CN88100041A - The method that turmeric series products is produced - Google Patents
The method that turmeric series products is produced Download PDFInfo
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- CN88100041A CN88100041A CN 88100041 CN88100041A CN88100041A CN 88100041 A CN88100041 A CN 88100041A CN 88100041 CN88100041 CN 88100041 CN 88100041 A CN88100041 A CN 88100041A CN 88100041 A CN88100041 A CN 88100041A
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Abstract
The present invention is to be main raw material with ecological turmeric, is processing medium with water, the novel method of disposable continuous separation and Extraction turmeric component.The present invention does not need a large amount of organic solvents and main equipment, has replaced the old technology method of organic solvent extraction pigment, has the low consumption of joint money, safe and simple, comprehensive utilization, the various advantage of product.Can produce the Nantural non-toxic of aspects such as being suitable for food, medicine, light industry, free of contamination turmeric toner, pigment, starch, bright volatilization wet goods product simultaneously.Enforcement of the present invention with promoting the coordination of the plantation of turmeric producing region, processing, has remarkable economic efficiency and vast market.
Description
The invention belongs to the processing method that turmeric series products is produced.
Turmeric series products is meant turmeric starch, toner, fresh ginger butter and refining pigment product etc.Be applicable to the aspects such as seasoning, dyeing and medical light industry of food.
Since food, medicine, light industry both at home and abroad develop rapidly and human to self healthy attention and to the heavy demand of Nantural non-toxic, free of contamination seasonings, foodstuff additive, cosmetic material and medical material, stimulated the rapid expansion of turmeric cultivated area and the increase of output.But the post-production of turmeric still belongs to traditional technology at present.After promptly the fresh ginger Huang being processed as the rhizoma zingiberis Huang, further be processed into curcuma powder, medicinal extract, pigment, volatilization wet goods product by application person again by the grower, the rhizoma zingiberis Huang be processed as manual operations, the curcuma powder that common so-called turmeric spices is the broken gained of rhizoma zingiberis bloom.Also have to make liquid with propylene glycol or ethanol extracting after turmeric worn into powder, makes medicinal extract or orange-yellow crystallization through concentrating.With behind the rhizoma zingiberis bloom mill, again through vacuum distillation recovered solvent, oven drying at low temperature makes turmeric paste and is used for the dyeing of can orange juice again with the ethanol extracting as Foochow canning factory.The processing mode of institute's summation in " aromatic seasoning " literary composition is shown by Japan too Tian Jinghang, also is after earlier aquatic foods being expected drying and crushing, adopts the method for water distillation or organic solvent extraction to extract flavouring ingredient again.Therefore, the technical process of known turmeric post-production is as follows:
1. rhizoma zingiberis is yellow concocts:
→ wash naughty removal of impurities → boiling → solarization dry dry → arrangement →
2 use processing:
Above-mentioned post-production technology is divided into two sections processes: the yellow labour intensity of concocting of rhizoma zingiberis is big; Production cycle is long; Because boiling makes starch pasting; Light constituent partial loss in the volatile oil is dried when dry in solarization.The extraction of using pigment in the processing is a physical properties of utilizing its alcohol molten, adopts organic extraction process of siccative; Volatile oil further loss in the production process of medicinal extract; Organic solvent extractions such as sherwood oil are generally adopted in degreasing; In the production process of medicinal extract, pigment, because the use of a large amount of organic solvents, facility investment is big, cost is high and operate dangerous; Because the gelatinization of starch brings difficulty for the extraction of pigment, volatile oil; Contain a large amount of spirit-soluble resin class things in medicinal extract, pigment product, also give the refining certain difficulty of bringing of curcumine, and the loss of turmeric component is many, comprehensive utilization is few, and product is dull and can not satisfy service requirements.
