CN2715826Y - Multipurpose ultrasonic countercurrent circulating immersing and extracting device - Google Patents
Multipurpose ultrasonic countercurrent circulating immersing and extracting device Download PDFInfo
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- CN2715826Y CN2715826Y CN 200420084394 CN200420084394U CN2715826Y CN 2715826 Y CN2715826 Y CN 2715826Y CN 200420084394 CN200420084394 CN 200420084394 CN 200420084394 U CN200420084394 U CN 200420084394U CN 2715826 Y CN2715826 Y CN 2715826Y
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Abstract
A multipurpose ultrasonic backflow circulating leaching equipment of the utility model not only can be used for quick abstracting various effective components of animals and plants under the normal temperature and the low temperature, but also can be used for any other multipurpose of the ultrasonic mixing, the ultrasonic dispersal, the ultrasonic emulsification, ultrasonic strengthening reaction, etc. The utility model comprises an abstracting tank. A mixing shaft is arranged in the middle part of the abstracting tank, the upper end of the mixing shaft is connected with a shaft connector and a motor, and a guide mixing oar and a baffle plate are connected to the mixing shaft. Circulating connection pipes are arranged on the periphery of the abstracting tank. The lower end of each circulating connection pipe is communicated with the outlet of the lower side wall of the tank, and the upper part of each circulating connection pipe is communicated with the inlet of the upper side wall of the tank. Power-collecting type ultrasonic variable-amplitude rods are arranged in the circulating connection pipes. Because the circulating connection pipes are arranged on the periphery of the tank, the material in the tank is repeatedly passed through the ultrasonic field in the circulating connection pipe in the backflow, and thus the availability ratio of the ultrasonic field is greatly raised. The abstracting device can satisfy the requirements of various laboratories, pilot test and large scale industrialized production.
Description
Technical field
The utility model relates to ultrasonic wave extraction equipment technical field, is a kind of ultrasonic circulated in countercurrent leaching device of multipurpose that is applicable to.
Background technology
The animals and plants effective medicinal components overwhelming majority is a product in the cell, and the animals and plants effective medicinal components is fully extracted from animal and plant cells, is the basis that Chinese medicine is produced.At present, the conventional extracting method of domestic animals and plants effective medicinal components mainly contains diacolation and stirring and boils method such as put forward, and exists shortcomings such as recovery rate is low, time length, destructible medicinal ingredient (particularly thermal sensitivity composition) activity, energy consumption height mostly.
In recent years, ultrasonic disruption strengthen to extract with advantages such as its low temperature, quick, high yield, obtains people's approval day by day, and purposes is also increasingly extensive, according to statistics, has nearly 200 kinds of medicine prepared in laboratory to record hyperacoustic application in latest edition " pharmacopeia ".But because the ultrasonic field of ultrasonic wave extraction is concentrated, effective range is little, is difficult to engineering and amplifies, and for many years, ultrasound-enhanced extraction only limits to a small amount of extraction at intermittence on a small scale in laboratory scale, has limited hyperacoustic range of application greatly.
The application study of intensified by ultrasonic wave extractive technique in large-scale production in nearly 2 years is deep day by day, domestic some ultrasonic waves that use for suitability for industrialized production that occurred successively extract equipment, as: Yixing Ai Kang drugmaker improved ultrasonic wave traditional Chinese medicine extraction device (notification number is 1440739); The ultrasonic extractor of serialization adverse current (notification number is 2582599) and the ultrasonic wave traditional Chinese medicine extraction jar (notification number 2530639) of inventions such as Jining, Shandong Bai Zhongming; The shake ultrasonic wave multifunction extracting device (notification number 2551313) of state company of Ningbo; The ultrasonic wave extractor (notification number 2546069) of Shandong Rui Yang drugmaker invention; The ultrasonic wave extraction system (application number is 02100522.2) that the solid-liquid of Pueraria lobota Guia Hill, Shanghai invention extracts etc.Above ultrasonic wave extraction element is ultrasonic transducer to be placed in the middle of the big extractor or be installed on the big extraction tank skin a plurality of ultrasonic oscillators are objective mostly, because the ultrasonic field sphere of action is concentrated, effective range is little, ultrasonic field cavitation effect and other effect effective range concentrate on around immersion transducer or the ultrasonic oscillator, be difficult to guarantee that all materials can both pass through the ultrasonic field useful effect in the big extractor, the ultrasonic field effective rate of utilization is low, and extraction effect is difficult to guarantee.Though serialization adverse current ultrasonic wave natural drug extractor combines counter-flow extraction and ultrasound-enhanced extraction, because not circulation is difficult to guarantee the ultrasound-enhanced extraction effect of large-scale production equipment.
