CN217189601U - Batching and reaction integrated equipment for water-oxygen sensitive material - Google Patents
Batching and reaction integrated equipment for water-oxygen sensitive material Download PDFInfo
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- CN217189601U CN217189601U CN202221150878.XU CN202221150878U CN217189601U CN 217189601 U CN217189601 U CN 217189601U CN 202221150878 U CN202221150878 U CN 202221150878U CN 217189601 U CN217189601 U CN 217189601U
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Abstract
The utility model relates to the technical field of integrated production equipment of an operation box and a reaction kettle, and discloses integrated equipment for proportioning and reacting a water-oxygen sensitive material; the utility model discloses carry out closed connection with inert gas control box and reation kettle through material conveyor, in order to ensure to accomplish in the control box can get into reation kettle under the influence of moisture and oxygen after the proportion of water oxygen sensitive material, the process continuity is high, work efficiency has been promoted, and set up the valve between each subassembly, through closing the valve in order to ensure that single subassembly does not communicate with other subassemblies, can open the breather valve this moment, make the inside gas of vacuum pump extraction subassembly, make the inert gas circulation in the inert gas steel bottle get into this subassembly, can not receive the influence that comes from the outside air in ensureing the integration equipment through this kind of mode, the problem that the sensitive material of water oxygen shifts to reation kettle's in-process easy contact air from the inert gas control box among the prior art and leads to the material inefficacy is solved.
Description
Technical Field
The utility model belongs to the technical field of the technique of control box, reation kettle integration production facility and specifically relates to a batching and reaction integration equipment of sensitive material of water oxygen.
Background
In the production of medicine, new energy and semiconductor industries, materials and production processes sensitive to water vapor and oxygen are often used, in order to avoid negative influence of the water vapor and the oxygen on the water-oxygen sensitive materials in the production process, an inert gas operation box is often used for removing oxygen, moisture and other active gases in the air, an operation environment mainly comprising an inert atmosphere is created, and weighing, configuration and other operations of the materials are performed under the environment.
The materials need to react in a reaction kettle, at present, the reaction kettle is usually prevented from being deteriorated due to contact with the external environment by two modes, the first mode is to put the reaction kettle into an inert gas operation box for operation, and the first mode has the defects that the volume of the reaction kettle is limited by the volume of the inert gas operation box, and partial operation in the inert gas operation box is limited, such as high-temperature reaction; the second mode is to take out the water-oxygen sensitive material from the inert gas operation box, place the material into a special container, transfer the water-oxygen sensitive material through the special container, take out the water-oxygen sensitive material from the special container, place the material into a reaction kettle, and the shortcoming of this mode lies in that the operation is tedious, and has the risk that the contact with the outside air leads to the water-oxygen sensitive material to lose efficacy.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a batching and reaction integration equipment of water oxygen sensitive material aims at solving among the prior art water oxygen sensitive material and shifts to reation kettle's in-process easy contact air from the inert gas control box and lead to the problem of material inefficacy.
The utility model discloses a realize like this, this use is novel to provide a batching and reaction integration equipment of water oxygen sensitive material, include:
the device comprises a feeding device, an inert gas operation box, a material conveying device, a reaction kettle, a material collecting device, an inert gas steel cylinder, a vacuum pump assembly and a ventilation valve assembly;
the feeding device, the inert gas operation box, the material conveying device, the reaction kettle and the material collecting device are sequentially connected, wherein the material collecting device is arranged below the reaction kettle;
the vacuum pump assembly comprises a first vacuum pump, a second vacuum pump and a third vacuum pump;
the vent valve assembly comprises a first vent valve, a second vent valve, a third vent valve, a fourth vent valve, a fifth vent valve and a sixth vent valve;
the first vacuum pump, the second vacuum pump and the third vacuum pump are respectively connected with the first vent valve and the feeding device, the second vent valve and the material conveying device, and the third vent valve and the reaction kettle through vent pipelines;
the inert gas steel cylinder is respectively connected with the fourth vent valve and the feeding device, the fifth vent valve and the inert gas operation box, and the sixth vent valve and the material conveying device through vent pipelines.
