CN217202632U - Efficient and integrated essential oil distillation device - Google Patents
Efficient and integrated essential oil distillation device Download PDFInfo
- Publication number
- CN217202632U CN217202632U CN202220833540.8U CN202220833540U CN217202632U CN 217202632 U CN217202632 U CN 217202632U CN 202220833540 U CN202220833540 U CN 202220833540U CN 217202632 U CN217202632 U CN 217202632U
- Authority
- CN
- China
- Prior art keywords
- water
- collector
- heating
- essential oil
- tank
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000000341 volatile oil Substances 0.000 title claims abstract description 37
- 238000004821 distillation Methods 0.000 title claims abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 98
- 238000010438 heat treatment Methods 0.000 claims abstract description 50
- 238000000605 extraction Methods 0.000 claims abstract description 35
- 238000001704 evaporation Methods 0.000 claims abstract description 20
- 239000006260 foam Substances 0.000 claims abstract description 14
- 230000003020 moisturizing effect Effects 0.000 claims abstract description 8
- 239000008236 heating water Substances 0.000 claims abstract description 7
- 239000011521 glass Substances 0.000 claims description 7
- 238000000034 method Methods 0.000 claims description 6
- 238000004891 communication Methods 0.000 claims description 4
- 238000001577 simple distillation Methods 0.000 claims description 3
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 2
- 229910000838 Al alloy Inorganic materials 0.000 claims 1
- 239000002994 raw material Substances 0.000 abstract description 4
- 239000007788 liquid Substances 0.000 description 13
- 238000009835 boiling Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000000376 reactant Substances 0.000 description 3
- FGRBYDKOBBBPOI-UHFFFAOYSA-N 10,10-dioxo-2-[4-(N-phenylanilino)phenyl]thioxanthen-9-one Chemical compound O=C1c2ccccc2S(=O)(=O)c2ccc(cc12)-c1ccc(cc1)N(c1ccccc1)c1ccccc1 FGRBYDKOBBBPOI-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- 238000001256 steam distillation Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- TVEXGJYMHHTVKP-UHFFFAOYSA-N 6-oxabicyclo[3.2.1]oct-3-en-7-one Chemical compound C1C2C(=O)OC1C=CC2 TVEXGJYMHHTVKP-UHFFFAOYSA-N 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 230000000507 anthelmentic effect Effects 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000001754 anti-pyretic effect Effects 0.000 description 1
- 239000002221 antipyretic Substances 0.000 description 1
- 230000001877 deodorizing effect Effects 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000035876 healing Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 210000002345 respiratory system Anatomy 0.000 description 1
- 230000000580 secretagogue effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 230000035900 sweating Effects 0.000 description 1
- 230000002936 tranquilizing effect Effects 0.000 description 1
Images
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a high-efficient integrative essential oil distillation plant, its structural feature is: the heating cabinet is connected to the moisturizing case, the heating cabinet embeds there is the foam bobble, moisturizing case and heating cabinet constitute automatic water supply heating water tank, the evaporating pot is connected to the heating cabinet, straight condenser pipe is connected on evaporating pot top right side, collector is connected to straight condenser pipe, extraction device is connected to collector, be equipped with the piston between collector and the extraction device No. one, three opening under the extraction device, No. two receivers are connected to three opening one end, three opening one end water trap, water bath generator is connected to water trap, straight condenser pipe is connected to water bath generator, No. three receivers are connected to straight condenser pipe. The utility model has the advantages that: the integrated operation is convenient, the high-efficiency utilization of raw materials is achieved, so that the yield is improved, and the automatic water replenishing also enables the water vapor to be always in a sufficient state.
Description
Technical Field
The utility model relates to an essential oil distillation field, concretely relates to high-efficient integrative essential oil distillation plant.