In order to overcome the above problems, it is the disposable continuous separation-extraction technology process of main raw material that the present invention changes the post-production process of turmeric with ecological turmeric into; It is main adopting water-soluble Jie's technology to extract pigment, double other component of carrying.Its operational path is: with ecological turmeric (the fresh ginger Huang that comprises the yellow and dehydration of fresh ginger) be main raw material, also available rhizoma zingiberis Huang (therefrom can not propose starch), through the elutriation removal of impurities, grinding gets slip, through filter wash separate turmeric starch; Molten through soaking again, sedimentation, filtration etc. operate the turmeric toner; Soak slag and get fresh ginger butter (the yellow rhizoma zingiberis butter that gets of rhizoma zingiberis) through steam distillation; From distillation residue, also can produce the turmeric Mierocrystalline cellulose; The sedimentation waste liquid can further fully utilize; The turmeric toner is made with extra care.Can produce the product of pigment, pigment and SILVER REAGENT curcumine.Its technical process is as scheming:
The present invention realizes through the following steps:
1. the preparation of charge pulp and starch separate:
Ecological turmeric is removed the earth foreign material through elutriation, and with the pigment mill, material-water ratio is 1: 1～10, and properties of powder performace is in 0.01～1mm scope, carries out under normal temperature to 50 ℃, and the gained charge pulp is for the polycomponent separation and Extraction; Charge pulp after separating, starch is got thick starch and gumming slip.
The producing and decolour of 2 turmeric starch:
Thick starch is got yellow turmeric starch through washing, dry (in room temperature to 60 ℃ scope); Thick starch is decoloured in destainer, and destainer is 0.1～10% strong basicity hydroxide aqueous solution, can be potassium hydroxide or sodium hydroxide; The destainer consumption to be comparatively fast decolouring and be convenient to degree of being operating as, bleaching temperature between room temperature to 50 ℃, again through washing, dry (in room temperature to 60 ℃ scope), white turmeric starch.
The gumming slip soak molten:
The gumming slip is added water adjust material-water ratio 1: 1～10, add oxyhydroxide (for highly basic such as sodium hydroxide or potassium hydroxide) then and soak moltenly, the oxyhydroxide consumption is 0.1～10% of a raw material weight; Temperature is in room temperature to 50 ℃ scope; Soaking the molten time is 4～12 hours; Be interrupted and stir,, get immersion liquid after filtration and soak slag so that pigment is dissolved in the aqueous solution.
4. the producing of turmeric toner in the immersion liquid:
In immersion liquid, add muriate and carry out sedimentation.The muriate that adds is salt and acid, and salt is sodium, the nontoxic chlorinated thing of potassium plasma type edibility; Acid is hydrochloric acid.The salt consumption is 5～30% of raw material; The acid consumption is degree so that the PH of immersion liquid equals 5～7; Settling temperature is room temperature to 90 a ℃ scope, and the settling time is 1～10 hour; Leave standstill,, must precipitate after filtration so that the sedimentation of dissolved pigment is separated out, again through washing, dry (temperature be room temperature to 90 ℃), pulverize (granularity for≤0.1mm), the turmeric toner.
5. the turmeric toner is refining:
Toner with edible alcohols dissolving, is expected that the agent ratio is 1: 1～10, and extraction temperature is room temperature to 78 a ℃ scope, removes alcohol insoluble solids, gets turmeric yellow I type.As foodstuff flavouring, dyeing and serial spicy yellow pigment raw material; Toner is removed pungent, alcohol insoluble solids, get turmeric yellow II type, as dyeing and serial flavored type yellow pigment raw materials such as food-drink, makeup; Pigment, II type are liquid type product, if re-refine, can get the SILVER REAGENT curcumine.
6. soak the extraction of fresh ginger butter in the slag:
Soak slag and add water to adjust material-water ratio be 1: 3～10, put in the steam distillation device under 100～110 ℃ of temperature, water distillation 4～24 hours, soaking slag solution, to transfer PH be 7～8, soaks volatile oil in the slag with recovery.Light oil gets the fresh ginger butter in the collection phegma.
7. extract the turmeric robust fibre:
Distillation residue are through repeatedly washing, and temperature can be in room temperature to 110 ℃ scope, and drying gets the turmeric robust fibre again.
Principal feature of the present invention is that 1. the course of processing is disposable successive processes, adopts water-soluble Jie's technology to extract the producing and manufacturing technique of series product such as turmeric starch, toner, fresh ginger butter.2. be the water-based solvating agent of pigment, be the water-based sinking agent of pigment with the muriate with strong basicity oxyhydroxide.3. volatile oil extracts the raw materials used slag that soaks after extracting through starch, toner that is.4. the purified product turmeric yellow I of toner, the II type pigment content of making thinner for the edibility alcohols is the liquid type product of prescribed value.Because with ecological turmeric is raw material, comprehensive utilization rationally, the materials of effective ingredients loss is little.Adopt water-soluble Jie's technology to avoid the pollution of organic solvent to starch, toner, bright wet goods product, product has higher inner quality and wider range of application.Basic product kind of the present invention and uses thereof sees Table one.