In one embodiment, the device further comprises a water oxygen detection device, and the water oxygen detection device is connected with the inert gas operation box.
In one embodiment, the apparatus further comprises a temperature control device, the temperature control device comprising:
a temperature control terminal and a heating resistance wire;
the temperature control terminal comprises a power supply and an operation panel, the temperature control terminal is arranged at the outer end of the reaction kettle, the heating resistance wires are arranged inside the side surface and the bottom surface of the reaction kettle, and the temperature control terminal is electrically connected with the heating resistance wires.
In one embodiment, the material conveying device comprises a material conveying pipeline, a feeding valve, a discharging valve and a belt conveyor;
the feeding valve and the discharging valve are arranged at two ends of the material conveying pipeline, and the belt conveyor is arranged on the bottom surface of the material conveying pipeline.
In one embodiment, a stirring device is arranged inside the reaction kettle, the stirring device comprises a motor and a stirrer, the stirrer comprises a connecting rod body and a stirring piece, two ends of the connecting rod body are respectively connected with the motor and the stirring piece, and the stirring piece is in a fan shape.
In one embodiment, a material collecting bin valve is arranged between the reaction kettle and the material collecting bin.
In one embodiment, a control box valve is arranged between the feeding device and the inert gas control box.
In one of the embodiments, the feeding device is provided with a feeding device valve.
In one embodiment, the inert gas enclosure comprises a CLX1 type inert gas enclosure.
In one embodiment, the autoclave comprises a SS-20L autoclave.
Compared with the prior art, the utility model connects the inert gas operation box and the reaction kettle in a closed way through the material conveying device, so as to ensure that the water-oxygen sensitive material can enter the reaction kettle without being influenced by moisture and oxygen after the proportioning of the water-oxygen sensitive material is finished in the operation box, the process continuity is high, the working efficiency is improved, and valves are arranged among the components, the valves are closed to ensure that the single component is not communicated with other components, at the moment, the vent valve can be opened to enable the vacuum pump to extract gas in the component and enable the inert gas in the inert gas steel cylinder to flow into the component, by the method, the integrated equipment is prevented from being influenced by external air, and the problem that materials are invalid due to the fact that water and oxygen sensitive materials are easy to contact with air in the process of transferring the materials from the inert gas operation box to the reaction kettle in the prior art is solved.
Drawings
FIG. 1 is a schematic structural view of a dosing and reaction integrated device for a water oxygen sensitive material provided by an embodiment of the present invention;
fig. 2 is a schematic structural view of a material conveying device of a batching and reaction integrated device for water and oxygen sensitive materials provided by an embodiment of the present invention.
Reference numerals: 1-feeding device, 2-inert gas operation box, 3-material conveying device, 4-reaction kettle, 5-material collecting device, 6-inert gas steel cylinder, 7-vacuum pump assembly, 8-vent valve assembly, 71-first vacuum pump, 72-second vacuum pump, 73-third vacuum pump, 81-first vent valve, 82-second vent valve, 83-third vent valve, 84-third vent valve, 85-fifth vent valve, 86-sixth vent valve, 9-water oxygen detecting device, 10-temperature control device, 101-temperature control terminal, 102-heating resistance wire, 31-material conveying pipeline, 32-feeding valve, 33-discharging valve, 34-belt conveyor, 11-stirring device, 111-motor, 112-agitator, 1121-connecting rod body, 1122-agitating piece, 50-material collecting cabin valve, 20-operation box valve and 10-feeding device valve.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more clearly understood, the present invention will be further described in detail with reference to the accompanying drawings and embodiments. It should be understood that the specific embodiments described herein are for purposes of illustration only and are not intended to limit the invention.
The same or similar reference numerals in the drawings of the present embodiment correspond to the same or similar components; in the description of the present invention, it should be understood that if there are the terms "upper", "lower", "left", "right", etc. indicating the orientation or positional relationship based on the orientation or positional relationship shown in the drawings, it is only for convenience of description and simplification of the description, but it is not intended to indicate or imply that the device or element referred to must have a specific orientation, be constructed in a specific orientation, and be operated, and therefore the terms describing the positional relationship in the drawings are only for illustrative purposes and are not to be construed as limitations of the present patent, and those skilled in the art can understand the specific meanings of the terms according to specific situations.
