CN219963972U - A circulation distillation purification device for acetate feed additive production - Google Patents
A circulation distillation purification device for acetate feed additive production Download PDFInfo
- Publication number
- CN219963972U CN219963972U CN202321368990.5U CN202321368990U CN219963972U CN 219963972 U CN219963972 U CN 219963972U CN 202321368990 U CN202321368990 U CN 202321368990U CN 219963972 U CN219963972 U CN 219963972U
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- China
- Prior art keywords
- electric heating
- heating rod
- feed additive
- purification device
- additive production
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- 238000004821 distillation Methods 0.000 title claims abstract description 58
- 238000000746 purification Methods 0.000 title claims abstract description 26
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 title claims abstract description 20
- 239000003674 animal food additive Substances 0.000 title claims abstract description 20
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 20
- 238000005485 electric heating Methods 0.000 claims abstract description 63
- 238000010438 heat treatment Methods 0.000 claims abstract description 28
- 125000004122 cyclic group Chemical group 0.000 claims description 10
- 238000004321 preservation Methods 0.000 claims description 5
- 230000003068 static effect Effects 0.000 claims description 2
- 230000009286 beneficial effect Effects 0.000 abstract description 3
- 238000003756 stirring Methods 0.000 abstract description 3
- 238000001704 evaporation Methods 0.000 abstract description 2
- 230000008020 evaporation Effects 0.000 abstract description 2
- 238000009413 insulation Methods 0.000 description 3
- 238000009835 boiling Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 230000017525 heat dissipation Effects 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- SXRSQZLOMIGNAQ-UHFFFAOYSA-N Glutaraldehyde Chemical compound O=CCCCC=O SXRSQZLOMIGNAQ-UHFFFAOYSA-N 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000010977 unit operation Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model relates to a circulating distillation purification device for acetate feed additive production, which relates to the field of distillation technical equipment and comprises a distillation kettle, wherein a heating mechanism is arranged in the distillation kettle and comprises an electric heating wire, a supporting component and an electric heating rod, the electric heating wire is uniformly arranged on the inner wall of the distillation kettle, the electric heating rod is connected with the supporting component, the supporting component is used for supporting the electric heating rod, and the electric heating rod is positioned in a cavity of the distillation kettle; the utility model has the beneficial effects that the electric heating wires and the electric heating rods are arranged in the distillation kettle, so that the solution in the distillation kettle is heated in multiple directions, the solution is heated more uniformly, the evaporation efficiency of the solution is improved, the rotating piece and the supporting frame are arranged, the rotation of the electric heating rods is realized, the stirring of the solution is realized while the position of the electric heating rods is continuously changed, and the phenomenon of uneven heating of the solution is further reduced.
Description
Technical Field
The utility model relates to the technical field of distillation equipment, in particular to a circulating distillation purification device for acetate feed additive production.
Background
Distillation is a thermodynamic separation process that utilizes the difference in boiling points of the components of a mixed liquid or liquid-solid system to vaporize the lower boiling components and recondensing to separate the entire components, a combination of both the vaporizing and condensing unit operations. Compared with other separation means, such as extraction, filtration crystallization, etc., it has the advantage that no other solvents than the system components are required, thereby ensuring that no new impurities are introduced.
Related prior art discloses glutaraldehyde purifying devices, which include a distiller body, a movable block, a circulation pump, and a movable assembly; the distiller body is provided with a discharge hole and a mounting groove, and the movable block is movably mounted on the distiller body
In the mounting groove, be equipped with the spread groove in the movable block, the spread groove communicates with the discharge gate, movable block upper end fixed mounting has the connecting pipe, the connecting pipe other end and circulating pump intercommunication, fixed mounting has the fixed pipe in the distiller main part, fixed pipe and circulating pump intercommunication, fixed pipe fixed mounting has the shower nozzle, distiller main part is equipped with the movable groove, movable assembly installs in the movable groove, the movable block is equipped with the fixed orifices, movable assembly cooperates with the fixed orifices, fixed mounting has electric heating pipe in the distiller main part. During the use, carry out the circulation distillation through the extraction of circulating pump to the solution in the distiller main part, increase the effect of purification, through movable component and fixed orifices cooperation, upward movement movable block opens the discharge gate, conveniently takes out the solution after the purification finishes fast.
