711 bornane-2,3-dione Natural products 0.000 description 2
- 239000002775 capsule Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 229920001577 copolymer Polymers 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000011159 matrix material Substances 0.000 description 2
- 210000003739 neck Anatomy 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 238000010526 radical polymerization reaction Methods 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- XMAWUPHYEABFDR-UHFFFAOYSA-N 1,2-bis(4-chlorophenyl)ethane-1,2-dione Chemical compound C1=CC(Cl)=CC=C1C(=O)C(=O)C1=CC=C(Cl)C=C1 XMAWUPHYEABFDR-UHFFFAOYSA-N 0.000 description 1
- YNANGXWUZWWFKX-UHFFFAOYSA-N 1,2-bis(4-methoxyphenyl)ethane-1,2-dione Chemical compound C1=CC(OC)=CC=C1C(=O)C(=O)C1=CC=C(OC)C=C1 YNANGXWUZWWFKX-UHFFFAOYSA-N 0.000 description 1
- PTZRYAAOQPNAKU-UHFFFAOYSA-N 2-[(1-carboxy-3-cyanobutyl)diazenyl]-4-cyanopentanoic acid Chemical compound N#CC(C)CC(C(O)=O)N=NC(C(O)=O)CC(C)C#N PTZRYAAOQPNAKU-UHFFFAOYSA-N 0.000 description 1
- JUVSRZCUMWZBFK-UHFFFAOYSA-N 2-[n-(2-hydroxyethyl)-4-methylanilino]ethanol Chemical compound CC1=CC=C(N(CCO)CCO)C=C1 JUVSRZCUMWZBFK-UHFFFAOYSA-N 0.000 description 1
- YDIYEOMDOWUDTJ-UHFFFAOYSA-N 4-(dimethylamino)benzoic acid Chemical compound CN(C)C1=CC=C(C(O)=O)C=C1 YDIYEOMDOWUDTJ-UHFFFAOYSA-N 0.000 description 1
- QSJXEFYPDANLFS-UHFFFAOYSA-N Diacetyl Chemical group CC(=O)C(C)=O QSJXEFYPDANLFS-UHFFFAOYSA-N 0.000 description 1
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical class CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 1
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 description 1
- 244000028419 Styrax benzoin Species 0.000 description 1
- 235000000126 Styrax benzoin Nutrition 0.000 description 1
- 235000008411 Sumatra benzointree Nutrition 0.000 description 1
- 150000001252 acrylic acid derivatives Chemical class 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 150000004982 aromatic amines Chemical class 0.000 description 1
- 229960005070 ascorbic acid Drugs 0.000 description 1
- 235000010323 ascorbic acid Nutrition 0.000 description 1
- 239000011668 ascorbic acid Substances 0.000 description 1
- 125000000751 azo group Chemical group [*]N=N[*] 0.000 description 1
- 229940125717 barbiturate Drugs 0.000 description 1
- HNYOPLTXPVRDBG-UHFFFAOYSA-N barbituric acid Chemical compound O=C1CC(=O)NC(=O)N1 HNYOPLTXPVRDBG-UHFFFAOYSA-N 0.000 description 1
- 229960002130 benzoin Drugs 0.000 description 1
- -1 benzoin ethers Chemical class 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 239000003479 dental cement Substances 0.000 description 1
- 239000011350 dental composite resin Substances 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- ISAOCJYIOMOJEB-UHFFFAOYSA-N desyl alcohol Natural products C=1C=CC=CC=1C(O)C(=O)C1=CC=CC=C1 ISAOCJYIOMOJEB-UHFFFAOYSA-N 0.000 description 1
- LSXWFXONGKSEMY-UHFFFAOYSA-N di-tert-butyl peroxide Chemical compound CC(C)(C)OOC(C)(C)C LSXWFXONGKSEMY-UHFFFAOYSA-N 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 235000019382 gum benzoic Nutrition 0.000 description 1