The following describes the implementation of the present invention in detail with reference to specific embodiments.
Referring to fig. 1, fig. 1 is a schematic structural diagram of a batching and reaction integrated device for a water-oxygen sensitive material according to an embodiment of the present invention:
this use is novel to provide a batching and reaction integration equipment of water oxygen sensitive material, include:
the device comprises a feeding device 1, an inert gas operation box 2, a material conveying device 3, a reaction kettle 4, a material collecting device 5, an inert gas steel cylinder 6, a vacuum pump assembly 7 and a ventilation valve assembly 8.
Specifically, feed arrangement 1, inert gas operation box 2, material conveyor 3, reation kettle 4 and material collection device 5 connect gradually the setting, and water oxygen sensitive material gets into integrated equipment from feed arrangement 1, accomplishes the batching in inert gas operation box 2, and the reaction takes place in getting into reation kettle 4 via material conveyor 3 again, and the residual after the reaction will get into the material collection device 5 that sets up in reation kettle 4 below, and the extra change that water oxygen sensitive material leads to because of the contact air has been avoided in whole process.
More specifically, the vacuum pump assembly 7 includes a first vacuum pump 71, a second vacuum pump 72, and a third vacuum pump 73; the vent valve assembly 8 comprises a first vent valve 81, a second vent valve 82, a third vent valve 83, a fourth vent valve 84, a fifth vent valve 85 and a sixth vent valve 86; the first vacuum pump 71, the second vacuum pump 72 and the third vacuum pump 73 are respectively connected with the feeding device 1, the material conveying device 3 and the reaction kettle 4 through a first vent valve 81, a second vent valve 82 and a third vent valve 83, namely, the first vacuum pump 71 is connected with the feeding device 1 through the first vent valve 81, the second vacuum pump 72 is connected with the material conveying device 3 through the second vent valve 82, and the third vacuum pump 73 is connected with the reaction kettle 4 through the third vent valve 83; more specifically, a vacuum pump refers to a device or apparatus for obtaining a vacuum by mechanically, physically, chemically or physico-chemically pumping a pumped container, and it is understood that a vacuum pump is an apparatus for improving, generating and maintaining a vacuum in a certain closed space by various methods.
More specifically, the inert gas cylinder 6 is connected to the feeding device 1, the inert gas operation box 2 and the material conveying device 3 through a fourth vent valve 84, a fifth vent valve 85 and a sixth vent valve 86; namely, the inert gas steel cylinder 6 is connected with the feeding device 1 through a fourth vent valve 84, connected with the inert gas operation box 2 through a fifth vent valve 85, and connected with the material conveying device 3 through a sixth vent valve 86; more specifically, the inert gas cylinder 6 is used to store the inert gas in a high compressed state, and the inert gas does not react with the water oxygen sensitive material, and it is understood that operating the water oxygen sensitive material in an inert gas filled environment can ensure that the water oxygen sensitive material does not undergo additional changes.
More specifically, the first vent valve 81, the second vent valve 82, the third vent valve 83, the fourth vent valve 84, the fifth vent valve 85, and the sixth vent valve 86 are all disposed on vent pipes, the vent pipes are respectively connected to the feeding device 1, the inert gas operation box 2, the material conveying device 3, and the reaction kettle 4, and the gas is circulated through the vent pipes.
More specifically, the shape of the feeding device 1 is a closed cabin body, the feeding device 1 is provided with a feeding device valve 10 communicated with the outside, after the feeding device valve 10 is opened, the non-unsealed and packaged water and oxygen sensitive material is placed into the cabin body, and then the feeding device valve 10 is closed, it can be understood that air enters the feeding device 1 in the process of opening the feeding device valve 10, and the air cannot influence the water and oxygen sensitive material because the package of the water and oxygen sensitive material is not unsealed at the time.