Aiming at the related technology, when the method is used for realizing the cyclic purification, the position of the electric heating pipe is kept unchanged, the contact between the solution to be purified in the distiller body and the electric heating pipe is insufficient, and the heating is uneven under the heating of the electric heating pipe, so that the phenomenon of slow purification efficiency is caused.
Disclosure of Invention
In order to realize uniform heating of the solution with distillation purification and improve the distillation purification efficiency, the utility model provides a circulating distillation purification device for acetate feed additive production.
The utility model provides a circulating distillation purification device for acetate feed additive production, which adopts the following technical scheme:
the utility model provides a circulation distillation purification device for acetate feed additive production, includes the still, be provided with heating mechanism in the still, heating mechanism includes electric heating wire, supporting component and electric heating rod, electric heating wire evenly set up in the inner wall of still, electric heating rod connect in supporting component, supporting component is used for supporting electric heating rod, electric heating rod is located in the cavity of still.
Through adopting above-mentioned technical scheme, through setting up electric heating wire and electric heating rod in the stills, realize the diversified heating of solution realization in the stills for the solution is heated more evenly, with this evaporation efficiency that realizes improving the solution, improves the speed of distillation.
Optionally, the supporting component includes rotation piece and support frame, the one end of support frame connect in the output of rotation piece, rotate the piece and be used for the drive the support frame is rotatory, the support frame keep away from the one end of rotation piece with the electrical heating rod is connected, the support frame with the electrical heating rod keeps static relatively.
Through adopting above-mentioned technical scheme, rotating piece drive support frame rotates, and the support frame rotates and drives electric heating rod and rotate simultaneously, when realizing constantly changing the heating position of electric heating rod, can also realize the stirring of the solution of waiting to distill for the heating of solution is more abundant even, further improves the distillation efficiency of solution.
Optionally, the side wall of the electric heating rod is provided with a concave-convex layer.
Through adopting above-mentioned technical scheme, the setting on unsmooth layer can realize increasing the area of contact between heating rod and the solution that waits to distill, has further improved the distillation efficiency of solution.
Optionally, a heat conducting plate is further arranged on the electric heating rod, the side edge of the heat conducting plate is connected to the electric heating rod, and the heat conducting plate does not interfere with rotation of the electric heating rod.
Through adopting above-mentioned technical scheme, the area of contact between heating source and the solution that waits to distill has further been improved to the setting of heat-conducting plate for the solution is heated more fully even when being heated, has improved distillation efficiency.
Optionally, a diversion hole is arranged on the heat conducting plate.
Through adopting above-mentioned technical scheme, the setting of water conservancy diversion hole has reduced the possibility that the heat conduction board obstructs solution flow, has reduced the insufficient phenomenon of solution heating.
Optionally, a temperature sensor is arranged in the distillation kettle, the temperature sensor is electrically connected with a controller, and the controller is used for controlling the opening and closing of the electric heating wire and the electric heating rod.
By adopting the technical scheme, the temperature sensor detects the temperature in the distillation still, and when the temperature sensor detects that the temperature in the distillation still exceeds a specified critical value, a stop signal is sent to the controller, and the controller controls the electric heating wire and the electric heating rod to stop heating when receiving the stop signal, so that the safety is ensured.
Optionally, an insulating layer is arranged on the outer side wall of the distillation kettle.
Through adopting above-mentioned technical scheme, the setting of heat preservation can improve the heat preservation performance of stills, reduces the heat dissipation of the interior solution of stills, is favorable to improving the distillation efficiency of solution.
