CS253554B2 - Method of 2-alkoxy-4,6-dichloro-s-triazines preparation - Google Patents
Method of 2-alkoxy-4,6-dichloro-s-triazines preparation Download PDFInfo
- Publication number
- CS253554B2 CS253554B2 CS797566A CS756679A CS253554B2 CS 253554 B2 CS253554 B2 CS 253554B2 CS 797566 A CS797566 A CS 797566A CS 756679 A CS756679 A CS 756679A CS 253554 B2 CS253554 B2 CS 253554B2
- Authority
- CS
- Czechoslovakia
- Prior art keywords
- cyanuric chloride
- liquid
- sprayed
- reactant
- dichloro
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 13
- 238000002360 preparation method Methods 0.000 title claims description 5
- 239000007788 liquid Substances 0.000 claims abstract description 34
- MGNCLNQXLYJVJD-UHFFFAOYSA-N cyanuric chloride Chemical compound ClC1=NC(Cl)=NC(Cl)=N1 MGNCLNQXLYJVJD-UHFFFAOYSA-N 0.000 claims abstract description 20
- 238000002156 mixing Methods 0.000 claims abstract description 19
- 239000002253 acid Substances 0.000 claims abstract description 11
- 239000000376 reactant Substances 0.000 claims abstract description 11
- 239000011230 binding agent Substances 0.000 claims abstract description 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 9
- 239000000460 chlorine Substances 0.000 claims description 3
- QPJDMGCKMHUXFD-UHFFFAOYSA-N cyanogen chloride Chemical compound ClC#N QPJDMGCKMHUXFD-UHFFFAOYSA-N 0.000 claims description 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 2
- 229910052801 chlorine Inorganic materials 0.000 claims description 2
- HPXRVTGHNJAIIH-UHFFFAOYSA-N cyclohexanol Chemical compound OC1CCCCC1 HPXRVTGHNJAIIH-UHFFFAOYSA-N 0.000 claims description 2
- 239000011261 inert gas Substances 0.000 claims description 2
- 238000002844 melting Methods 0.000 claims description 2
- 230000008018 melting Effects 0.000 claims description 2
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 claims 1
- 230000003247 decreasing effect Effects 0.000 claims 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 abstract description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 5
- 210000000481 breast Anatomy 0.000 abstract 1
- 230000036632 reaction speed Effects 0.000 abstract 1
- 239000007921 spray Substances 0.000 description 14
- 230000015572 biosynthetic process Effects 0.000 description 9
- 238000005755 formation reaction Methods 0.000 description 9
- 239000002904 solvent Substances 0.000 description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- 239000000243 solution Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 239000000370 acceptor Substances 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 238000005507 spraying Methods 0.000 description 3
- BWZVCCNYKMEVEX-UHFFFAOYSA-N 2,4,6-Trimethylpyridine Chemical compound CC1=CC(C)=NC(C)=C1 BWZVCCNYKMEVEX-UHFFFAOYSA-N 0.000 description 2
- 229910052684 Cerium Inorganic materials 0.000 description 2
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 description 2
- 150000007530 organic bases Chemical class 0.000 description 2
- 239000012074 organic phase Substances 0.000 description 2
- WLJWJOQWLPAHIE-YLXLXVFQSA-N (2s)-2-[[(2s)-2-[[(2s)-2-[[(2s,3s)-2-amino-3-methylpentanoyl]amino]propanoyl]amino]-3-methylbutanoyl]amino]pentanedioic acid Chemical compound CC[C@H](C)[C@H](N)C(=O)N[C@@H](C)C(=O)N[C@@H](C(C)C)C(=O)N[C@H](C(O)=O)CCC(O)=O WLJWJOQWLPAHIE-YLXLXVFQSA-N 0.000 description 1
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
- 229920001651 Cyanoacrylate Polymers 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- MWCLLHOVUTZFKS-UHFFFAOYSA-N Methyl cyanoacrylate Chemical compound COC(=O)C(=C)C#N MWCLLHOVUTZFKS-UHFFFAOYSA-N 0.000 description 1
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 229910001514 alkali metal chloride Inorganic materials 0.000 description 1
- 229910000318 alkali metal phosphate Inorganic materials 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- HOPRXXXSABQWAV-UHFFFAOYSA-N anhydrous collidine Natural products CC1=CC=NC(C)=C1C HOPRXXXSABQWAV-UHFFFAOYSA-N 0.000 description 1
- 210000000436 anus Anatomy 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 125000001309 chloro group Chemical group Cl* 0.000 description 1
- UTBIMNXEDGNJFE-UHFFFAOYSA-N collidine Natural products CC1=CC=C(C)C(C)=N1 UTBIMNXEDGNJFE-UHFFFAOYSA-N 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- XLJMAIOERFSOGZ-UHFFFAOYSA-M cyanate Chemical compound [O-]C#N XLJMAIOERFSOGZ-UHFFFAOYSA-M 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 125000001033 ether group Chemical group 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 125000005843 halogen group Chemical group 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hcl hcl Chemical compound Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 235000020095 red wine Nutrition 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- GFYHSKONPJXCDE-UHFFFAOYSA-N sym-collidine Natural products CC1=CN=C(C)C(C)=C1 GFYHSKONPJXCDE-UHFFFAOYSA-N 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