Summary of the invention
The purpose of this utility model provides the ultrasonic circulated in countercurrent leaching device of a kind of multipurpose, it is little at ultrasonic echography field action scope, be difficult to the shortcoming that engineering is amplified, to existing large-scale ultrasonic extraction equipment existing problems, adopt the engineering amplifying technique, by controlling Flow of Goods and Materials with the many circulation pipe designs of peculiar adverse current, the energy gathering type ultrasonic transducer rationally is distributed in each thin circulation pipe, extract material and can both circulate reverse to guarantee all by effective ultrasonic field, thereby improve extraction effect greatly, the advanced extractive technique of circulated in countercurrent extraction and intensified by ultrasonic wave is combined, to satisfy industrialization production needs rapidly and efficiently.
For achieving the above object, the utility model is taked following design:
The ultrasonic circulated in countercurrent leaching device of a kind of multipurpose, it includes the extraction tank body, be provided with charge door and window at the tank body top, be provided with drain hole in tank base, it is characterized in that: the middle part in the described extraction tank body is provided with a shaft, the top that tank body is stretched out in the upper end of this shaft is connected with motor with shaft joint, and the lower end of shaft is arranged in the axle head positioning sleeve, is connected with at least one secondary guiding stirring arm on shaft; Around the extraction tank body, be provided with at least one circulation tube connector, the lower end of every circulation tube connector is communicated with the outlet of the lower wall of tank body, the top of every circulation tube connector is communicated with the upper side wall of tank body inlet, is provided with energy-gathered ultrasonic luffing bar in circulation pipe.
Be connected with at least one truncated cone-shaped deflector on the inwall of described tank body, described guiding stirring arm is arranged on the shaft of truncated cone-shaped deflector bottom, is connected with circle or pyramid type baffle plate on the plate axle stirring of described guiding stirring arm top.
Described extraction tank body inner bottom part one side is provided with the steam heated hole, and the upper side wall of circulation tube connector is provided with form.
In circulation pipe, be provided with energy-gathered ultrasonic luffing bar, temperature sensor.
Be connected with the tube connector of cold cycling pump on the chuck on the tank body; The liquid level tube connector that also has the long-pending indicating graduation of at least one belt body in the tank body outside.
During use, the extraction material input of fluid is extracted in the tank body, drive at the motor shaft under the effect of guiding stirring arm, material is upwards flowed in the circulation tube connector by the extractor bottom, material flows from lower to upper in circulation pipe, be arranged on the energy-gathered ultrasonic luffing bar in the circulation tube connector, in circulation pipe, produce ultrasonic field from top to bottom, when material flows through the circulation tube connector from bottom to top, thereby can guarantee the material that extracts can both be reverse by effective ultrasonic wave effect, then improved extraction effect greatly.Flow back in the extraction tank body by tank body upper side wall inlet after the effect of material process ultrasonic field, again by of the effect of truncated cone-shaped deflector with the guiding stirring arm, making the material that stirs continue to survey wall outlet by the extractor bottom upwards flows in the circulation tube connector, form the ultrasonic extraction of another reverse circulation, reach the purpose of the ultrasonic extraction of circulated in countercurrent, thereby can improve extraction effect greatly, to satisfy need of industrial production.
