CN201353436Y - Volatile oil extraction device with multi-layer of separation plates - Google Patents
Volatile oil extraction device with multi-layer of separation plates Download PDFInfo
- Publication number
- CN201353436Y CN201353436Y CNU2008202410335U CN200820241033U CN201353436Y CN 201353436 Y CN201353436 Y CN 201353436Y CN U2008202410335 U CNU2008202410335 U CN U2008202410335U CN 200820241033 U CN200820241033 U CN 200820241033U CN 201353436 Y CN201353436 Y CN 201353436Y
- Authority
- CN
- China
- Prior art keywords
- volatile oil
- heater
- oil extraction
- insulating panel
- multilayer insulating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000000341 volatile oil Substances 0.000 title claims abstract description 42
- 238000000605 extraction Methods 0.000 title claims abstract description 33
- 238000000926 separation method Methods 0.000 title abstract description 7
- 239000000463 material Substances 0.000 claims abstract description 23
- 238000010438 heat treatment Methods 0.000 claims abstract description 17
- 239000002904 solvent Substances 0.000 claims abstract description 15
- 239000003921 oil Substances 0.000 claims abstract description 7
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 239000000126 substance Substances 0.000 abstract description 2
- 230000001174 ascending effect Effects 0.000 abstract 2
- 238000004321 preservation Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 238000009833 condensation Methods 0.000 description 5
- 230000005494 condensation Effects 0.000 description 5
- 239000000284 extract Substances 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 239000010410 layer Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 239000011229 interlayer Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 230000000630 rising effect Effects 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- 238000001256 steam distillation Methods 0.000 description 2
- 241000208125 Nicotiana Species 0.000 description 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 1
- 239000003125 aqueous solvent Substances 0.000 description 1
- 235000019504 cigarettes Nutrition 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000006837 decompression Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
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Abstract
The utility model discloses a volatile oil extraction device with multi-layer of separation plates, which belongs to the technical field of the chemicals extraction equipment, and comprises a condenser, a volatile oil extraction separator and a heater, wherein at least two layers of mesh separation plates which are arranged above the solvent and can carry the extracted materials are arranged inside the heater. The quantity of the layers of the mesh separation plate which can carry the extracted materials is 2 to 12. The aperture of the mesh separation plate which can carry the extracted materials is 10 to 100 meshes. An ascending pipe of the volatile oil extraction separator is provided with a heat-preservation sleeve. The bottom part of the heater is provided with a heating sleeve, and the heating sleeve is communicated with a digital display control instrument. The angle which is formed between the ascending pipe and a collecting pipe is 30 to 40 degrees. The volatile oil extraction device has reasonable design and simple structure, and can separate the materials and the solution through the multi-layer of separation plates, and has large processing capacity, high extraction efficiency and high oil output, and has almost the same production conditions with the real production conditions, and can be used for searching the production conditions.
Description
Technical field
The utility model belongs to the chemical extraction equipment technical field, is specifically related to a kind of extraction separator that is used to extract volatile oil that material and solvent are separated.
Background technology
Plant volatile oil all has important application in industries such as tobacco, medicine, essence, spices, cosmetics in the prior art, and extraction separates and obtains from plant usually.At present, industrial volatile oil extractor commonly used is to adopt conventional steam distillation device, and this device is unfavorable for that the extraction of low-content volatile oil in the plant separates.Volatile oil extraction separator is that volatile oil extracts most important parts in the separator, present volatile oil extraction separator adopts conventional steam distillation device, partly constitute by condenser pipe, steam generator, glove container etc., there are deficiencies such as structure is too simple, extraction efficiency is low in this structure, in addition, material distills in water, also can cause certain destruction to some volatile ingredient in the material, is unfavorable for the collection of some feature volatile ingredient.
The utility model content
Above-mentioned deficiency at prior art, the technical problems to be solved in the utility model provides a kind of volatile oil extractor with multilayer insulating panel, it will be extracted material and solvent separates, can not damage its volatile ingredient, and operate more conveniently and simple, help the collection of volatile oil.
The technical solution of the utility model is: the volatile oil extractor with multilayer insulating panel contains condenser, volatile oil extraction separator, heater, is provided with at least 2 in the described heater and is placed on the mesh dividing plate that carrying on the solvent is extracted material.The mesh dividing plate that described carrying is extracted material is 2～12 layers.The aperture that described carrying is extracted the mesh dividing plate of material is 10～100 orders.The tedge of volatile oil extraction separator is provided with muff.The angle number of degrees of tedge and collecting pipe are the 30-40 degree.Be provided with heating jacket in heater base, heating jacket is connected with digital display controller.Described heating jacket is the double glazing heating jacket of oil bath heating.