Enforcement of the present invention will provide a large amount of Nantural non-toxics free of contamination turmeric series products for society; Promote the production of producing region plantation and processing to coordinate, the economic benefit that improves the producing region is had positive effect.Utilize the present invention, implement frock can soil can the ocean; Low energy, easy to operate and safe, with short production cycle; Cost is low, comprehensive utilization, product is various and easy to use.Enforcement of the present invention will further promote the deep development of zingiberaceous plant and starch, fruit juice, volatile oil plant, implements frock and has versatility.
The turmeric yellow I of novel process and old technology medicinal extract production cost of products relatively see Table two.
Pigment is 2: 3 with the production cost ratio of medicinal extract, and pigment I is that liquid type product can directly use; Medicinal extract could use after also need adding the alcohol dissolving.Novel process has and pay to produce starch～200 kilogram in addition, and bright oil does not count economic benefit for 20 kilograms.
Foochow canning factory is 0.035 gram/kilogram with the consumption that medicinal extract dyes orange juice, then is 0.04 gram/kilogram with pigment I; The dyeing of 1 ton of orange juice is 5.25 yuan (if the medicinal extract price is 150 yuan/kilogram) with the cost of medicinal extract, and is 4.00 yuan (are 100 yuan/kilogram as if the pigment price) with pigment I.This shows, adopt new technology, develop turmeric series products, will improve the economic benefit of turmeric greatly.
The invention will be further described below in conjunction with embodiment:
Embodiment 1:
Half-dried ecological turmeric, clear water are soaked to rise and get 1000 grams after cleaning, and add water 1500 grams, and grinding becomes granularity 0.1～1mm slip, filter wash in 100 eye mesh screens adds water 1000 gram filter washes again, and filtrate goes out to precipitate through settlement separate, washing is once dried down for 50 ℃, gets yellow turmeric starch 38 grams.
Gumming liquid mixes with screenings, adds water 1000 gram (material-water ratio 1: 3.5), adds sodium hydrate solid 20 grams, stirs molten back room temperature cold soaking 8 hours, is interrupted and stirs, filter immersion liquid and soak slag; Add sodium-chlor 100 grams in immersion liquid, drips 1: 1 hydrochloric acid and transfer solution PH to equal 6, room temperature leaves standstill, incline to supernatant liquor and leach precipitation and press dry, less than 60 ℃ of oven dry down, turmeric toner 24 restrains.
Soak slag and add water 4000 and restrain and in water distilling apparatus, carried out steam distillation 10 hours, treat that not having oil substantially distillates, take out volatile oil in separator top, fresh ginger butter 4 grams.
Robust fibre 20 grams are dried, got to distillation residue through washing repeatedly.
Get turmeric toner 10 grams with 95% ethanol 50ml thermosol under little boiling, with the filtrate evaporate to dryness, get turmeric yellow I 4.3 grams after the heat filter.
Bright material extraction yield: turmeric starch (Huang) 3.8%; Turmeric toner 2.4%(pigment: 1.03%); Fresh ginger butter 0.4%; Robust fibre 2%.
Embodiment 2:
Bright attitude turmeric is cleaned back 1400 grams and wears into bright thick slurry 2000 grams with pigment, slurry granularity 0.01～1mm, add water 2000 and restrain filter wash on 100 mesh sieves, add 1000 gram washing filters more once, merge that washing filtrate is settlement separate to go out thick starch slurry, adding 0.5% sodium hydroxide solution 500ml, to stir the back settlement separate, takes out washing of precipitate three times, grind in oven dry below 60 ℃, get white turmeric starch 45 grams.
Mixed pulp wash heat filtrate (material-water ratio is 1: 3～4) adds sodium hydroxide 25 grams, stir to leave standstill the room temperature cold soaking 12 hours after molten, after the filtration immersion liquid and soak slag; Add sodium-chlor 250 grams in immersion liquid, concentrated hydrochloric acid transfers PH to equal 5, heat 50 ℃ after standing demix, press dry after collecting bottom precipitation washing once, 60 ℃ down oven dry grind, turmeric toner 33 restrains.