The utility model has the advantages that: the ultrasonic circulated in countercurrent extraction element of this multipurpose has solved extraction material that present large-scale ultrasonic extraction equipment exists can not ultrasonic fully effective fragmentation, the ultrasonic field utilization rate is low, the defective that ultrasonic extraction effect is difficult to guarantee, angle from the engineering amplification, provide a kind of high-quality and high-efficiency to strengthen extraction equipment for the ultrasonic circulated in countercurrent that suitability for industrialized production is used, this equipment is applied widely, can satisfy the extraction of the animal and plant cells active ingredient of using volatility and non-volatile extraction medium, extraction efficiency height, extract purity height.This device adopts the design of guiding stirring arm and truncated cone-shaped deflector and circulation tube connector, spent material can be constantly by the extractor bottom circulation tube connector of upwards flowing through, by in the circulation tube connector, adding the energy gathering type ultrasonic amplitude transformer, thereby guaranteed ultrasonic intensity; In circulation pipe, produce ultrasonic field from top to bottom, material reverse flow from lower to upper passes through ultrasonic field, then strengthened ultrasound-enhanced extraction effect greatly, move in circles the flow continuous reverse circulation of feed liquid make whole extractor of material flows through ultrasonic field in the circulation pipe, thereby has improved the utilization rate of ultrasonic field among a small circle greatly.This extraction element is the combination of circulated in countercurrent extraction and ultrasound-enhanced extraction, can satisfy need of industrial production.
Description of drawings
Fig. 1 is a structural representation of the present utility model
The specific embodiment
Referring to shown in Figure 1: the ultrasonic circulated in countercurrent leaching device of a kind of multipurpose, it includes extracts tank body 7, be provided with charge door 13 and window 3 at tank body 7 tops, be provided with drain hole 14 in tank body 7 bottoms, middle part in described extraction tank body 7 is provided with a shaft 15, the top that tank body 7 is stretched out in the upper end of this shaft 15 is connected with motor 1 with shaft joint 2, and the lower end of shaft 15 is arranged in the axle head positioning sleeve 12, is connected with three secondary guiding stirring arms 11 on shaft 15; Extract tank body 7 around be provided with two (or more than two) circulation tube connectors 8, the lower end of every circulation tube connector 8 is communicated with the lower wall outlet 16 of tank body 7, the top of every circulation tube connector 8 is communicated with the upper side wall inlet 17 of tank body 7, inserts in circulation pipe 8 and is provided with energy-gathered ultrasonic luffing bar 5 and temperature sensor 22.
Uniformly on the inwall of described tank body 7 be connected with three truncated cone-shaped deflectors 9, first top truncated cone-shaped deflector is arranged on the bottom of sidewall inlet 17, make the material that enters tank body by circulation tube connector 8 flow to the middle part of tank body along truncated cone-shaped deflector 9, its effect is to make guiding stirring arm 11 can carry out all even sufficient stirring material; Described guiding stirring arm 11 is arranged on the shaft of truncated cone-shaped deflector 9 bottoms, is connected with circular baffle plate 10 (or pyramid type baffle plate) on the shaft on described guiding stirring arm top, and the effect of this circular baffle plate 10 is to prevent that material from flowing backwards; By the stirring material of basipetal three secondary guiding stirring arms 11 and the effects of three truncated cone-shaped deflectors 9, material is stirred after, enter in the circulation tube connector 8 from the lower wall outlet 16 of tank body, carry out the ultrasonic extraction of reverse circulation repeatedly.
Be provided with the steam heated hole in extraction tank body 7 inner bottom parts one side, be used to add thermal material and use; The upper side wall of circulation tube connector 8 is provided with form 4, is used to observe the Flow of Goods and Materials situation.
This ultrasonic circulated in countercurrent extraction element has steam heated hole 6, hydro-peening head 18, and the pneumatic slag dumping drain hole 14 of turnover plate type, can conveniently carry out blowing, heat up and the cleaning and sterilizing processing, easy to use, this device adopts the energy gathering type ultrasonic amplitude transformer bar, can guarantee ultrasound intensity.
Be connected with the tube connector 21 of cold cycling pump on the chuck 19 on the tank body, can in chuck 19, import circulating cooling liquid or circulation hydrothermal by tube connector 21 as required, the material in the tank body is carried out cooling fluid or heating; Also have the liquid level tube connector 22 of the long-pending indicating graduation of at least one belt body in the tank body outside, it is used to connect liquid level tube usefulness, to show the state of material in tank.