Background
Essential oils in the broad sense are generic terms for volatile, material-containing preparations obtained by processing and extraction from perfumery plants or secretagogues. However, the essential oil used in daily life is a product containing an aromatic substance extracted from an aromatic plant by steam distillation, or squeezing, or cold milling, or dry distillation, and these products are mostly in a liquid state at normal temperature, and only a few varieties are in a solid state. The pure natural plant essential oil has the following main functions: the smell is fragrant, and the spirit is in a comfortable state. In addition, the essential oil has antibacterial, antiinflammatory, healing, deodorizing, tranquilizing, anthelmintic, respiratory tract immunity enhancing, sweating or antipyretic, phlegm eliminating, and digestion promoting effects.
The existing essential oil extraction adopts a distillation method, adopts high-temperature steam to heat a mixture of a spice plant and water so as to volatilize the essential oil from the mixture of the spice plant and the water, obtains the mixture of the essential oil and the water by a cold condensation method, and finally obtains the essential oil by extraction. This involves the use of multiple switches of the instrument, which wastes a lot of time, and it is necessary to connect the series of instruments in a reasonable and good way to achieve a convenient and quick action.
Disclosure of Invention
To the problem that prior art exists, this use is novel to provide a high-efficient integrative essential oil distillation plant, can solve calorific loss, operates inconveniently, needs the problem of a large amount of time.
The utility model is realized in such a way that a high-efficiency and integrated essential oil distillation device mainly comprises a water replenishing tank, a foam ball, a heating box, an evaporating pot, a straight condensing pipe, a first collector, a first piston, an extraction device, a three-way opening, a second receiver, a dewatering device, a water bath generator and a third receiver; the method is characterized in that: the heating cabinet is connected to the moisturizing case, the heating cabinet embeds there is the foam bobble, moisturizing case and heating cabinet constitute automatic water supply heating water tank, the evaporating pot is connected to the heating cabinet, straight condenser pipe is connected on evaporating pot top right side, collector is connected to straight condenser pipe, extraction device is connected to collector, be equipped with the piston between collector and the extraction device No. one, three opening under the extraction device, No. two receivers are connected to three opening one end, three opening one end water trap, water bath generator is connected to water trap, straight condenser pipe is connected to water bath generator, No. three receivers are connected to straight condenser pipe.
Furthermore, the automatic water replenishing heating water tank is formed by combining a heating tank and a water replenishing tank, the water replenishing tank is connected with the heating tank, a small foam ball controls the communication of the heating tank and the water replenishing tank, the small foam ball drives the piston to move downwards to replenish water to the heating tank when the water level in the heating tank drops, and the small foam ball floats upwards to enable the piston to move upwards when the water level reaches a certain time, so that the communication is closed.
Furthermore, the top of the heating box is provided with a double-open cover, the left cover is provided with two small holes, one is connected with a water replenishing box and the other is connected with an evaporating pot, the right cover is provided with an opening, and the concave mesh cage is used for fixing the water bath generator; the heating box is a water tank with the width and the depth of 750mm by 350mm by 260mm, and a water tank heating rod (DN 50304, thickened stainless steel 380v 12KW) is added.
Further, automatic water supply heating water tank can guarantee that vapor content is sufficient and can not have the condition of burning dry pot, can guarantee the improvement of distillation efficiency under vapor content is sufficient, connects a straight condenser pipe then liquid phase entering extraction device under the evaporating pot and makes our required essential oil further purify, after getting into a water trap, gets into a water bath heating device again and separates out essential oil and extract to reach the effect of integration.
Furthermore, the joint in evaporating pot middle part has the polylith sieve, and the sieve can be followed the retort side and taken out and insert. So that the water vapor was sufficiently accessible to the reactants and the associated straight condenser tube was then available to the laboratory.
Furthermore, the first collector is a glass instrument which is communicated with an upper glass tube, the middle part of the first collector is spherical, the capacity of the first collector is 500ml, and the lower part of the first collector is provided with a piston.
Further, the collector number one, two, three serve as the collector number one, or with a 500ml erlenmeyer flask or beaker.
Further, the extraction device is a three-neck flask, before extraction, extraction liquid is added according to the extracted essential oil, if supplement addition or replacement is needed in the middle, the three-neck flask can be directly added from the other two holes without detaching the device.