The utility model is reasonable in design, simple in structure, multilayer insulating panel is set in this device separates material and solution, extract solvent and can extract multilayer dose simultaneously through heating generation steam, material and separated from solvent, the material handling amount is big, the extraction efficiency height, the oil yield height, close with actual production conditions, can be used for groping working condition.
Description of drawings
Accompanying drawing acceptance of the bid keep the score state as follows: 1-U type conduit; The 2-condenser; The 3-tedge; The 4-muff; The 5-valve; The 6-volatile oil extraction separator; The 7-adapter; 8,9,10-mesh dividing plate; The 11-solvent; The 12-valve; The 13-collecting pipe; 14-communicating pipe; The 15-valve; The 16-receiving flask; The 17-heater; The 18-heating jacket; The 19-digital display controller.
The specific embodiment
Below in conjunction with accompanying drawing the specific embodiment of the present utility model is described in further detail.As shown in Figure 1, the volatile oil extractor with multilayer insulating panel of the present utility model adopts heater 17 to connect volatile oil extraction separator 6, realizes extracting continuously, and volatile oil is realized separating by condenser 2 condensed layerings with steam.Realize many valve controls, valve-off 15 is opened valve 5 and valve 12, can realize that the extraction of volatile oil separates; Valve-off 5 and valve 12 can be realized the distillation extraction or the decompression distillation of material are extracted.
This device has clear superiority on the continuity of validity that guarantees Separation of Solid and Liquid and extraction, not only simple to operate, and makes whole extraction efficiency be greatly improved.Have efficiently characteristics simple to operate.Be fit to the extraction of volatile oil, thereby be particularly suitable for the extraction preparation of essence spice for cigarette.
This device is made of heater 17, volatile oil extraction separator 6 and condenser 2, each several part is described below respectively: heater 17 is to be used for containing solvent and material, solvent contacts with heating jacket 18 interlayers, by the temperature in the heat exchange realization control heater 17, temperature controlling range is spent between 350 degree subzero 80, can accurately control; Temperature in 19 pairs of leaching process of digital display temperature controller is monitored in real time, accurately writes down the temperature in the heater 17; Add last layer thermal insulating cover 4 around the tedge 3 of volatile oil extraction separator 6, be beneficial to the rising of steam, avoid too early condensation and reflux, guarantee the yield of volatile oil; Solvent and volatile oil steam that 2 pairs of heating of condenser produce carry out condensation, drip in the collecting pipe 13.
The basic principle of this device is: dress extracts solvent and material in the heater 17, injects aqueous solvent in heater 17, places material on the multilayer mesh dividing plate 8,9,10 that is positioned on the solvent; During extraction, open valve 5 and valve 12, valve-off 15; After conduction oil in heating jacket 18 interlayers of heater 17 heats by oil heater, realize the temperature control of solvent in the heater 17 by heat exchange; Solvent vaporization back produces water vapour, and material is carried out steam extraction, by volatile oil extraction separator 6, enters condenser 2, splashes into after the condensation in the collecting pipe 13; Usually phytovolatilization oil ratio water is light, and water vapour and volatile oil are through forming layering in collecting pipe after the condensation, and water level is in lower floor, and volatile oil is positioned at the upper strata; Along with the carrying out of extracting, the liquid level in the collecting pipe is more and more higher, and when liquid level reached the high-end height of communicating pipe 14, condensed water just was back in the heater; After treating that whole extraction is finished, open valve 15,, collect the volatile oil that obtains with receiving flask 16 then the water emptying of lower floor.
Multilayer insulating panel described in the utility model can have the 3-12 layer, even more.Described mesh dividing plate, its hole can be square hole or circular hole and other difform holes, and the size in hole is difficult for falling with material is advisable, and the 10-100 order all can.Described thermal insulation casing 4 is to wrap up one deck thermal insulating cover around tedge 3, prevent that heat scatters and disappears, reduce steam condensation too early in uphill process and form backflow and cause the volatile oil yield to reduce, in addition, the angle number of degrees of thermal insulation casing and collecting pipe are beneficial to the rising of steam at the 30-40 degree.
Claims (7)
1, a kind of volatile oil extractor with multilayer insulating panel, contain condenser, volatile oil extraction separator, heater, it is characterized in that: be provided with at least 2 in the described heater (17) and be placed on the mesh dividing plate (8,9,10) that carrying on the solvent is extracted material.