Owing to around tank body, be provided with the many circulation tube connectors that have the energy gathering type ultrasonic amplitude transformer bar, make the material that stirs in the tank body repeatedly adverse current through the ultrasound field in the circulation tube connector, material is carried out ultrasound-enhanced extraction, thereby improved the utilization rate of ultrasonic field among a small circle greatly.The circulated in countercurrent extraction of this extraction element and the combination of ultrasound-enhanced extraction can be satisfied industrialization production needs rapidly and efficiently.Not only can be used for the normal temperature and the low temperature rapid extraction of various active ingredients such as animals and plants, but also can be used for other multiple uses such as ultrasonic mixing, dispersion, emulsification and ultrasound-enhanced reaction,
Claims (5)
1, the ultrasonic circulated in countercurrent leaching device of a kind of multipurpose, it includes the extraction tank body, chuck, be provided with charge door and window at the tank body top, be provided with drain hole in tank base, it is characterized in that: the middle part in the described extraction tank body is provided with a shaft, and the top that tank body is stretched out in the upper end of this shaft is connected with motor with shaft joint, the lower end of shaft is arranged in the axle head positioning sleeve, is connected with at least one secondary guiding stirring arm on shaft; Around the extraction tank body, be provided with at least one circulation tube connector, the lower end of every circulation tube connector is communicated with the outlet of the lower wall of tank body, the top of every circulation tube connector is communicated with the upper side wall of tank body inlet, is provided with energy-gathered ultrasonic luffing bar in circulation pipe.
2, the ultrasonic circulated in countercurrent leaching device of multipurpose according to claim 1, it is characterized in that: be connected with at least one truncated cone-shaped deflector on the inwall of described tank body, described guiding stirring arm is arranged on the shaft of truncated cone-shaped deflector bottom, is connected with circle or pyramid type baffle plate on the plate axle stirring of described guiding stirring arm top.
3, the ultrasonic circulated in countercurrent leaching device of multipurpose according to claim 1 is characterized in that: described extraction tank body inner bottom part one side is provided with the steam heated hole, and the upper side wall of circulation tube connector is provided with form.
4, the ultrasonic circulated in countercurrent leaching device of multipurpose according to claim 1 is characterized in that: be provided with temperature sensor in circulation pipe.
5, the ultrasonic circulated in countercurrent leaching device of multipurpose according to claim 1 is characterized in that: the tube connector that is connected with the cold cycling pump on the chuck on the tank body; The liquid level tube connector that also has the long-pending indicating graduation of at least one belt body in the tank body outside.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200420084394 CN2715826Y (en) | 2004-08-24 | 2004-08-24 | Multipurpose ultrasonic countercurrent circulating immersing and extracting device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200420084394 CN2715826Y (en) | 2004-08-24 | 2004-08-24 | Multipurpose ultrasonic countercurrent circulating immersing and extracting device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN2715826Y true CN2715826Y (en) | 2005-08-10 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200420084394 Expired - Lifetime CN2715826Y (en) | 2004-08-24 | 2004-08-24 | Multipurpose ultrasonic countercurrent circulating immersing and extracting device |
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| Country | Link |
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| CN (1) | CN2715826Y (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100431653C (en) * | 2004-08-24 | 2008-11-12 | 北京弘祥隆生物技术开发有限公司 | Multipurpose ultrasonic backflow circulating leaching equipment |
| CN103007866A (en) * | 2011-09-28 | 2013-04-03 | 中国石油化工股份有限公司 | Agitation reactor |
| CN105194902A (en) * | 2015-10-19 | 2015-12-30 | 成都健腾生物技术有限公司 | Percolating tank and heat percolating extraction system |
| CN108687669A (en) * | 2018-05-10 | 2018-10-23 | 太原理工大学 | A kind of liquid circulating apparatus of ultrasonic cavitation auxiliary stirring Magnetorheologicai polishing liquid |
-
2004
- 2004-08-24 CN CN 200420084394 patent/CN2715826Y/en not_active Expired - Lifetime
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100431653C (en) * | 2004-08-24 | 2008-11-12 | 北京弘祥隆生物技术开发有限公司 | Multipurpose ultrasonic backflow circulating leaching equipment |
| CN103007866A (en) * | 2011-09-28 | 2013-04-03 | 中国石油化工股份有限公司 | Agitation reactor |
| CN105194902A (en) * | 2015-10-19 | 2015-12-30 | 成都健腾生物技术有限公司 | Percolating tank and heat percolating extraction system |
| CN108687669A (en) * | 2018-05-10 | 2018-10-23 | 太原理工大学 | A kind of liquid circulating apparatus of ultrasonic cavitation auxiliary stirring Magnetorheologicai polishing liquid |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| AV01 | Patent right actively abandoned |
Effective date of abandoning: 20081112 |
|
| C25 | Abandonment of patent right or utility model to avoid double patenting |