- 238000001746 injection moulding Methods 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 150000001451 organic peroxides Chemical class 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229920003229 poly(methyl methacrylate) Polymers 0.000 description 1
- 239000004848 polyfunctional curative Substances 0.000 description 1
- 239000004926 polymethyl methacrylate Substances 0.000 description 1
- 230000002028 premature Effects 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000003847 radiation curing Methods 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 239000012966 redox initiator Substances 0.000 description 1
- 230000000754 repressing effect Effects 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- BUUPQKDIAURBJP-UHFFFAOYSA-N sulfinic acid Chemical compound OS=O BUUPQKDIAURBJP-UHFFFAOYSA-N 0.000 description 1
- GJBRNHKUVLOCEB-UHFFFAOYSA-N tert-butyl benzenecarboperoxoate Chemical compound CC(C)(C)OOC(=O)C1=CC=CC=C1 GJBRNHKUVLOCEB-UHFFFAOYSA-N 0.000 description 1
- BWSZXUOMATYHHI-UHFFFAOYSA-N tert-butyl octaneperoxoate Chemical compound CCCCCCCC(=O)OOC(C)(C)C BWSZXUOMATYHHI-UHFFFAOYSA-N 0.000 description 1
- 150000003512 tertiary amines Chemical class 0.000 description 1
- 229920001169 thermoplastic Polymers 0.000 description 1
- 239000012815 thermoplastic material Substances 0.000 description 1
- 229920001187 thermosetting polymer Polymers 0.000 description 1
- 239000004416 thermosoftening plastic Substances 0.000 description 1
- 230000001960 triggered effect Effects 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- SXPUVBFQXJHYNS-UHFFFAOYSA-N α-furil Chemical compound C=1C=COC=1C(=O)C(=O)C1=CC=CO1 SXPUVBFQXJHYNS-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K6/00—Preparations for dentistry
- A61K6/80—Preparations for artificial teeth, for filling teeth or for capping teeth
- A61K6/884—Preparations for artificial teeth, for filling teeth or for capping teeth comprising natural or synthetic resins
- A61K6/887—Compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S525/00—Synthetic resins or natural rubbers -- part of the class 520 series
- Y10S525/902—Core-shell
Landscapes
- Health & Medical Sciences (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Plastic & Reconstructive Surgery (AREA)
- Epidemiology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Dental Preparations (AREA)
- Graft Or Block Polymers (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102006010075A DE102006010075B4 (de) | 2006-03-04 | 2006-03-04 | Verfahren zur Herstellung von im Dentalbereich einsetzbaren Kunststoffformteilen |
| PCT/EP2007/051975 WO2007099158A2 (de) | 2006-03-04 | 2007-03-02 | Material zur herstellung von im dentalbereich einsetzbaren kunststoffformteilen |
| EP16163084.3A EP3090724B1 (de) | 2006-03-04 | 2007-03-02 | Verfahren zur herstellung von dentalprothesen |
| EP07712418.8A EP1991197B1 (de) | 2006-03-04 | 2007-03-02 | Material zur herstellung von im dentalbereich einsetzbaren kunststoffformteilen |
| US12/224,699 US8067482B2 (en) | 2006-03-04 | 2007-03-02 | Material for producing plastic molded parts that can be used in the field of dentistry |
| JP2008557726A JP5455378B2 (ja) | 2006-03-04 | 2007-03-02 | 歯科分野で使用可能なプラスチック成形部材を製造するための材料 |