More specifically, after the feeding device valve 10 is closed, the first vent valve 81 is opened to enable the first vacuum pump 71 to start gas extraction from the feeding device 1, when the pressure inside the feeding device 1 is reduced to 10-2 to 10-3mbar, the first vent valve 81 is closed, at this time, the mixed air is clear when the cabin door is opened, the fourth vent valve 84 is opened, the inert gas in the inert gas cylinder 6 will flow into the feeding device 1 due to uneven pressure, and when a certain amount of inert gas is supplemented into the feeding device 1, the fourth vent valve 84 is closed when the pressures in the feeding device 1 and the inert gas operation box 2 are consistent.
More specifically, the inert gas operation box 2 is provided with a pair of operation gloves into which the user can insert both hands to operate the inside of the inert gas operation box 2, that is, the inert gas operation box 2 is provided with a pair of openings, the openings are provided with operation gloves into which the user can insert both hands, and the operation gloves are made of rubber and tightly connected with the openings, so that the inert gas operation box 2 is in an internally closed state, and the user can operate the inside through the operation gloves; more specifically, the operation box valve 20 is provided at a position where the inert gas operation box 2 is connected to the feeding device 1, and after the fourth vent valve 84 is closed, the user opens the operation box valve 20 through the operation gloves, transfers the water and oxygen sensitive material in the feeding device 1 to the inert gas operation box 2, and closes the operation box valve 20.
More specifically, the inert gas operation box 2 has a structure for a user to observe the inside, such as a glass window; after the water and oxygen sensitive material is transferred into the inert gas operation box 2, a user can unseal the water and oxygen sensitive material through the operation gloves, and it can be understood that the inert gas operation box 2 is filled with inert gas without oxygen and moisture, so that no additional reaction occurs after the water and oxygen sensitive material is unsealed; more specifically, the water and oxygen sensitive materials put into the reaction vessel 4 need to be proportioned in a ratio required for the experiment, and therefore, the water and oxygen sensitive materials need to be weighed and proportioned in the inert gas operation box 2.
Referring to fig. 2, fig. 2 is a schematic structural diagram of a material conveying device 3 of a batching and reaction integrated device for water and oxygen sensitive materials according to an embodiment of the present invention:
more specifically, the material conveying device 3 comprises a material conveying pipeline 31, a feeding valve 32, a discharging valve 33 and a belt conveyor 34, wherein the feeding valve 32 and the discharging valve 33 are arranged at two ends of the material conveying pipeline 31, it can be understood that the feeding valve 32 is arranged at a position where the material conveying device 3 is connected with the inert gas operation box 2, and the discharging valve 33 is arranged at a position where the material conveying device 3 is connected with the reaction kettle 4; the belt conveyor 34 is disposed on the bottom surface of the material conveying pipe 31, and the belt conveyor 34 is a conveying device having a conveyor belt thereon, which is moved from the initial stage to the final stage by the motor 111, so that the material placed on the conveyor belt is also moved along with the movement of the conveyor belt.
More specifically, after the weighing and proportioning of the water and oxygen sensitive material are completed in the inert gas operation box 2, the feed valve 32 is opened, the water and oxygen sensitive material is placed on the belt conveyor 34, the feed valve 32 is closed and the discharge valve 33 is opened, the belt conveyor 34 conveys the water and oxygen sensitive material to the reaction kettle 4, and the discharge valve 33 is closed.
More specifically, after the discharge valve 33 is closed, the water-oxygen sensitive material enters the reaction kettle 4, the water-oxygen sensitive material reacts in the reaction kettle 4, after the reaction is completed, the material collecting bin valve 50 arranged between the material collecting device 5 and the reaction kettle 4 is opened, the residual product after the reaction is completed enters the material collecting bin, the third air valve 83 is opened, the gas in the reaction kettle 4 is extracted from the reaction kettle 4 through the third vacuum valve, so as to extract the gas generated after the reaction of the water-oxygen sensitive material, and the reaction kettle 4 is recovered to the state of only inert gas.
More specifically, the material conveying device 3 is connected with the second vacuum pump 72 through a second vent valve 82, and is communicated with the inert gas cylinder 6 through a fifth vent valve 85; it will be appreciated that at regular intervals, the second vent valve 82 may be opened to allow internal gas to be drawn from the material delivery device 3 using the second vacuum pump 72, and then the fifth vent valve 85 opened to allow the inert gas from the inert gas cylinder 6 to enter the material delivery device 3; more specifically, the discharge valve 33 between the material conveying device 3 and the reaction kettle 4 may be opened at this time, so that the material conveying device 3 and the reaction kettle 4 are communicated, and the inert gas in the inert gas steel cylinder 6 is communicated to the reaction kettle 4, so as to supplement the inert gas to the reaction kettle 4.
