CN218686434U

CN218686434U - Short-range molecular distillation device for removing ganoderma lucidum spore oil plasticizer

Info

Publication number: CN218686434U
Application number: CN202222305076.8U
Authority: CN
Inventors: 田克赞; 陶磊; 李晓颖; 胡金奎; 陶志铸; 陶岩
Original assignee: Shandong Zhirentang Pharmaceutical Co ltd
Current assignee: Shandong Zhirentang Pharmaceutical Co ltd
Priority date: 2022-08-31
Filing date: 2022-08-31
Publication date: 2023-03-24
Anticipated expiration: 2032-08-31

Abstract

The utility model discloses a short distance molecular distillation device for dispelling glossy ganoderma spore oil plasticizing agent relates to glossy ganoderma spore processing field. The utility model provides a short distance molecular distillation device for dispelling glossy ganoderma spore oil plasticizing agent, includes base, stills fixed connection is on the base, set up the heating chamber in stills's the inner wall, still include: the driving motor is fixedly connected to the upper end of the distillation kettle; the utility model discloses the effectual oil plasticizing agent and other invalid and poisonous harmful substance's that have improved in the ganoderma lucidum spore appear the effect, increased the security of ganoderma lucidum spore, solved the difficult problem that ganoderma lucidum spore poor stability, easy be oxidized, acid value is high, peroxide value is high, the plasticizing agent is difficult to dispel, improve the security and the quality that the ganoderma lucidum spore took, be suitable for using widely.

Description

Short-range molecular distillation device for removing ganoderma lucidum spore oil plasticizer

Technical Field

The utility model belongs to the technical field of the processing of glossy ganoderma spore, specifically speaking relates to a short distance molecular distillation plant for dispelling glossy ganoderma spore oil plasticizing agent.

Background

Short-path molecular distillation is a special liquid-liquid separation technology, different from the traditional distillation based on the separation principle of the boiling point difference of substances, and realizes the separation based on the difference of the molecular motion mean free path of each substance in a mixture.

The ganoderma lucidum spores are seeds of the extremely tiny ovoid germ cells ejected from ganoderma lucidum folds in the growth and maturation period of the ganoderma lucidum, have a double-wall structure, are surrounded by hard chitin cellulose, are difficult to be fully absorbed by human bodies, are more suitable for direct absorption of intestines and stomach of the human bodies after wall breaking, have clear requirements on the content of plasticizer in the ganoderma lucidum spores in the current pharmaceutical industry, but the plasticizer in the existing spore powder raw materials seriously exceeds the standard and is mainly introduced in the processes of cultivation, planting soil, collection and even airing.

In the in-process of processing the glossy ganoderma gown, need appear invalid and poisonous harmful substance and plasticizer wherein, among the prior art, adopt short distance molecular distillation device to process the purification to glossy ganoderma gown usually, but current short distance molecular distillation device, often the direct heating is distillated, do not possess the function of preheating to the mixed liquid of glossy ganoderma gown, consequently lead to can not carrying out even abundant heating process to the mixed liquid, so that what plasticizer and other impurity dispeled is abundant inadequately, the purification precision is lower, in view of this the special proposition the utility model discloses a.

SUMMERY OF THE UTILITY MODEL

The to-be-solved technical problem of the utility model lies in overcoming the not enough of prior art, provides one kind and can overcome above-mentioned problem or solve above-mentioned problem at least partially for dispel the short distance molecular distillation plant of glossy ganoderma spore oil plasticizing agent.