| EP16163080.1A EP3090723B1 (de) | 2006-03-04 | 2007-03-02 | Verfahren zur herstellung von dentalprothesen |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102006010075A DE102006010075B4 (de) | 2006-03-04 | 2006-03-04 | Verfahren zur Herstellung von im Dentalbereich einsetzbaren Kunststoffformteilen |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE102006010075A1 DE102006010075A1 (de) | 2007-09-06 |
| DE102006010075B4 true DE102006010075B4 (de) | 2010-01-28 |
Family
ID=38316649
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE102006010075A Expired - Fee Related DE102006010075B4 (de) | 2006-03-04 | 2006-03-04 | Verfahren zur Herstellung von im Dentalbereich einsetzbaren Kunststoffformteilen |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US8067482B2 (https=) |
| EP (3) | EP3090724B1 (https=) |
| JP (1) | JP5455378B2 (https=) |
| DE (1) | DE102006010075B4 (https=) |
| WO (1) | WO2007099158A2 (https=) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102007032836A1 (de) * | 2007-07-12 | 2009-01-15 | Evonik Röhm Gmbh | Emulsionspolymerisat enthaltend Aktivatoren, Verfahren zu dessen Herstellung sowie dessen Verwendung in Zwei- oder Mehrkomponentensystemen |
| DE102008056293A1 (de) | 2008-11-07 | 2010-09-02 | Retec Kunststofftechnik Gmbh | Polymerisierbares Mehrkomponenten-Prothesenausgangsmaterial, insbesondere für Dentalprothesen |
| DE102009029786B3 (de) | 2009-06-18 | 2010-09-30 | Heraeus Kulzer Gmbh | Behälter enthaltend den PMMA-Pulveranteil eines Zweikomponentensystems aus PMMA-Pulverkomponente und MMA-Monomerkomponente sowie Verwendungen derartiger Behälter |
| ES2723399T3 (es) | 2015-09-28 | 2019-08-27 | Coltene/Whaledent Ag | Procedimiento para producir bloques odontológicos de material compuesto |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1544924A1 (de) * | 1965-10-22 | 1969-07-24 | Bayer Ag | Verfahren zur Herstellung von zahnaerztlichem Reparaturmaterial |
| DE19841342A1 (de) * | 1998-09-10 | 2000-04-20 | Merck Patent Gmbh | Neue Reaktivsysteme aus polymerisierbaren Monomeren , die Peroxide und stabilisierten Boralkylverbindungen enthalten |
| DE10137968A1 (de) * | 2001-08-08 | 2003-03-06 | Roehm Gmbh | Depot-Polymerisationsstarter-Perlen |
| DE10339329A1 (de) * | 2003-08-25 | 2005-03-24 | Röhm GmbH & Co. KG | Monomer - Polymer-Systeme mit steuerbarer Topfzeit |
| DE10355992A1 (de) * | 2003-11-27 | 2005-06-30 | Curasan Ag | Bioresorbierbares Kompositmaterial |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE940493C (de) | 1952-12-06 | 1956-03-22 | Bayer Ag | Verfahren zur Herstellung von geformten Koerpern, insbesondere Zahnprothesen |
| DE2408640A1 (de) | 1973-03-02 | 1974-09-12 | Dentsply Int Inc | Acrylpolymermischungen |
| DE2312934C3 (de) * | 1973-03-15 | 1980-01-24 | Et. Dentaire Ivoclar, Schaan (Liechtenstein) | Verfahren und Vorrichtung zur Herstellung von Dentalprothesen aus Kunststoff |
| DE2403211C3 (de) | 1974-01-23 | 1981-12-24 | Etablissement Dentaire Ivoclar, Schaan | Werkstoff für Dentalzwecke |
| US4284551A (en) * | 1979-11-30 | 1981-08-18 | American Dental Association Health Foundation | Tertiary aromatic amine accelerators derived from para-aminophenethanol |
| JPH04187609A (ja) * | 1990-11-22 | 1992-07-06 | Nikkiso Co Ltd | 歯科用複合材料 |