In the embodiment, the utility model connects the inert gas operation box 2 and the reaction kettle 4 in a closed way through the material conveying device 3, so as to ensure that the water-oxygen sensitive material can enter the reaction kettle 4 without being influenced by moisture and oxygen after the proportioning of the water-oxygen sensitive material is finished in the operation box, the process continuity is high, the working efficiency is improved, and valves are provided between each component to ensure that a single component is not communicated with other components by closing the valves, at this time, the vent valve can be opened to allow the vacuum pump to draw gas inside the component, allow the inert gas in the inert gas cylinder 6 to flow into the component, by the method, the integrated equipment is prevented from being influenced by external air, and the problem that materials are invalid due to the fact that water and oxygen sensitive materials are easy to contact with air in the process of transferring the materials from the inert gas operation box 2 to the reaction kettle 4 in the prior art is solved.
In some embodiments, a water oxygen detection device 9 is also included.
Specifically, the water oxygen detecting device 9 is connected to the inert gas operation box 2 through a pipeline, that is, the gas in the inert gas operation box 2 flows to the water oxygen detecting device 9 through the pipeline, and more specifically, a sensor for detecting moisture and oxygen is arranged in the water oxygen detecting device 9, and the moisture and oxygen in the gas can be detected to determine whether the gas in the inert gas operation box 2 can cause adverse effects on the water oxygen sensitive material.
In some embodiments, a temperature control device 10 is also included.
Specifically, the temperature control device 10 includes a temperature control terminal 101 and a heating resistance wire 102; more specifically, the temperature control terminal 101 is arranged at the outer end of the reaction kettle 4, and the heating resistance wire 102 is arranged inside the side surface and the bottom surface of the reaction kettle 4, that is, the heating resistance wire 102 is arranged inside the side wall of the reaction kettle 4; more specifically, the temperature controlled terminal 101 and the heating resistance wire 102 are electrically connected.
More specifically, the temperature control terminal 101 includes a power supply for supplying power to the heating resistance wire 102 to heat the heating resistance wire 102, so as to raise the temperature inside the reaction vessel 4, and an operation panel for controlling the magnitude and time of the power supply output to control the temperature inside the reaction vessel 4.
More specifically, the temperatures required for the reaction of different types of water and oxygen sensitive materials are different, so after the water and oxygen sensitive materials are not put into the reaction kettle 4, the temperature of the reaction kettle 4 needs to be set through the temperature control terminal 101, and the temperature of the reaction kettle 4 needs to be adjusted to the temperature suitable for the reaction of the water and oxygen sensitive materials.
In some embodiments, a stirring device 11 is disposed inside the reaction kettle 4.
Specifically, the stirring device 11 includes an electric motor 111 and a stirrer 112, the stirrer 112 is connected to the electric motor 111, and the electric motor 111 is electrically connected to the stirrer 112, it is understood that the electric motor 111 has a power source and a rotation motor, the power source provides power to the rotation motor, the rotation motor can rotate, and the rotation of the rotation motor drives the rotation of the stirrer 112 due to the connection between the stirrer 112 and the electric motor 111.
More specifically, the agitator 112 includes a connection rod 1121 and an agitator 1122, and one end of the connection rod 1121 is connected to the motor 111 and the other end is connected to the agitator 1122, so that the motor 111 can drive the agitator 1122 to rotate, and more specifically, the agitator 1122 can be provided in various shapes, such as a fan shape, a rectangular plate shape, a cylindrical shape, and the like.
More specifically, the stirrer 112 is used for stirring the gas inside the reaction tank 4 to accelerate the uniform mixing of the gas inside the reaction tank 4, thereby accelerating the reaction of the water-oxygen sensitive material.
In some examples, the inert gas cabinet was a CLX1 type inert gas cabinet and the autoclave was a SS-20L autoclave.