Optionally, the lateral wall of stills with the heat preservation is provided with the observation groove, the inner wall in observation groove is connected with transparent observation piece.
Through adopting above-mentioned technical scheme, the setting of observation groove and transparent viewing element can conveniently observe the condition in the stills in real time, is convenient for in time make the reaction to the condition in the stills.
In summary, the present utility model includes at least one of the following beneficial technical effects:
1. the electric heating wires and the electric heating rods at different positions are arranged to fully heat the solution to be distilled in the distillation kettle in multiple directions, so that the solution is heated more uniformly, the heating efficiency of the solution is improved, and the distillation speed of the solution is accelerated.
2. The setting of rotating piece and support frame has realized the rotation of electrical heating rod, when realizing constantly changing the position of electrical heating rod, can also realize the stirring of solution, has further reduced the inhomogeneous phenomenon of solution heating.
3. The heat insulation layer reduces heat dissipation in the distillation kettle, and is beneficial to energy conservation.
Drawings
FIG. 1 is an overall schematic diagram of a cyclic distillation purification apparatus for acetate feed additive production of the present utility model.
FIG. 2 is a schematic cross-sectional view of a cyclic distillation purification apparatus for acetate feed additive production of the present utility model.
Reference numerals illustrate: 1. a base; 2. a diversion pipeline; 3. a condenser; 4. a circulation pump; 5. a distillation still; 6. a heating mechanism; 601. an electric heating wire; 602. a support assembly; 6021. a support frame; 6022. a rotating member; 603. an electrically heated wand; 7. a concave-convex layer; 8. a heat conductive plate; 9. a deflector aperture; 10. a controller; 11. a temperature sensor; 12. a heat preservation layer; 13. an observation groove; 14. a transparent viewing member.
Detailed Description
The utility model is described in further detail below with reference to fig. 1-2.
The embodiment of the utility model discloses a circulating distillation purification device for acetate feed additive production. Referring to fig. 1, a circulation distillation purification device for acetate feed additive production includes a distillation still 5, a base 1 is welded at the bottom of the distillation still 5, a diversion pipeline 2 is communicated with the top of the distillation still 5, a condenser 3 and a circulation pump 4 are sequentially arranged on the diversion pipeline 2, an insulation layer 12 is adhered to the outer side wall of the distillation still 5, an observation groove 13 is formed in the same position of the insulation layer 12 and the side wall of the distillation still 5, a transparent observation piece 14 is adhered to the inner wall of the observation groove 13, and the transparent observation piece 14 in this embodiment can be made of transparent glass.
Referring to the figure, a controller 10 is installed on a still 5, the controller 10 of this embodiment may be a PLC controller 10, a temperature sensor 11 is installed in the still 5, the temperature sensor 11 is electrically connected to the controller 10, a heating mechanism 6 is provided in the still 5, the heating mechanism 6 includes an electric heating wire 601, a supporting component 602 and an electric heating rod 603, three groups of electric heating rods 603 are provided in this embodiment, the electric heating wire 601 is uniformly installed on the inner wall of the still 5, and both the electric heating wire 601 and the electric heating rod 603 are controlled by the controller 10.
Referring to the figure, the circumferential wall of the electric heating rod 603 is welded with a concave-convex layer 7, the concave-convex layer 7 is made of a heat conducting material, the side wall of the electric heating rod 603 is welded with a heat conducting plate 8, the heat conducting plate 8 has a certain radian, the movement of the electric heating rod 603 is not interfered, and a plurality of diversion holes 9 are uniformly formed in the side wall of the heat conducting plate 8.
Referring to the figure, the supporting component 602 includes a rotating member 6022 and a supporting member, the rotating member 6022 of this embodiment may be a rotating motor, one end of a supporting frame 6021 is welded to an output end of the rotating member 6022, the rotating member 6022 is used for driving the supporting frame 6021 to rotate, one end of the supporting frame 6021 far away from the rotating member 6022 is welded to the electric heating roller 603, and the supporting frame 6021 can drive the electric heating roller 603 to rotate together.