| US5154762A (en) * | 1991-05-31 | 1992-10-13 | Minnesota Mining And Manufacturing Company | Universal water-based medical and dental cement |
| DE19706064C2 (de) | 1997-02-17 | 1999-04-08 | Schmidt Karl Heinz Dr | Plastische aushärtbare Einkomponentenmasse, insbesondere zur Herstellung von Zahnprothesen |
| US6605651B1 (en) * | 1998-09-09 | 2003-08-12 | Biomat Sciences, Inc. | Curing methods and material compositions having dental and other applications |
| DE19919581A1 (de) | 1999-04-29 | 2000-11-02 | Espe Dental Ag | Dentalmaterialien, Verfahren zu ihrer Aushärtung und deren Verwendung |
| DE19941829A1 (de) | 1999-09-02 | 2001-03-15 | Voco Gmbh | Autopolymerisierende Dentalzusammensetzung und ihre Verwendung |
| JP2004010529A (ja) * | 2002-06-06 | 2004-01-15 | Kazuo Okuma | 歯科用充填材料および歯科用合着材料として用いられる材料 |
| US7393493B2 (en) * | 2003-02-27 | 2008-07-01 | A Enterprises, Inc. | Crosslinkable polymeric materials and their applications |
| JP2005289961A (ja) * | 2004-03-12 | 2005-10-20 | Shiyoufuu:Kk | 微小カプセルを含有する硬化性組成物 |
-
2006
- 2006-03-04 DE DE102006010075A patent/DE102006010075B4/de not_active Expired - Fee Related
-
2007
- 2007-03-02 JP JP2008557726A patent/JP5455378B2/ja not_active Expired - Fee Related
- 2007-03-02 EP EP16163084.3A patent/EP3090724B1/de active Active
- 2007-03-02 EP EP16163080.1A patent/EP3090723B1/de active Active
- 2007-03-02 US US12/224,699 patent/US8067482B2/en active Active
- 2007-03-02 WO PCT/EP2007/051975 patent/WO2007099158A2/de not_active Ceased
- 2007-03-02 EP EP07712418.8A patent/EP1991197B1/de active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1544924A1 (de) * | 1965-10-22 | 1969-07-24 | Bayer Ag | Verfahren zur Herstellung von zahnaerztlichem Reparaturmaterial |
| DE19841342A1 (de) * | 1998-09-10 | 2000-04-20 | Merck Patent Gmbh | Neue Reaktivsysteme aus polymerisierbaren Monomeren , die Peroxide und stabilisierten Boralkylverbindungen enthalten |
| DE10137968A1 (de) * | 2001-08-08 | 2003-03-06 | Roehm Gmbh | Depot-Polymerisationsstarter-Perlen |
| DE10339329A1 (de) * | 2003-08-25 | 2005-03-24 | Röhm GmbH & Co. KG | Monomer - Polymer-Systeme mit steuerbarer Topfzeit |
| DE10355992A1 (de) * | 2003-11-27 | 2005-06-30 | Curasan Ag | Bioresorbierbares Kompositmaterial |
Also Published As
| Publication number | Publication date |
|---|---|
| US20090036612A1 (en) | 2009-02-05 |
| WO2007099158A3 (de) | 2008-03-13 |
| EP3090724A1 (de) | 2016-11-09 |
| EP3090724B1 (de) | 2018-09-12 |
| DE102006010075A1 (de) | 2007-09-06 |
| EP3090723A1 (de) | 2016-11-09 |
| EP3090723B1 (de) | 2018-12-12 |
| JP2009529021A (ja) | 2009-08-13 |
| WO2007099158A2 (de) | 2007-09-07 |
| JP5455378B2 (ja) | 2014-03-26 |
| EP1991197A2 (de) | 2008-11-19 |
| US8067482B2 (en) | 2011-11-29 |
| EP1991197B1 (de) | 2016-09-21 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OP8 | Request for examination as to paragraph 44 patent law | ||
| 8364 | No opposition during term of opposition | ||
| R119 | Application deemed withdrawn, or ip right lapsed, due to non-payment of renewal fee | ||
| R079 | Amendment of ipc main class |
Free format text: PREVIOUS MAIN CLASS: A61K0006083000 Ipc: A61K0006887000 |