The above description is only exemplary of the present invention and should not be taken as limiting the scope of the present invention, as any modifications, equivalents, improvements and the like made within the spirit and principles of the present invention are intended to be included within the scope of the present invention.
Claims (10)
1. The integrated equipment for proportioning and reacting water and oxygen sensitive materials is characterized by comprising:
the device comprises a feeding device, an inert gas operation box, a material conveying device, a reaction kettle, a material collecting device, an inert gas steel cylinder, a vacuum pump assembly and a ventilation valve assembly;
the feeding device, the inert gas operation box, the material conveying device, the reaction kettle and the material collecting device are sequentially connected, wherein the material collecting device is arranged below the reaction kettle;
the vacuum pump assembly comprises a first vacuum pump, a second vacuum pump and a third vacuum pump;
the vent valve assembly comprises a first vent valve, a second vent valve, a third vent valve, a fourth vent valve, a fifth vent valve and a sixth vent valve;
the first vacuum pump, the second vacuum pump and the third vacuum pump are respectively connected with the first vent valve, the feeding device, the second vent valve, the material conveying device and the third vent valve and the reaction kettle through vent pipelines;
the inert gas steel cylinder is respectively connected with the fourth vent valve and the feeding device, the fifth vent valve and the inert gas operation box, and the sixth vent valve and the material conveying device through vent pipelines.
2. The integrated apparatus for proportioning and reacting water and oxygen sensitive material according to claim 1, further comprising a water and oxygen detecting device, wherein the water and oxygen detecting device is connected to the inert gas operation box.
3. The integrated apparatus for dosing and reacting a water-oxygen sensitive material according to claim 1, further comprising a temperature control device, wherein the temperature control device comprises:
a temperature control terminal and a heating resistance wire;
the temperature control terminal comprises a power supply and an operation panel, the temperature control terminal is arranged at the outer end of the reaction kettle, the heating resistance wires are arranged inside the side surface and the bottom surface of the reaction kettle, and the temperature control terminal is electrically connected with the heating resistance wires.
4. The integrated apparatus for proportioning and reacting water and oxygen sensitive material according to claim 1, wherein the material conveying device comprises a material conveying pipeline, a feeding valve, a discharging valve and a belt conveyor;
the feeding valve and the discharging valve are arranged at two ends of the material conveying pipeline, and the belt conveyor is arranged on the bottom surface of the material conveying pipeline.
5. The integrated equipment for proportioning and reacting water and oxygen sensitive materials according to claim 1, wherein a stirring device is arranged in the reaction kettle, the stirring device comprises a motor and a stirrer, the stirrer comprises a connecting rod body and a stirring piece, two ends of the connecting rod body are respectively connected with the motor and the stirring piece, and the stirring piece is in a fan shape.
6. The integrated apparatus for proportioning and reacting water and oxygen sensitive material according to claim 1, wherein a valve of the material collecting bin is arranged between the reaction kettle and the material collecting bin.
7. The integrated apparatus for dosing and reacting a water and oxygen sensitive material according to claim 1, wherein a chamber valve is disposed between said feeding means and said inert gas chamber.
8. The integrated apparatus for dosing and reacting a water and oxygen sensitive material according to claim 1, wherein the feeding device is provided with a feeding device valve.
9. The integrated apparatus for dosing and reacting a water oxygen sensitive material as claimed in claim 1 wherein the inert gas enclosure comprises a CLX1 type inert gas enclosure.
10. The integrated apparatus for dosing and reacting a water and oxygen sensitive material of claim 1 wherein the reaction vessel comprises a SS-20L reaction vessel.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202221150878.XU CN217189601U (en) | 2022-05-14 | 2022-05-14 | Batching and reaction integrated equipment for water-oxygen sensitive material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202221150878.XU CN217189601U (en) | 2022-05-14 | 2022-05-14 | Batching and reaction integrated equipment for water-oxygen sensitive material |
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| Publication Number | Publication Date |
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| CN217189601U true CN217189601U (en) | 2022-08-16 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202221150878.XU Active CN217189601U (en) | 2022-05-14 | 2022-05-14 | Batching and reaction integrated equipment for water-oxygen sensitive material |
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| CN (1) | CN217189601U (en) |
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