Further, the water removal device is a glass instrument of a first collector, and anhydrous sodium sulfate is filled in the glass instrument to remove water in the distillation device.
Furthermore, the water bath generator is a simple distillation device, and the extraction liquid and the essential oil are separated by depending on the temperature of water in the heating box. Since the boiling point of the extract is generally lower than the temperature of the essential oil, and the boiling point of the extract (ethanol, petroleum ether …) which is commonly used by us is lower than 100 ℃, the extract and the essential oil can be separated by steam distillation.
Compared with the prior art, the utility model has the advantages of: the automatic water replenishing technology is added in the experiment, so that the water level is always in a balanced state, the phenomenon of boiling off the pan is prevented, reactants and water vapor are fully contacted, the efficiency is higher, and then follow-up operation does not need to consume a large amount of time and does not need to be switched to other devices, so that the purpose and the efficiency of saving time are achieved. The extraction liquid and the essential oil can be quickly separated, so that the purposes of saving medicines and heat energy are achieved, the utilization rate of experimental energy and the yield and the efficiency of realization are improved, and the operation is more convenient as an integral whole.
Drawings
Fig. 1 is a schematic structural diagram of the present invention.
Fig. 2 is a schematic diagram of the structure of the evaporation tank of the present invention.
Reference numerals: 1-water replenishing tank; 2-foam pellets; 3-heating the box; 4-evaporating pot; 5-straight condenser pipe; 6-collector number one; piston No. 7-one; 8-an extraction device; 9-three ports; receiver number 10-two; 11-a water removal device; 12-a water bath generator; receiver number 13-three.
Detailed Description
The utility model will be further understood by the following examples and the accompanying drawings.
As shown in fig. 1 and 2, the utility model is operated and implemented in this way, a high-efficiency and integrated essential oil distillation device, which mainly comprises a water replenishing tank 1, a foam ball 2, a heating tank 3, an evaporating pot 4, a straight condenser pipe 5, a first collector 6, a first piston 7, an extraction device 8, a three-way port 9, a second receiver 10, a water removal device 11, a water bath generator 12, a third receiver 13 and a straight condenser pipe 5; the method is characterized in that: heating cabinet 3 is connected to moisturizing box 1, the built-in foam bobble 2 that has of heating cabinet 3, moisturizing box 1 and heating cabinet 3 constitute automatic water supply heating water tank, evaporating pot 4 is connected to heating cabinet 3, 4 top right sides of evaporating pot are connected and are straightened condenser pipe 5, No. 6 collectors are connected to straight condenser pipe 5, extraction device 8 is connected to No. 6 collectors, No. 6 collectors and extraction device 8 are equipped with piston 7, No. 9 three-way openings 9 connect down of extraction device 8, No. two receivers 10 are connected to 9 one end of three-way opening, water trap 11 is connected to 9 one end of three-way opening, water bath generator 12 is connected to water bath generator 11, water bath generator 12 connects straight condenser pipe 5, No. three receivers 13 are then connected to straight condenser pipe 5. The joint in evaporating pot middle part has the polylith sieve, and the sieve can be followed the retort side and taken out and insert.
The method specifically comprises the following steps: only raw materials are put into the distillation retort 4, then the heating box 3 is opened, and after the water replenishing box 1 connected with the heating box 3 is filled with water, redundant operation on an instrument is not needed; when the heating box 3 starts to operate, the steam starts to evaporate into the distillation tank 4 after the water reaches a certain temperature, when the water level in the heating box 3 drops, the small ball 2 in the water box drops, the water replenishing device is communicated with the water replenishing box 1, then the water replenishing operation is carried out on the heating box 3, after the water vapor enters the distillation tank 4, the water vapor distillation is carried out on the raw materials, then enters a first collector 6 along a straight condensing pipe 5 and then enters an extraction device 8, mixing with the extractive solution in the extraction device 8, removing water from the extractive solution by a dewatering device 11 if only the lower layer liquid is needed, separating the extractive solution from essential oil in a water bath generator 12 in the heating tank 3, collecting the extractive solution, and collecting the essential oil with high concentration in the water bath generator 12. If the liquid of the lower layer is not needed, the three-port 9 is connected into the second receiver 10, the liquid of the lower layer is discharged firstly, then the three-port 9 is adjusted, and then the operation is carried out.
