CN218250309U - A porous glass plate absorption tube - Google Patents
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- CN218250309U CN218250309U CN202222452976.5U CN202222452976U CN218250309U CN 218250309 U CN218250309 U CN 218250309U CN 202222452976 U CN202222452976 U CN 202222452976U CN 218250309 U CN218250309 U CN 218250309U
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- 238000010521 absorption reaction Methods 0.000 title claims abstract description 25
- 239000005373 porous glass Substances 0.000 title claims abstract description 23
- 239000007788 liquid Substances 0.000 claims abstract description 61
- 230000007704 transition Effects 0.000 claims abstract description 18
- 210000005239 tubule Anatomy 0.000 claims abstract 2
- 239000011521 glass Substances 0.000 claims description 6
- 239000006096 absorbing agent Substances 0.000 claims 6
- 238000007789 sealing Methods 0.000 claims 2
- 238000001514 detection method Methods 0.000 abstract description 7
- 238000007599 discharging Methods 0.000 abstract description 7
- 238000005452 bending Methods 0.000 abstract description 6
- 238000010079 rubber tapping Methods 0.000 abstract 2
- 238000000926 separation method Methods 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- 238000010586 diagram Methods 0.000 description 7
- 238000004140 cleaning Methods 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- 238000012360 testing method Methods 0.000 description 4
- 238000007664 blowing Methods 0.000 description 3
- 238000005070 sampling Methods 0.000 description 3
- 230000004888 barrier function Effects 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 230000003749 cleanliness Effects 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000012295 chemical reaction liquid Substances 0.000 description 1
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Abstract
Description
技术领域technical field
本实用新型涉及的是气体测量设备工具领域,具体的说是一种多孔玻板吸收管。The utility model relates to the field of gas measuring equipment and tools, in particular to a porous glass plate absorption tube.
背景技术Background technique
现有对气体成分检测和分析时,通常采用多孔玻板吸收管作为反应器皿,其原理在管内置有液体试剂,通过吸收管作为气体通道使待检测气体(以下统称气体)与试剂(以下统称液体)发生接触反应,其中,为提高气液反应效率,在管体内设置有能够将气体气流分散的多孔玻板,进而气体与液体接触时产生很多细碎的小气泡与液体进行充分接触,进而实现高效检测和分析。In the existing detection and analysis of gas components, the porous glass plate absorption tube is usually used as the reaction vessel. The principle is that there is a liquid reagent in the tube, and the gas to be detected (hereinafter collectively referred to as gas) and the reagent (hereinafter collectively referred to as liquid) in a contact reaction, wherein, in order to improve the gas-liquid reaction efficiency, a porous glass plate capable of dispersing the gas flow is arranged in the tube body, and then when the gas contacts the liquid, many finely divided small bubbles are generated to fully contact the liquid, thereby realizing Efficient detection and analysis.
但由于现有多孔玻板吸收管容量多在150ML以下以致其体积较小和管道进出口管道较细,并且进出口处管通常道折弯设置,导致现有移液管或注射器头部排液端无法送至宽敞的球形管内,这样一定程度上会导致液体难以注入,极易使液体溢出,造成采样液体不准,进而使检测结果产生偏差。However, due to the capacity of the existing porous glass plate absorption tube is mostly below 150ML, its volume is small and the inlet and outlet pipes are thinner, and the inlet and outlet pipes are usually bent, resulting in the discharge of liquid from the head of the existing pipette or syringe. The end cannot be sent into the spacious spherical tube, which will make it difficult to inject the liquid to a certain extent, and the liquid will easily overflow, resulting in inaccurate sampling of the liquid, which will cause deviations in the test results.
另外,现有吸收管在其底部设置有U弯折储液和气液反应区域,排液时通常通过采样从粗管侧向细管吹气的方式将反应后的液体从细管出口排出并收集或直接从粗管端倒出。但这种收集方式收集效率较低,容易造成液体残留,同样,由于设置有U弯折和多孔玻璃板,也不便于吸收管的清理。In addition, the existing absorption tube is equipped with a U-bend liquid storage and gas-liquid reaction area at its bottom. When discharging liquid, the liquid after reaction is usually discharged from the outlet of the thin tube and collected by sampling from the side of the thick tube to the thin tube. Or pour directly from the end of the thick tube. However, the collection efficiency of this collection method is low, and it is easy to cause liquid residue. Similarly, due to the U-bending and porous glass plates, it is not convenient for the cleaning of the absorption pipe.