2, the volatile oil extractor with multilayer insulating panel according to claim 1 is characterized in that: the mesh dividing plate (8,9,10) that described carrying is extracted material is 2～12 layers.
3, the volatile oil extractor with multilayer insulating panel according to claim 1 is characterized in that: the aperture that described carrying is extracted the mesh dividing plate (8,9,10) of material is 10～100 orders.
4, the volatile oil extractor with multilayer insulating panel according to claim 1 is characterized in that: the tedge (3) of volatile oil extraction separator (6) is provided with muff (4).
5, the volatile oil extractor with multilayer insulating panel according to claim 4 is characterized in that: tedge (3) is the 30-40 degree with the angle number of degrees of collecting pipe (13).
6, the volatile oil extractor with multilayer insulating panel according to claim 1 is characterized in that: be provided with heating jacket (18) in heater (17) bottom, heating jacket (18) is connected with digital display controller (19).
7, the volatile oil extractor with multilayer insulating panel according to claim 6 is characterized in that: described heating jacket (18) is the double glazing heating jacket of oil bath heating.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2008202410335U CN201353436Y (en) | 2008-12-26 | 2008-12-26 | Volatile oil extraction device with multi-layer of separation plates |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNU2008202410335U CN201353436Y (en) | 2008-12-26 | 2008-12-26 | Volatile oil extraction device with multi-layer of separation plates |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201353436Y true CN201353436Y (en) | 2009-12-02 |
Family
ID=41409776
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNU2008202410335U Expired - Fee Related CN201353436Y (en) | 2008-12-26 | 2008-12-26 | Volatile oil extraction device with multi-layer of separation plates |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN201353436Y (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102350072A (en) * | 2011-09-02 | 2012-02-15 | 江苏斯威森生物医药工程研究中心有限公司 | Vacuum reduced pressure concentration system |
| CN103877741A (en) * | 2012-12-19 | 2014-06-25 | 江苏飞亚化学工业有限责任公司 | Condensing reflux distributor |
| CN104812453A (en) * | 2012-06-21 | 2015-07-29 | 阿罗马托尔有限责任公司 | Distillation apparatus for extraction of essential oils and hydrosols from plant matter within a capsule |
| CN105038992A (en) * | 2015-09-01 | 2015-11-11 | 湖南时代阳光药业股份有限公司 | Multifunctional volatile oil distilling and extracting tank |
| CN107400562A (en) * | 2017-09-03 | 2017-11-28 | 南京同仁堂黄山精制药业有限公司 | A kind of ethereal oil collection device and method |
| CN109609280A (en) * | 2019-02-19 | 2019-04-12 | 重庆中烟工业有限责任公司 | Plants essential oil distills extraction element |
-
2008
- 2008-12-26 CN CNU2008202410335U patent/CN201353436Y/en not_active Expired - Fee Related
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102350072A (en) * | 2011-09-02 | 2012-02-15 | 江苏斯威森生物医药工程研究中心有限公司 | Vacuum reduced pressure concentration system |
| CN104812453A (en) * | 2012-06-21 | 2015-07-29 | 阿罗马托尔有限责任公司 | Distillation apparatus for extraction of essential oils and hydrosols from plant matter within a capsule |
| CN105907470A (en) * | 2012-06-21 | 2016-08-31 | 阿罗马托尔有限责任公司 | Distillation apparatus for extraction of essential oils and hydrosols from plant matter within a capsule |
| US9956501B2 (en) | 2012-06-21 | 2018-05-01 | Aromator Llc | Distillation apparatus for extraction of essential oils and hydrosols from plant matter within a capsule |
| CN105907470B (en) * | 2012-06-21 | 2020-02-04 | 阿罗马托尔有限责任公司 | Distillation apparatus for extracting essential oils and hydrosols from plant matter in a container |
| CN103877741A (en) * | 2012-12-19 | 2014-06-25 | 江苏飞亚化学工业有限责任公司 | Condensing reflux distributor |
| CN105038992A (en) * | 2015-09-01 | 2015-11-11 | 湖南时代阳光药业股份有限公司 | Multifunctional volatile oil distilling and extracting tank |
| CN107400562A (en) * | 2017-09-03 | 2017-11-28 | 南京同仁堂黄山精制药业有限公司 | A kind of ethereal oil collection device and method |
| CN109609280A (en) * | 2019-02-19 | 2019-04-12 | 重庆中烟工业有限责任公司 | Plants essential oil distills extraction element |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20091202 Termination date: 20141226 |
|
| EXPY | Termination of patent right or utility model |