In order to solve the technical problem, the utility model adopts the following basic concept: the utility model provides a short distance molecular distillation device for dispelling glossy ganoderma spore oil plasticizing agent, includes base, stills fixed connection is on the base, set up the heating chamber in stills's the inner wall, still include: the driving motor is fixedly connected to the upper end of the distillation kettle; the liquid separating disc is arranged above the inner part of the distillation kettle and is fixedly connected with the output end of the driving motor through an output shaft; the first scraping blade is fixedly connected to two sides of the lower end of the liquid distribution disc; the condensing assembly is arranged in the middle of the interior of the distillation kettle; the liquid accumulation disc is arranged at the lower end of the condensing assembly, and a liquid discharge pipe extending out of the distillation still is fixedly connected to a liquid discharge port of the liquid accumulation disc; the heating assembly is used for heating water in the heating cavity and is arranged in the heating cavity; the preheating box is fixedly connected to one side of the base close to the liquid inlet of the distillation kettle; first heat exchange tube installs in the preheating cabinet, wherein, one side upper end that the heating chamber is close to the preheating cabinet is equipped with steam outlet, be linked together through the connecting pipe between the steam outlet in heating chamber and the air inlet of first heat exchange tube.

In order to facilitate the condensation that lasts light component, furtherly, the condensation subassembly includes refrigeration case, delivery pump, condenser pipe, catheter, refrigeration case fixed connection is in the bottom of base, delivery pump fixed connection be in on the refrigeration case, and the lotion mouth with the liquid outlet of refrigeration case is linked together, condenser pipe fixed connection is in the inside intermediate position department of stills, catheter fixed connection is in the condenser pipe, and the lower extreme extends still, be linked together through the transfer line between the lower extreme of catheter and the liquid outlet of delivery pump, hydrops dish cup joints the below at the condenser pipe, the liquid return mouth of condenser pipe and the liquid return mouth of refrigeration case pass through liquid return pipe and communicate.

In order to improve the heating effect, further, the heating assembly comprises a heater and a spiral heating rod, the heater is fixedly connected to one side, far away from the preheating box, of the distillation kettle, the heating rod is wound in the heating cavity, and the input end of the heating rod is fixedly connected with the output end of the heater.

In order to facilitate heat dissipation of the driving motor, the end, far away from the connecting pipe, of the first heat exchange pipe extends out of the preheating box and is fixedly connected with a second heat exchange pipe, and the second heat exchange pipe is wound on the surface of the driving motor.

In order to further improve the purification effect, the lower end of the first scraping blade is fixedly connected with a second scraping blade through a connecting rod.

In order to facilitate quick discharge of the condensate, third scraping pieces are symmetrically and fixedly connected to the two sides of the lower end of the liquid distribution plate, which are close to the condensation pipe, and are attached to the surface of the condensation pipe, and the third scraping pieces are fixedly connected with the first scraping pieces, the second scraping pieces and the connecting rod through fixing rods.

After the technical scheme is adopted, compared with the prior art, the utility model following beneficial effect has: the utility model discloses can utilize the waste heat that heating element produced, the heat that makes the waste heat can carry out heat transfer treatment with mixed liquid, thereby be convenient for carry out preheating operation to mixed liquid, through preheating treatment to mixed liquid, not only can shorten distillation purification's time, improve purification efficiency, can also carry out abundant heating to mixed liquid, thereby effectual the precipitation effect of oil plasticizing agent and other invalid and poisonous harmful substance in the glossy ganoderma robe that has improved, the security of glossy ganoderma robe has been increased, the glossy ganoderma robe stability is poor has been solved, easily be oxidized, the acid value is high, the peroxide value is high, the difficult problem that plasticizing agent is difficult to dispel, improve the security and the quality that glossy ganoderma robe was taken, and the device is suitable for being generalized to use.

The following describes embodiments of the present invention in further detail with reference to the attached drawings.

Drawings

The accompanying drawings, which are included to provide a further understanding of the invention, are incorporated in and constitute a part of this specification, illustrate embodiments of the invention and together with the description serve to explain the invention without undue limitation. It is obvious that the drawings in the following description are only some embodiments and that for a person skilled in the art, other drawings can also be derived from them without inventive effort.

