CS241545B2 - Method of s-(thiophosphoryl)-thioglycol acid's bromides production - Google Patents
Method of s-(thiophosphoryl)-thioglycol acid's bromides production Download PDFInfo
- Publication number
- CS241545B2 CS241545B2 CS280184A CS280184A CS241545B2 CS 241545 B2 CS241545 B2 CS 241545B2 CS 280184 A CS280184 A CS 280184A CS 280184 A CS280184 A CS 280184A CS 241545 B2 CS241545 B2 CS 241545B2
- Authority
- CS
- Czechoslovakia
- Prior art keywords
- bromides
- thiophosphoryl
- production
- ppm
- temperature
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 7
- 150000001649 bromium compounds Chemical class 0.000 title description 3
- 239000002253 acid Substances 0.000 title description 2
- 238000004519 manufacturing process Methods 0.000 title description 2
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims description 9
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 6
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 claims description 6
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 6
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical group ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 claims description 6
- 239000000010 aprotic solvent Substances 0.000 claims description 4
- CCGKOQOJPYTBIH-UHFFFAOYSA-N ethenone Chemical compound C=C=O CCGKOQOJPYTBIH-UHFFFAOYSA-N 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 2
- 239000003208 petroleum Substances 0.000 claims description 2
- CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 description 7
- 239000002904 solvent Substances 0.000 description 6
- -1 2-dimethylpropoxythiophosphorylthioglycolic acid Chemical compound 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 239000011541 reaction mixture Substances 0.000 description 3
- 229920006395 saturated elastomer Polymers 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 150000002576 ketones Chemical class 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000010183 spectrum analysis Methods 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- CWERGRDVMFNCDR-UHFFFAOYSA-N thioglycolic acid Chemical compound OC(=O)CS CWERGRDVMFNCDR-UHFFFAOYSA-N 0.000 description 2
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical group [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical group [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical group [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Chemical group BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
- 229910052794 bromium Chemical group 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 125000005842 heteroatom Chemical group 0.000 description 1
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical class [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 235000011007 phosphoric acid Nutrition 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Chemical group 0.000 description 1
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL24149183A PL137160B1 (en) | 1983-04-14 | 1983-04-14 | Process for preparing bromides of -s-/dialkoxythiophosphoryl/-thioglycolic acid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CS241545B2 true CS241545B2 (en) | 1986-03-13 |
Family
ID=20016635
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CS280184A CS241545B2 (en) | 1983-04-14 | 1984-04-12 | Method of s-(thiophosphoryl)-thioglycol acid's bromides production |
Country Status (6)
| Country | Link |
|---|---|
| BG (1) | BG42357A3 (ro) |
| CS (1) | CS241545B2 (ro) |
| DD (1) | DD217521A5 (ro) |
| IN (1) | IN158583B (ro) |
| PL (1) | PL137160B1 (ro) |
| RO (1) | RO89405A (ro) |
-
1983
- 1983-04-14 PL PL24149183A patent/PL137160B1/pl unknown
-
1984
- 1984-04-12 CS CS280184A patent/CS241545B2/cs unknown
- 1984-04-13 DD DD26197284A patent/DD217521A5/de unknown
- 1984-04-13 BG BG065086A patent/BG42357A3/xx unknown
- 1984-04-14 RO RO84114259A patent/RO89405A/ro unknown
- 1984-04-19 IN IN254/CAL/84A patent/IN158583B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| IN158583B (ro) | 1986-12-13 |
| BG42357A3 (en) | 1987-11-14 |
| RO89405A (ro) | 1986-06-30 |
| PL241491A1 (en) | 1984-10-22 |
| DD217521A5 (de) | 1985-01-16 |
| PL137160B1 (en) | 1986-05-31 |
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