The embodiment of the utility model relates to a circulating distillation purification device for acetate feed additive production, which is implemented by the following principle: when the distillation kettle is used, solution to be distilled and purified is injected into the distillation kettle 5, the controller 10 controls the electric heating wire 601 and the electric heating rod 603 to open heating distillation, the rotating piece 6022 drives the supporting frame 6021 to rotate, the supporting frame 6021 rotates to drive the electric heating rod 603 and the heat conducting plate 8 to rotate together, full contact heating of the solution in the distillation kettle 5 is realized, and the embodiment can realize improvement of the heating efficiency of the solution and acceleration of distillation speed.
The above embodiments are not intended to limit the scope of the present utility model, so: all equivalent changes in structure, shape and principle of the utility model should be covered in the scope of protection of the utility model.
Claims (8)
1. A circulation distillation purification device for acetate feed additive production, its characterized in that: including still (5), be provided with heating mechanism (6) in still (5), heating mechanism (6) are including electric heating wire (601), supporting component (602) and electric heating rod (603), electric heating wire (601) evenly set up in the inner wall of still (5), electric heating rod (603) connect in supporting component (602), supporting component (602) are used for supporting electric heating rod (603), electric heating rod (603) are located in the cavity of still (5).
2. The cyclic distillation purification device for acetate feed additive production according to claim 1, wherein: the support assembly (602) comprises a rotating piece (6022) and a support frame (6021), one end of the support frame (6021) is connected to the output end of the rotating piece (6022), the rotating piece (6022) is used for driving the support frame (6021) to rotate, one end, away from the rotating piece (6022), of the support frame (6021) is connected with the electric heating rod (603), and the support frame (6021) and the electric heating rod (603) are kept relatively static.
3. The cyclic distillation purification device for acetate feed additive production according to claim 1, wherein: the side wall of the electric heating rod (603) is provided with a concave-convex layer (7).
4. The cyclic distillation purification device for acetate feed additive production according to claim 1, wherein: the electric heating rod (603) is further provided with a heat conducting plate (8), the side edge of the heat conducting plate (8) is connected to the electric heating rod (603), and the heat conducting plate (8) does not interfere with rotation of the electric heating rod (603).
5. The cyclic distillation purification device for acetate feed additive production according to claim 4, wherein: and the heat conducting plate (8) is provided with a diversion hole (9).
6. The cyclic distillation purification device for acetate feed additive production according to claim 1, wherein: the distillation kettle (5) is internally provided with a temperature sensor (11), the temperature sensor (11) is electrically connected with a controller (10), and the controller (10) is used for controlling the opening and closing of the electric heating wire (601) and the electric heating rod (603).
7. The cyclic distillation purification device for acetate feed additive production according to claim 1, wherein: the outer side wall of the distillation kettle (5) is provided with an insulating layer (12).
8. The cyclic distillation purification device for acetate feed additive production according to claim 7, wherein: the side wall of the distillation kettle (5) and the heat preservation layer (12) are provided with an observation groove (13), and the inner wall of the observation groove (13) is connected with a transparent observation piece (14).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321368990.5U CN219963972U (en) | 2023-05-31 | 2023-05-31 | A circulation distillation purification device for acetate feed additive production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202321368990.5U CN219963972U (en) | 2023-05-31 | 2023-05-31 | A circulation distillation purification device for acetate feed additive production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN219963972U true CN219963972U (en) | 2023-11-07 |
Family
ID=88587309
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202321368990.5U Active CN219963972U (en) | 2023-05-31 | 2023-05-31 | A circulation distillation purification device for acetate feed additive production |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN219963972U (en) |
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2023
- 2023-05-31 CN CN202321368990.5U patent/CN219963972U/en active Active
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