In the drawings:

FIG. 1 is a schematic structural diagram of a short-path molecular distillation device for removing ganoderma lucidum spore oil plasticizer according to the present invention;

FIG. 2 is a schematic structural view of part A of FIG. 1 of a short-path molecular distillation apparatus for removing ganoderma lucidum spore oil plasticizer according to the present invention;

fig. 3 is a schematic structural diagram of a part B in fig. 1 of a short-path molecular distillation apparatus for removing ganoderma lucidum spore oil plasticizer according to the present invention.

In the figure: 1. a base; 2. a distillation kettle; 201. a heating cavity; 3. a preheating box; 4. a drive motor; 5. an output shaft; 6. a liquid separation disc; 7. a first blade; 8. a third wiper blade; 9. a second wiper blade; 10. a connecting rod; 11. fixing the rod; 12. a heater; 13. heating a rod; 14. a connecting pipe; 15. a first heat exchange tube; 16. a second heat exchange tube; 17. a refrigeration case; 18. a delivery pump; 19. a condenser tube; 20. a catheter; 21. liquid accumulation plate.

It should be noted that the drawings and the description are not intended to limit the scope of the inventive concept in any way, but to illustrate the inventive concept by those skilled in the art with reference to specific embodiments.

Detailed Description

To make the purpose, technical solution and advantages of the embodiments of the present invention clearer, the attached drawings in the embodiments of the present invention are combined below to clearly and completely describe the technical solution in the embodiments, and the following embodiments are used to illustrate the present invention, but do not limit the scope of the present invention.

Example 1:

referring to fig. 1-3, a short distance molecular distillation device for dispelling glossy ganoderma spore oil plasticizer, includes base 1, stills 2, and stills 2 fixed connection has seted up heating chamber 201 in stills 2's the inner wall on base 1, still includes: the driving motor 4 is fixedly connected to the upper end of the distillation kettle 2; the liquid separating disc 6 is arranged above the inner part of the distillation kettle 2 and is fixedly connected with the output end of the driving motor 4 through an output shaft 5; the first scraping blade 7 is fixedly connected to two sides of the lower end of the liquid distribution disc 6; the condensing assembly is arranged in the middle of the interior of the distillation kettle 2; the liquid accumulation disc 21 is arranged at the lower end of the condensing assembly, and a liquid discharge pipe extending out of the distillation still 2 is fixedly connected at a liquid discharge port of the liquid accumulation disc 21; a heating assembly for heating water in the heating chamber 201, installed in the heating chamber 201; the preheating box 3 is fixedly connected to one side of the base 1 close to the liquid inlet of the distillation kettle 2; the first heat exchange tube 15 is arranged in the preheating box 3, wherein a steam outlet is formed in the upper end of one side, close to the preheating box 3, of the heating cavity 201, and the steam outlet of the heating cavity 201 is communicated with an air inlet of the first heat exchange tube 15 through a connecting tube 14;

the condensing assembly comprises a refrigerating box 17, a delivery pump 18, a condensing tube 19 and a liquid guide tube 20, the refrigerating box 17 is fixedly connected to the bottom of the base 1, the delivery pump 18 is fixedly connected to the refrigerating box 17, a washing liquid port is communicated with a liquid outlet of the refrigerating box 17, the condensing tube 19 is fixedly connected to the middle position inside the distillation still 2, the liquid guide tube 20 is fixedly connected into the condensing tube 19, the lower end of the liquid guide tube 20 extends out of the distillation still 2, the lower end of the liquid guide tube 20 is communicated with the liquid outlet of the delivery pump 18 through a liquid conveying tube, a liquid accumulating disc 21 is sleeved below the condensing tube 19, and a liquid return port of the condensing tube 19 is communicated with a liquid return port of the refrigerating box 17 through a liquid return tube;

the heating component comprises a heater 12 and a spiral heating rod 13, the heater 12 is fixedly connected to one side, far away from the preheating box 3, of the distillation kettle 2, the heating rod 13 is coiled in the heating cavity 201, and the input end of the heating rod 13 is fixedly connected with the output end of the heater 12.