因此,鉴于上述缺陷,设计一种多孔玻板吸收管。Therefore, in view of the above defects, a porous glass plate absorption tube is designed.
发明内容Contents of the invention
本实用新型要解决的技术问题是:解决现有多孔玻板吸收管注液困难问题。The technical problem to be solved by the utility model is to solve the problem of difficulty in injecting liquid into the existing porous glass plate absorption tube.
本实用新型解决其技术问题所采用的技术方案是:The technical scheme that the utility model solves its technical problem adopts is:
提供了一种多孔玻板吸收管,包括竖直并列设置的细管和粗管,二者底端通过U形管连通,所述粗管顶部连通有直径大于所述粗管直径的球形管,所述粗管底部内侧设置有多孔玻璃板。A porous glass plate absorption tube is provided, comprising thin tubes and thick tubes arranged vertically side by side, the bottom ends of which are communicated through a U-shaped tube, and the top of the thick tubes is communicated with a spherical tube with a diameter greater than that of the thick tube, A porous glass plate is arranged inside the bottom of the thick tube.
所述细管顶端设有向其外侧弯折并且与其连通的第一顶管,以及与所述细管同轴设置并且与其连通第二顶管;所述球形管顶部连通设置有过渡管,所述过渡管顶端设有向其外侧弯折并且与其连通的第三顶管,以及与所述过渡管同轴设置并且与其连通第四顶管;The top of the thin tube is provided with a first top pipe that is bent to its outside and communicates with it, and a second top pipe that is coaxially arranged with the thin tube and communicates with it; the top of the spherical tube is communicated with a transition pipe, The top end of the transition pipe is provided with a third top pipe which is bent to the outside and communicates with it, and a fourth top pipe which is arranged coaxially with the transition pipe and communicates with it;
所述吸收管顶部设置有两个上堵头,能够密封扣合在所述第二顶管和所述第四顶管端部或能够密封扣合在所述第一顶管和所述第三顶管端部。The top of the absorption pipe is provided with two upper plugs, which can be sealed and fastened to the ends of the second top pipe and the fourth top pipe or can be sealed and fastened to the ends of the first top pipe and the third top pipe. Top tube end.
作为优选,所述U形管底端设置有排液口,所述排液口密封扣合有下堵头。Preferably, the bottom end of the U-shaped tube is provided with a drain port, and the drain port is sealed and fastened with a lower plug.
作为优选,所述排液口设置在所述U形管底端正下方位置。Preferably, the liquid discharge port is arranged directly below the bottom end of the U-shaped tube.
作为优选,所述下堵头两侧端设置有沿其轴向延伸的卡臂,两所述卡臂夹设在所述U形管的外壁。Preferably, two ends of the lower plug are provided with clamping arms extending axially, and the two clamping arms are clamped on the outer wall of the U-shaped tube.
作为优选,两个上堵头通过连接绳连接。Preferably, the two upper plugs are connected by a connecting rope.
作为优选,所述连接绳为弹性连接绳。Preferably, the connecting rope is an elastic connecting rope.
作为优选,所述第一顶管轴线与所述第二顶管轴线之间的夹角以及所述第三顶管与所述第四顶管之间的夹角均为65°-80°。Preferably, the angle between the axis of the first pipe jacking and the axis of the second pipe jacking and the angle between the third pipe jacking and the fourth pipe jacking are both 65°-80°.
本实用新型的有益效果是,通过在折弯的第一顶管和第三顶管的上方设置有竖直设置的第二顶管和第四顶管。放液时,通过竖直设置的第二顶管和第四顶管进行放液。由于管体没有折弯阻隔直接可将移液管或注射器头部排液端送至球形管内,放液时,第一顶管或第三顶管可辅助管内气体的排出,减少放液阻力有效控制放液精准度,也避免放液溢流,一定程度上提高放液效率和检测精度。The beneficial effect of the utility model is that the vertically arranged second jacking pipe and the fourth jacking pipe are arranged above the bent first jacking pipe and the third jacking pipe. When discharging liquid, discharge liquid through the second jacking pipe and the fourth jacking pipe arranged vertically. Since the tube body has no bending barrier, the liquid discharge end of the pipette or syringe head can be directly sent to the spherical tube. When discharging the liquid, the first or third ejecting pipe can assist the discharge of the gas in the tube, which is effective in reducing the resistance of the liquid discharge. Control the accuracy of liquid discharge, and avoid overflow of liquid discharge, and improve the efficiency of liquid discharge and detection accuracy to a certain extent.