A first piston 7 is arranged between the first collector 6 and the extraction device 8, the first piston 7 can be opened to enter the continuous extraction device 8 after the liquid in the first collector 6 reaches a certain amount, a three-way port 9 between the continuous extraction device 8 and the water removal device 11 is determined by the required upper layer liquid or lower layer liquid through adjustment, and substances which do not react with the essential oil are also arranged in the water removal device 11 only by achieving the effect of removing water.
The water bath generator 12 is integrated with the heating box 3, the heating box is provided with two small holes on the double-open-cover left cover, one is connected with the water replenishing tank and the other is connected with the evaporating pot, and the right opening is provided with a concave mesh cage for fixing the water bath generator. The effect of saving heat energy is achieved, and the water bath generator is a simple distillation device which can directly separate the extract liquor.
The automatic water replenishing tank 1 is arranged in the heating tank 3, so that the water level can be always kept at a certain level and cannot be reduced, the reactant is wrapped by water vapor, then the heating tank 3 is connected with the distillation retort 4, the water vapor can directly reach the distillation retort 4, the distillation retort 4 is connected with the straight condensation pipe 5, then the distillation tank is connected with the first collector 6, a first piston 7 can be opened after certain liquid is collected in the first collector 6, the liquid in the extraction device 8 enters the lower extraction device 8, the liquid in the extraction device 8 is separated and then enters the lower dewatering device 11 for dewatering, the extracting agent and the essential oil are separated in the water bath generator 12 returning to the heating tank 3, and the third collection tank 13 is connected to collect the distilled extracting agent.
Furthermore, the utilization rate of raw materials of the whole device can be high, and the heat loss is also reduced to be small, so that the aims of high efficiency and convenience are fulfilled.
After further shut down of the apparatus, the recovered extract may be fed to extraction apparatus 8, from which essential oil of high concentration may be obtained, taking out water bath generator 12.
Claims (9)
1. An efficient and integrated essential oil distillation device mainly comprises a water replenishing tank, a small foam ball, a heating box, an evaporating pot, a straight condensing pipe, a first collector, a first piston, an extraction device, a three-way port, a second receiver, a water removal device, a water bath generator and a third receiver; the method is characterized in that: the heating cabinet is connected to the moisturizing case, the heating cabinet embeds there is the foam bobble, moisturizing case and heating cabinet constitute automatic water supply heating water tank, the evaporating pot is connected to the heating cabinet, straight condenser pipe is connected on evaporating pot top right side, No. one collector is connected to straight condenser pipe, an extraction device is connected to the collector, be equipped with the piston No. one between a collector and the extraction device, three openings under the extraction device, No. two receivers are connected to three opening one end, three opening one end water trap, water bath generator is connected to the water trap, straight condenser pipe is connected to water bath generator, No. three receivers are connected to straight condenser pipe.
2. The efficient and integrated essential oil distillation device as claimed in claim 1, wherein: the automatic water replenishing heating water tank is formed by combining a heating tank and a water replenishing tank, the water replenishing tank is connected with the heating tank, a small foam ball controls the communication of the heating tank and the water replenishing tank, the small foam ball drives the piston to move downwards to replenish water to the heating tank when the water level in the heating tank drops, and the small foam ball floats upwards to enable the piston to move upwards when the water level reaches a certain time, so that the communication is closed.
3. A highly efficient integrated essential oil distillation apparatus according to claim 2, wherein: the top of the heating box is provided with a double-open cover, the left cover is provided with two small holes, one is connected with the water replenishing box and the other is connected with the evaporating pot, the right cover is provided with an opening, and the concave mesh cage is used for fixing the water bath generator; the heating box and the water replenishing box are both aluminum alloy water tanks with the width and the height of 750mm 350mm 260mm, and a water tank heating rod is added in the heating box.