When the device is used, a worker firstly moves the device to a designated working position, then fixes the device to improve the stability of the device during working, then connects a vacuum tube on the distillation still 2 with an external vacuum pump, then connects a liquid outlet tube at a liquid outlet of the distillation still 2 and a liquid outlet tube on the liquid accumulation disc 21 with different external collection barrels respectively, then switches on an electric device on the device, when oil plasticizer in ganoderma spores needs to be removed, firstly carries out wall breaking treatment through ganoderma robe at the moment to process the ganoderma robe into powder, then adds the processed ganoderma robe powder into an organic solvent for dissolving, diluting and mixing, then conveys the mixed liquid into a preheating box 3 through a conveying tube, then conveys water into a heating cavity 201 of the distillation still 2, and then starts a heater 12, the heater 12 heats the water in the heating chamber 201 through the heating rod 13, when the water in the heating chamber 201 starts to boil, the hot steam in the heating chamber 201 enters the first heat exchange tube 15 through the connecting tube 14, wherein the first heat exchange tube 15 is bent in the preheating tank 3 in a serpentine shape, so that after the hot steam is introduced into the first heat exchange tube 15, the contact time between the hot steam and the mixed liquid can be increased, thereby effectively improving the preheating effect on the mixed liquid, when the temperature of the inner wall of the distillation kettle 2 reaches a specified value and the vacuumizing operation is completed, the suction pump on the preheating tank 3 is started, then the preheated mixed liquid is conveyed into the distillation kettle 2 through the liquid inlet of the distillation kettle 2 by the suction pump, then the mixed liquid falls onto the liquid distribution plate 6, then the driving motor 4 is started, the driving motor 4 drives the liquid distribution plate 6 to rotate through the output shaft 5, then the mixed liquid is thrown to the side wall of the distillation still 2 under the action of the liquid separating disc 6, the gap between the liquid separating disc 6, the first scraping blade 7 and the inner wall of the distillation still 2 is only one millimeter, therefore, when the liquid separating disc 6 drives the first scraping blade 7 to rotate, the mixed liquid flowing downwards along the inner wall of the distillation still 2 forms a thin water film on the inner wall of the distillation still 2, then the water film is heated by the inner wall of the distillation still 2 with higher temperature, so that the water film is maintained at a stable temperature, at the moment, the light and heavy components in the solution overflow the liquid level, because the heavy components are heavier, the free path is low, then the heavy components flow downwards together with the mixed liquid, finally the mixed liquid is discharged through a liquid outlet pipe at the bottom of the distillation still 2, because the light components are lighter, the free path is larger, then the light components of the oil plasticizer float far away, then fall onto the condensing pipe 19, while the heater 12 heats the conveying pump 18, the conveying liquid in the conveying pump 18 conveys the distilled liquid in the distillation still 17 to the liquid guiding pipe 20, then the distillation still 2 to be purified, finally, the condensed liquid flows back to the distillation still 2 through the condensing pipe 19, and then the condensing pipe 19, the condensed liquid is purified, finally, the condensed liquid can be purified, and purified, the condensed liquid can be collected and purified, and purified again, and purified, the condensed liquid can be purified continuously, and purified, the mixed liquid can be purified, and purified, the mixed liquid can be obtained, the device passes through heating device, connecting pipe 14, first heat exchange tube 15's setting, can carry out heat transfer treatment with the steam that the heating produced and mixed liquid, thereby be convenient for carry out preheating operation to mixed liquid, through carrying out preheating treatment to mixed liquid, not only can shorten distillation purification's time, improve purification efficiency, can also carry out abundant heating to mixed liquid, thereby effectual improved glossy ganoderma robe in oil plasticizing agent and other invalid and poisonous harmful substance's the effect of appearing, the security of glossy ganoderma robe has been increased, it is poor to have solved glossy ganoderma robe stability, easily be oxidized, the acid value is high, the peroxide value is high, the difficult problem that the plasticizing agent is difficult to dispel, improve the security and the quality that glossy ganoderma robe was taken, and is suitable for being generalized to use.