另一方面,在管体排液时,通过向第二顶管和第四顶管内或第一顶管和第三顶管内进行鼓气,可利用U形管最低端的排液口将液体排出。On the other hand, when the pipe body is draining, the liquid can be discharged by using the discharge port at the lowest end of the U-shaped pipe by blowing air into the second jacking pipe and the fourth jacking pipe or the first jacking pipe and the third jacking pipe.
在清洗管体时,竖直设置第二顶管和第四顶管能够减小对水流的阻力,并且第二顶管和第四顶管开口端朝下能够将管内水快速甩出,减少管内清理水的残留,提高管体的清洁度。When cleaning the pipe body, vertically setting the second and fourth jacking pipes can reduce the resistance to water flow, and the opening ends of the second and fourth jacking pipes can quickly throw out the water in the pipe and reduce the water flow in the pipe. Clean up the water residue and improve the cleanliness of the pipe body.
附图说明Description of drawings
为了更清楚地说明本实用新型实施例或现有技术中的技术方案,下面将对实施例或现有技术描述中所需要使用的附图作简单地介绍,显而易见地,下面描述中的附图仅仅是本实用新型的一些实施例,对于本领域普通技术人员来讲,在不付出创造性劳动的前提下,还可以根据这些附图获得其他的附图。In order to more clearly illustrate the technical solutions in the embodiments of the present invention or the prior art, the following will briefly introduce the accompanying drawings that need to be used in the description of the embodiments or the prior art. Obviously, the accompanying drawings in the following description These are only some embodiments of the utility model, and those skilled in the art can also obtain other drawings based on these drawings without creative work.
图1是本实用新型实施例所提供的吸收管立体结构示意图;Fig. 1 is a schematic diagram of the three-dimensional structure of the absorption pipe provided by the embodiment of the present invention;
图2是图1的分解结构示意图;Fig. 2 is a schematic diagram of an exploded structure of Fig. 1;
图3是本实用新型实施例所提供的吸收管主视结构示意图;Fig. 3 is a schematic diagram of the front view structure of the absorption tube provided by the embodiment of the present invention;
图4图3的全剖结构示意图;The schematic diagram of the full-section structure of Fig. 4 Fig. 3;
图5是本实用新型实施例所提供吸收管进行注液时示意图;Fig. 5 is a schematic diagram of the absorption pipe provided by the embodiment of the present invention when injecting liquid;
图6是本实用新型实施例所提供吸收管进行气液反应过程示意图;Fig. 6 is a schematic diagram of the gas-liquid reaction process of the absorption tube provided by the embodiment of the present invention;
图7是本实用新型实施例所提供吸收管进行排液或清理排液过程示意图;Fig. 7 is a schematic diagram of the draining or cleaning draining process of the absorption pipe provided by the embodiment of the present invention;
图中:1-细管,1.1-第一顶管,1.2-第二顶管,2-U形管,2.1-排液口,3-粗管,3.1-多孔玻璃板,4-球形管,5-过渡管,5.1-第三顶管,5.2-第四顶管,6-上堵头,6.1-连接绳,7-下堵头,7.1-卡臂。In the figure: 1-thin tube, 1.1-first top tube, 1.2-second top tube, 2-U-shaped tube, 2.1-drainage port, 3-thick tube, 3.1-porous glass plate, 4-spherical tube, 5-transition pipe, 5.1-third pipe jacking, 5.2-fourth pipe jacking, 6-upper plug, 6.1-connecting rope, 7-lower plug, 7.1-arm.
具体实施方式detailed description
以下结合具体实施例对上述方案做进一步说明。应理解这些实施例是用于说明本实用新型而不是限制本实用新型的范围。实施例中采用的实施条件可以根据具体厂家的条件做进一步调整,未注明的实施条件通常为常规实验中的条件。The above solution will be further described below in conjunction with specific embodiments. It should be understood that these embodiments are used to illustrate the utility model rather than limit the scope of the utility model. The implementation conditions adopted in the examples can be further adjusted according to the conditions of specific manufacturers, and the implementation conditions not indicated are usually the conditions in routine experiments.