To soak slag and add sedimentation liquid 3000 grams, in water distilling apparatus, carry out steam distillation, not have oil droplet substantially in 8 hours, collect volatile oil in the separator, get fresh ginger butter 5.5 grams.
Press dry after the distillation residue water washing repeatedly, robust fibre 160 grams must wet.
Get turmeric toner 10 grams, after refining, get pigment 3 grams.
Bright material extraction yield: starch (in vain) 3.2%; Toner 2.35%(pigment: 0.7%); Bright oil 0.39%; Robust fibre (wetting) 11%.
Embodiment 3:
1. take a sample after analytical test is composed as follows greater than the turmeric toner mixing of 5 extractions: pigment: 3.85%; Alcohol leachable: 22.2%; Ash content: 4.6%; Arsenic: 0.4PPm; Plumbous: 1PPm.
2. turmeric starch sanitary index: arsenic: 0.5PPm, lead: 1ppm.
3. fresh ginger butter: proportion (20 ℃)=0.9178～0.9108
Refractive index (20 ℃)=1.5049 ± 40
Specific optical rotation (sodium lamp, 20 ℃)=-20 °～-40 °
Claims (8)
1, a kind of processing method of turmeric series products production.It is characterized in that water as processing medium, adopt grinding to separate, soak molten, sedimentation, water distil process process, the processing method of disposable continuous separation and Extraction turmeric starch, toner, volatile oil and refining pigment product from turmeric.
2, method according to claim 1, its operational path are characterised in that the order of disposable continuous separation and Extraction component is followed successively by starch, toner, volatile oil.
3, it is that pigment soaks molten medium that method according to claim 1, its pigment are soaked molten being characterised in that with the strong basicity hydroxide aqueous solution, and the oxyhydroxide consumption is 0.1～10% of a turmeric weight.
4, method according to claim 1, its toner settling characteristics are that with the edibility muriate be sinking agent, and its consumption is 5～30% of a turmeric weight.
5, method according to claim 4, the settled another feature of its toner is to add hydrochloric acid in immersion liquid, and its consumption equals 5～7 degree of being to regulate the immersion liquid pH value.
6, it is raw material that method according to claim 1, its volatile oil are extracted the slag that soaks that is characterised in that with having extracted behind starch, the toner, and the ph value of mixture that is distilled is adjusted in 7～8 scopes.
7, method according to claim 1 is characterised in that by the refining pigment of toner adopting the edibility alcohols is thinner; Material agent ratio is 1: 1～10.
8, method according to claim 1, white turmeric starch are produced and are characterised in that destainer is 0.1～10% sodium hydroxide or potassium hydroxide aqueous solution with the decolouring of strong basicity hydroxide aqueous solution.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 88100041 CN88100041A (en) | 1988-01-04 | 1988-01-04 | The method that turmeric series products is produced |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 88100041 CN88100041A (en) | 1988-01-04 | 1988-01-04 | The method that turmeric series products is produced |
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| Publication Number | Publication Date |
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| CN88100041A true CN88100041A (en) | 1988-09-07 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN 88100041 Pending CN88100041A (en) | 1988-01-04 | 1988-01-04 | The method that turmeric series products is produced |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1103375C (en) * | 2000-12-18 | 2003-03-19 | 华中农业大学 | Process for extracting glucose from waste hydrolyzed liquid of yam and refining it |
| CN108359019A (en) * | 2018-01-18 | 2018-08-03 | 大连豪翔生物酶工程有限公司 | A kind of method of the integrated extraction of multiple biological activities ingredient in turmeric |
-
1988
- 1988-01-04 CN CN 88100041 patent/CN88100041A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1103375C (en) * | 2000-12-18 | 2003-03-19 | 华中农业大学 | Process for extracting glucose from waste hydrolyzed liquid of yam and refining it |
| CN108359019A (en) * | 2018-01-18 | 2018-08-03 | 大连豪翔生物酶工程有限公司 | A kind of method of the integrated extraction of multiple biological activities ingredient in turmeric |
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