Example 2:

referring to fig. 1-3, a short path molecular distillation apparatus for removing ganoderma lucidum spore oil plasticizer, substantially the same as in example 1, further comprising: one end of the first heat exchange tube 15, which is far away from the connecting tube 14, extends out of the preheating box 3, and is fixedly connected with a second heat exchange tube 16, the second heat exchange tube 16 is wound on the surface of the driving motor 4, through the arrangement of the second heat exchange tube 16, when the heat exchange of steam in the first heat exchange tube 15 is completed, and the temperature is reduced, the gas with lower temperature in the first heat exchange tube 15 can be output through the second heat exchange tube 16, and because the second heat exchange tube 16 is wound on the driving motor 4, when the gas passes through the driving motor 4, the heat generated around the driving motor 4 can be rapidly and deadly absorbed, so that the heat dissipation effect on the driving motor 4 is facilitated, and the service life of the driving motor 4 is effectively prolonged;

the lower end of the first scraping blade 7 is fixedly connected with a second scraping blade 9 through a connecting rod 10, the lower end of the first scraping blade 7 is fixedly connected with the second scraping blade 9 through the connecting rod 10, when the first scraping blade 7 scrapes the membrane of the mixed liquor, the mixed liquor which is firstly separated can be subjected to membrane scraping separation again through the second scraping blade 9, so that the light and heavy components are separated more thoroughly, and the effect of purifying the ganoderma spores is effectively improved;

divide liquid dish 6 lower extreme to be close to the bilateral symmetry fixedly connected with third doctor-bar 8 of condenser pipe 19, third doctor-bar 8 pastes with the surface of condenser pipe 19 mutually, third doctor-bar 8 and first doctor-bar 7, second doctor-bar 9, through dead lever 11 fixed connection between the connecting rod 10, through the setting of third doctor-bar 8, when dividing liquid dish 6 to drive first doctor-bar 7, when second doctor-bar 9 carries out the knifing, can also drive third doctor-bar 8 simultaneously and rotate on the surface of condenser pipe 19, thereby alright strike off the light component that the condensation changed into liquid and impurity from condenser pipe 19 fast, thereby not only can improve the discharge efficiency of light component, can also prevent that impurity from depending on condenser pipe 19, thereby cause the influence to the refrigeration effect of condenser pipe 19, through the setting of dead lever 11, can be connected third doctor-bar 8 and first doctor-bar 7, second doctor-bar 9, connecting rod 10, thereby the effectual stability that improves the device at work is with first doctor-bar 7, second doctor-bar 9, the effectual stability that improves.

The utility model discloses can utilize the waste heat that heating element produced, the heat that makes the waste heat can carry out heat transfer treatment with mixed liquid, thereby be convenient for carry out preheating operation to mixed liquid, through preheating treatment to mixed liquid, not only can shorten distillation purification's time, improve purification efficiency, can also carry out abundant heating to mixed liquid, thereby effectual the precipitation effect of oil plasticizing agent and other invalid and poisonous harmful substance in the glossy ganoderma robe that has improved, the security of glossy ganoderma robe has been increased, the glossy ganoderma robe stability is poor has been solved, easily be oxidized, the acid value is high, the peroxide value is high, the difficult problem that plasticizing agent is difficult to dispel, improve the security and the quality that glossy ganoderma robe was taken, and the device is suitable for being generalized to use.

In the description provided herein, numerous specific details are set forth. It is understood, however, that embodiments of the invention may be practiced without these specific details. In some instances, well-known methods, structures and techniques have not been shown in detail in order not to obscure an understanding of this description.

The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention in any way, and although the present invention has been disclosed with reference to the above preferred embodiment, but not to limit the present invention, any person skilled in the art can make some changes or modifications to equivalent embodiments without departing from the scope of the present invention, and any simple modification, equivalent change and modification made to the above embodiments by the technical spirit of the present invention still fall within the scope of the present invention.