- B01J10/02—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor of the thin-film type
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2850339A DE2850339C2 (de) | 1978-11-20 | 1978-11-20 | Verfahren zur Herstellung von 2-Alkoxy-4,6-dichlor-s-triazinen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CS253554B2 true CS253554B2 (en) | 1987-11-12 |
Family
ID=6055173
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CS797566A CS253554B2 (en) | 1978-11-20 | 1979-11-06 | Method of 2-alkoxy-4,6-dichloro-s-triazines preparation |
Country Status (22)
| Country | Link |
|---|---|
| US (1) | US4271299A (ro) |
| JP (1) | JPS5573665A (ro) |
| AT (1) | AT368139B (ro) |
| BE (1) | BE880142A (ro) |
| BR (1) | BR7907284A (ro) |
| CA (1) | CA1101861A (ro) |
| CH (1) | CH642640A5 (ro) |
| CS (1) | CS253554B2 (ro) |
| DD (1) | DD147103A5 (ro) |
| DE (1) | DE2850339C2 (ro) |
| ES (1) | ES483876A1 (ro) |
| FR (1) | FR2441619A1 (ro) |
| GB (1) | GB2036736B (ro) |
| HU (1) | HU184070B (ro) |
| IL (1) | IL58606A (ro) |
| IN (1) | IN153839B (ro) |
| IT (1) | IT1119156B (ro) |
| NL (1) | NL7908438A (ro) |
| RO (1) | RO79414A (ro) |
| SE (1) | SE447252B (ro) |
| YU (1) | YU172279A (ro) |
| ZA (1) | ZA796282B (ro) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5229513A (en) * | 1992-09-17 | 1993-07-20 | General Electric Company | Method for preparing substituted dichlorotriazines |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE558354A (ro) * | 1956-06-15 | |||
| US3198797A (en) * | 1960-04-12 | 1965-08-03 | Geigy Chem Corp | 2, 4-dichloro-6-dialkylhydroxy-anilino-1, 3, 5-triazines |
| FR1534235A (fr) * | 1966-08-11 | 1968-07-26 | Bayer Ag | Procédé de préparation d'une suspension aqueuse neutre de chlorure de cyanuryle exempte de solvants |
| DD111378A5 (ro) * | 1973-06-27 | 1975-02-12 | ||
| RO70804A (ro) * | 1974-11-20 | 1980-08-15 | Deutsche Gold-Und Silber-Scheideanstalt Vormals Roessler,De | Procedeu si dispozitiv pentru prepararea unor solutii sau suspensii de clorura de cianuril |
-
1978
- 1978-11-20 DE DE2850339A patent/DE2850339C2/de not_active Expired
-
1979
- 1979-07-16 YU YU01722/79A patent/YU172279A/xx unknown
- 1979-08-14 IT IT68672/79A patent/IT1119156B/it active
- 1979-08-29 IN IN90/CAL/79A patent/IN153839B/en unknown
- 1979-09-04 ES ES483876A patent/ES483876A1/es not_active Expired
- 1979-10-25 DD DD79216460A patent/DD147103A5/de unknown
- 1979-11-01 IL IL58606A patent/IL58606A/xx unknown
- 1979-11-06 CS CS797566A patent/CS253554B2/cs unknown
- 1979-11-09 BR BR7907284A patent/BR7907284A/pt unknown
- 1979-11-13 GB GB7939170A patent/GB2036736B/en not_active Expired
- 1979-11-15 US US06/094,479 patent/US4271299A/en not_active Expired - Lifetime
- 1979-11-19 BE BE6/47016A patent/BE880142A/fr not_active IP Right Cessation
- 1979-11-19 AT AT0735379A patent/AT368139B/de not_active IP Right Cessation
- 1979-11-19 NL NL7908438A patent/NL7908438A/nl not_active Application Discontinuation
- 1979-11-19 HU HU79DE1025A patent/HU184070B/hu unknown
- 1979-11-19 CH CH1030579A patent/CH642640A5/de not_active IP Right Cessation
- 1979-11-19 SE SE7909570A patent/SE447252B/sv not_active IP Right Cessation
- 1979-11-19 CA CA340,148A patent/CA1101861A/en not_active Expired
- 1979-11-20 ZA ZA00796282A patent/ZA796282B/xx unknown
- 1979-11-20 FR FR7928610A patent/FR2441619A1/fr active Granted
- 1979-11-20 JP JP14963279A patent/JPS5573665A/ja active Pending
- 1979-11-20 RO RO7999287A patent/RO79414A/ro unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DE2850339C2 (de) | 1981-02-26 |
| BR7907284A (pt) | 1980-07-15 |
| IN153839B (ro) | 1984-08-18 |
| ATA735379A (de) | 1982-01-15 |
| FR2441619B1 (ro) | 1983-06-24 |
| GB2036736B (en) | 1983-03-09 |
| IT1119156B (it) | 1986-03-03 |
| US4271299A (en) | 1981-06-02 |
| AT368139B (de) | 1982-09-10 |
| FR2441619A1 (fr) | 1980-06-13 |
| GB2036736A (en) | 1980-07-02 |
| DE2850339B1 (de) | 1980-06-12 |
| CH642640A5 (de) | 1984-04-30 |
| ZA796282B (en) | 1980-11-26 |
| HU184070B (en) | 1984-06-28 |
| YU172279A (en) | 1983-12-31 |
| ES483876A1 (es) | 1980-04-16 |
| CA1101861A (en) | 1981-05-26 |
| RO79414A (ro) | 1982-06-25 |
| BE880142A (fr) | 1980-05-19 |
| SE447252B (sv) | 1986-11-03 |
| NL7908438A (nl) | 1980-05-22 |
| SE7909570L (sv) | 1980-05-21 |
| IL58606A0 (en) | 1980-02-29 |
| IL58606A (en) | 1984-02-29 |
| IT7968672A0 (it) | 1979-08-14 |
| JPS5573665A (en) | 1980-06-03 |
| DD147103A5 (de) | 1981-03-18 |
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