在一种具体实施例中,提供了一种多孔玻板吸收管,通常整体采用玻璃材料制成,具体包括竖直并列设置的细管1和粗管3,这里所述的细管1和粗管3的“细”和“粗”是相对的。二者底端通过U形管2连通。在粗管3顶部连通有直径大于粗管3直径的球形管4,粗管3底部内侧设置有多孔玻璃板3.1,当气体通过多孔玻璃板3.1时,能够将于检测气体气流分散使其与检测液体充分接触以提高反应效率,其中,粗管3直径的球形管4主要的作用在于能够提供一个反应的缓冲空间,避免反应过于强烈或产生过多气泡溢出管外。另外,能够避免气体压力将液体推出管外。上述具体管体结构形式和使用方式与现有多孔玻板吸收管的结构形式和使用方式相同。因此不再赘述。In a specific embodiment, a porous glass plate absorption tube is provided, which is generally made of glass material as a whole, and specifically includes a
为了进一步解决解决现有多孔玻板吸收管注液困难的问题,对现有多孔玻板吸收管的结构进行改进,主要对细管1和粗管3的顶端结构进行了改进。具体如下:In order to further solve the problem of difficulty in injecting liquid into the existing porous glass plate absorption tube, the structure of the existing porous glass plate absorption tube is improved, mainly the top structures of the
在细管1顶端设有向其外侧弯折并且与细管1连通的第一顶管1.1,以及与细管1同轴设置并且与其连通第二顶管1.2(参见图1-图4);At the top of the
同样,在其球形管4顶部连通设置有过渡管5,在过渡管5顶端设有向其外侧弯折并且与过渡管5连通的第三顶管5.1,以及与过渡管5同轴设置并且与其连通第四顶管5.2。(参见图1-图4)Similarly, a
作为本实施例的优选实施例,第一顶管1.1轴线与第二顶管1.2轴线之间的夹角以及第三顶管5.1与第四顶管5.2之间的夹角均为65°-80°,这样能够保证第一顶管1.1和第三顶管5.1的端口朝向斜上方设置,进而能够有效避免反应过于强烈或产生过多气泡溢出管外,也避免放液时液体外流。As a preferred embodiment of this embodiment, the included angle between the axis of the first jacking pipe 1.1 and the axis of the second jacking pipe 1.2 and the angle between the third jacking pipe 5.1 and the fourth jacking pipe 5.2 are both 65°-80° °, so as to ensure that the ports of the first jacking pipe 1.1 and the third jacking pipe 5.1 are set obliquely upwards, thereby effectively preventing the reaction from being too strong or excessive bubbles from overflowing the pipes, and also avoiding the outflow of liquid when discharging.
另外在吸收管顶部设置有两个上堵头6,能够密封扣合在第二顶管1.2和第四顶管5.2端部或密封扣合在第一顶管1.1和第三顶管5.1端部;In addition, two
作为本实施例的优选实施例,由于在实施中至少需要两个上堵头6,因此为了避免两个上堵头6丢失,两堵头通过连接绳6.1连接,并且可通过连接绳6.1将上堵头6固定在管体上。另外,为进一步方便上堵头6的插拔使用,将连接绳6.1设为弹性连接绳,这样在不松绑连接绳6.1的同时使上堵头6能够扣合在任意顶管上,提高使用方便性。As a preferred embodiment of this embodiment, since at least two
具体注液操作时,为解决注入反应液体的进口处管道折弯导致液体难以注入管内,使液体溢出造成采样液体不准,进一步造成检测结果产生偏差的问题,本实施例中在折弯的第一顶管1.1和第三顶管5.1的上方设置有竖直设置的第二顶管1.2和第四顶管5.2。放液时,首先打开上堵头6,通过移液管或注射器进行放液。由于管体没有折弯阻隔直接可将移液管或注射器头部排液端送至球形管4内,并且移液管或注射器头部排液端通常较细,会与管体内部留有空隙,此时,第一顶管1.1或第三顶管5.1可辅助管内气体的排出,减少放液阻力有效控制放液精准度,进而避免放液溢流,进而在一定程度提高放液的精准度和放液效率。(参见图5)In the specific liquid injection operation, in order to solve the problem that the pipe bending at the entrance of the injection reaction liquid makes it difficult to inject the liquid into the pipe, causing the liquid to overflow, causing the sampling liquid to be inaccurate, and further causing deviations in the test results, in this embodiment, the first step of the bending A second jacking pipe 1.2 and a fourth jacking pipe 5.2 are arranged vertically above the first jacking pipe 1.1 and the third jacking pipe 5.1. When draining, first open the
放液后将上堵头6扣合在第二顶管1.2和第四顶管5.2上,实现多孔玻板吸收管对气体成分检测和分析。(参见图5)After discharging the liquid, fasten the
具体检测过程,首先将第三顶管5.1端接取负压装置,并调节负压气流的流速和流量,使测气体从第一顶管1.1端口进入细管1并到达多孔玻璃板3.1产生大量微小气泡,在此使气体和液体发生充分融合或气体中的预要测得的物质与液体发生化学,达到检测时间后,将检测后液体取出进行进一步化验。通常取出方式有两种,第一种是直接将液体从第三顶管5.1倒出,第二种则是通过向第三顶管5.1内鼓气,使液体从第一顶管1.1排出。但是这两种方式均不能将底部U形结构内的液体完全排出,并且第一种排出效率较低。In the specific testing process, first connect the end of the third jacking pipe 5.1 to a negative pressure device, and adjust the flow rate and flow rate of the negative pressure airflow, so that the measured gas enters the
因此,在上述实施例基础之上,为便于检测后的液体排出收集以及便于对管体的清理,对管体底部进行了改进,具体如下:Therefore, on the basis of the above-mentioned embodiments, in order to facilitate the liquid discharge and collection after detection and facilitate the cleaning of the tube body, the bottom of the tube body has been improved, as follows:
在U形管2底端设置有排液口2.1,排液口2.1密封扣合有下堵头7,堵头通常采用橡胶材料制成,使其能够紧密的扣合在排液口2.1上进行封堵。A drain port 2.1 is arranged at the bottom of the
为了进一步利于液体完全能够通过排液口2.1排出,排液口2.1设置在所述U形管2底端正下方位置。In order to further facilitate the complete discharge of liquid through the liquid discharge port 2.1, the liquid discharge port 2.1 is arranged directly below the bottom end of the
作为优选实施例,在下堵头7两侧端设置有沿其轴向延伸的卡臂7.1,两卡臂7.1通常采用具有弹性和钢片或塑料片制成,下堵头7安装后通过两卡臂7.1弹性夹持在U形管2的外壁上,进一步提高下堵头7扣合的强度。As a preferred embodiment, the two sides of the
具体排液操作时,也采用向管内鼓气的形成进行排液,上堵头6堵在第一顶管1.1和第三顶管5.1或第二顶管1.2和第四顶管5.2上,利用未堵的两端口进行鼓气,通过压力使液体快速从排液口2.1排出;During the specific liquid discharge operation, the formation of blowing air into the pipe is also used for liquid discharge. The
另一方面,在清理管体时,优先将上堵头6堵在第一顶管1.1和第三顶管5.1上,采用第二顶管1.2或第四顶管5.2任意一端作为进水端,另一端则作为排水端,反复进行完成清理,其中,第二顶管1.2和第四顶管5.2竖直设置能够降低对水流的阻力。另外,竖直设置第二顶管1.2和第四顶管5.2能够减小对水流的阻力,并且第二顶管1.2和第四顶管5.2开口端朝下能够将管内水快速甩出,减少管内清理水的残留。提高管体的清洁度。On the other hand, when cleaning the pipe body, the
以上述依据本实用新型的理想实施例为启示,通过上述的说明内容,相关工作人员完全可以在不偏离本项实用新型技术思想的范围内,进行多样的变更以及修改。本项实用新型的技术性范围并不局限于说明书上的内容,必须要根据权利要求范围来确定其技术性范围。Inspired by the above ideal embodiment according to the utility model, through the above description content, relevant staff can completely make various changes and modifications within the scope of not deviating from the technical idea of the utility model. The technical scope of this utility model is not limited to the content in the description, but must be determined according to the scope of the claims.
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