Claims

1. The utility model provides a short distance molecular distillation device for dispelling glossy ganoderma spore oil plasticizer, includes base (1), stills (2) fixed connection is on base (1), its characterized in that, heating chamber (201) have been seted up in the inner wall of stills (2), still include:

the driving motor (4) is fixedly connected to the upper end of the distillation kettle (2);

the liquid separating disc (6) is arranged above the inner part of the distillation kettle (2) and is fixedly connected with the output end of the driving motor (4) through an output shaft (5);

the first scraping blade (7) is fixedly connected to two sides of the lower end of the liquid distribution disc (6);

the condensing assembly is arranged at the middle position in the distillation kettle (2);

the liquid accumulation disc (21) is installed at the lower end of the condensation assembly, and a liquid discharge pipe extending out of the distillation kettle (2) is fixedly connected to a liquid discharge port of the liquid accumulation disc (21);

a heating assembly for heating water in the heating chamber (201), mounted in the heating chamber (201);

the preheating box (3) is fixedly connected to one side of the base (1) close to the liquid inlet of the distillation kettle (2);

a first heat exchange tube (15) installed in the preheating tank (3),

the heating chamber (201) is provided with a steam outlet at the upper end of one side close to the preheating chamber (3), and the steam outlet of the heating chamber (201) is communicated with the air inlet of the first heat exchange pipe (15) through a connecting pipe (14).

2. The short path molecular distillation device for removing ganoderma lucidum spore oil plasticizer according to claim 1, wherein the short path molecular distillation device comprises: condensation assembly includes refrigeration case (17), delivery pump (18), condenser pipe (19), catheter (20), refrigeration case (17) fixed connection is in the bottom of base (1), delivery pump (18) fixed connection is in on refrigeration case (17), and the lotion mouth with the liquid outlet of refrigeration case (17) is linked together, condenser pipe (19) fixed connection is in the inside intermediate position department of stills (2), catheter (20) fixed connection is in condenser pipe (19), and the lower extreme extends stills (2), be linked together through the transfer line between the lower extreme of catheter (20) and the liquid outlet of delivery pump (18), amass liquid dish (21) cup joints the below at condenser pipe (19), the liquid return mouth of condenser pipe (19) and the liquid return mouth of refrigeration case (17) pass through liquid return pipe intercommunication.

3. The short path molecular distillation device for removing ganoderma lucidum spore oil plasticizer according to claim 1, wherein the short path molecular distillation device comprises: the heating assembly comprises a heater (12) and a spiral heating rod (13), the heater (12) is fixedly connected to one side, far away from the preheating box (3), of the distillation kettle (2), the heating rod (13) is coiled in the heating cavity (201), and the input end of the heating rod (13) is fixedly connected with the output end of the heater (12).

4. The short path molecular distillation device for removing ganoderma lucidum spore oil plasticizer according to claim 3, wherein the short path molecular distillation device comprises: one end, far away from the connecting pipe (14), of the first heat exchange pipe (15) extends out of the preheating box (3) and is fixedly connected with a second heat exchange pipe (16), and the second heat exchange pipe (16) is wound on the surface of the driving motor (4).

5. The short path molecular distillation device for removing ganoderma lucidum spore oil plasticizer according to claim 2, wherein the short path molecular distillation device comprises: the lower end of the first scraping blade (7) is fixedly connected with a second scraping blade (9) through a connecting rod (10).

6. The short-path molecular distillation device for removing ganoderma lucidum spore oil plasticizer according to claim 5, wherein the short-path molecular distillation device comprises: the liquid separating plate is characterized in that third scraping pieces (8) are symmetrically and fixedly connected to two sides of the lower end of the liquid separating plate (6) close to the condensing pipe (19), the third scraping pieces (8) are attached to the surface of the condensing pipe (19), and the third scraping pieces (8) are fixedly connected with the first scraping pieces (7), the second scraping pieces (9) and the connecting rods (10) through fixing rods (11).