4. The efficient and integrated essential oil distillation device as claimed in claim 1, wherein: the joint in evaporating pot middle part has the polylith sieve, and the sieve can be followed the retort side and taken out and insert.
5. The efficient and integrated essential oil distillation device as claimed in claim 1, wherein: the first collector is a glass instrument which is communicated with an upper glass tube, the middle part of the first collector is spherical, the capacity of the first collector is 500ml, and the lower part of the first collector is provided with a piston.
6. An efficient integrated essential oil distilling apparatus according to claim 5, wherein: the first collector, second collector, third collector or 500ml erlenmeyer flask or beaker.
7. The efficient and integrated essential oil distillation device as claimed in claim 1, wherein: the extraction device is a three-neck flask.
8. A high efficiency integrated essential oil distilling apparatus according to claim 1, wherein: the water removal device is a glass instrument of a first collector and is filled with anhydrous sodium sulfate.
9. The efficient and integrated essential oil distillation device as claimed in claim 1, wherein: the water bath generator is a simple distillation device.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202220833540.8U CN217202632U (en) | 2022-04-12 | 2022-04-12 | Efficient and integrated essential oil distillation device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202220833540.8U CN217202632U (en) | 2022-04-12 | 2022-04-12 | Efficient and integrated essential oil distillation device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN217202632U true CN217202632U (en) | 2022-08-16 |
Family
ID=82759588
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202220833540.8U Expired - Fee Related CN217202632U (en) | 2022-04-12 | 2022-04-12 | Efficient and integrated essential oil distillation device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN217202632U (en) |
-
2022
- 2022-04-12 CN CN202220833540.8U patent/CN217202632U/en not_active Expired - Fee Related
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105296163A (en) | Extraction equipment for fragrant plant essential oil and headspace volatile | |
| CN103215135B (en) | Method for synchronously extracting sage clary essential oil and sclareol from sage clary | |
| CN105861256A (en) | Impurity removal and purification system and method for white wine | |
| CN109207262B (en) | Extraction device and extraction method of volatile plant essential oil | |
| CN201485438U (en) | Blumea balsamifera processing and extracting equipment | |
| CN107418979A (en) | A kind of alcohol fuel energy-saving clean production method | |
| CN103585783B (en) | Honeysuckle extraction is steamed extraction element and method | |
| CN205412299U (en) | Multi -functional steam distillation and soxhlet extraction integration experimental apparatus | |
| CN206127245U (en) | Distillation edulcoration device of raw oil | |
| CN217202632U (en) | Efficient and integrated essential oil distillation device | |
| CN201353436Y (en) | Volatile oil extraction device with multi-layer of separation plates | |
| CN110465108A (en) | The multi-functional extraction concentration integrated equipment of one kind and technique | |
| CN204689970U (en) | The parallel extraction element of distillation plants essential oil and hydrosol | |
| CN212102640U (en) | System for preparing acetic anhydride by acetic acid cracking-ketene method | |
| CN201186168Y (en) | Multifunctional machine group for refluxing, extracting and concentrating | |
| CN205501254U (en) | Device that does not have solvent extraction natural fibre essential oil and pure dew fast | |
| CN102260141B (en) | Production method and device of refined glycerin in non-distillation techniques | |
| CN209204719U (en) | A kind of continous way traditional Chinese medicine extraction concentration systems | |
| CN206747231U (en) | A kind of kitchen garbage harmless treatment production line | |
| CN109504724A (en) | Stalk cleans co-production technology | |
| CN216663016U (en) | Re-steaming type wine brewing device | |
| CN209204703U (en) | A kind of reduced steam circulation distilling apparatus | |
| CN206418091U (en) | A kind of oily continuous rectification apparatus of plant material | |
| CN212640424U (en) | Plant extraction system | |
| CN209702693U (en) | A kind of wormwood essential oil extracting device |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20220816 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |