CN209576659U - A kind of drug synthetic reaction kettle device - Google Patents

A kind of drug synthetic reaction kettle device Download PDF

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Publication number
CN209576659U
CN209576659U CN201822133458.0U CN201822133458U CN209576659U CN 209576659 U CN209576659 U CN 209576659U CN 201822133458 U CN201822133458 U CN 201822133458U CN 209576659 U CN209576659 U CN 209576659U
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reaction chamber
casing
reaction
air pump
reaction box
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李思阳
王卫兵
孔庆新
朱吉人
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JIANGSU ZHENGDA QINGJIANG PHARMACEUTICAL CO Ltd
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Jiangsu Food and Pharmaceutical Science College
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Abstract

The utility model discloses a kind of drug synthetic reaction kettle devices, the upper surface of pedestal is equipped with reaction chamber, the interior lower end of reaction chamber is equipped with stock guide, the middle part of stock guide is equipped with discharge port, and solenoid valve one is equipped in discharge port, the top middle portion of reaction chamber is equipped with driving motor, and agitating shaft is connected on driving motor, multiple paddles are connected on agitating shaft, side top inside reaction chamber is connected with the casing for stretching to reaction chamber bottom, the side wall of casing is equipped with multiple liquid outlets, and the bottom end of casing is equipped with through-hole, the top of reaction chamber is equipped with air pump, and the tracheae reached in casing is connected on air pump, it is arranged on the side wall of tracheae, there is the multiple and one-to-one gas outlet of liquid outlet, the two sides of air pump are equipped with reagent box, reagent box is connected to by perfusion tube with casing, and solenoid valve two is equipped in perfusion tube, outside reaction chamber Side wall is equipped with power supply and controller.Device practicability in the utility model is extremely strong, is very suitable to promotion and application on the market.

Description

一种药物合成反应釜装置A drug synthesis reactor device

技术领域technical field

本实用新型涉及医药制造技术领域,具体涉及一种药物合成反应釜装置。The utility model relates to the technical field of medicine manufacturing, in particular to a medicine synthesis reactor device.

背景技术Background technique

反应釜的广义理解为物理或化学反应的容器,通过对容器的结构设计与参数配置,实现工艺要求的加热、蒸发、冷却及低高速的混配功能,反应釜广泛应用于石油、化工、橡胶、农药、染料、医药、食品等行业。The broad understanding of the reaction kettle is a container for physical or chemical reactions. Through the structural design and parameter configuration of the container, the heating, evaporation, cooling and low-speed mixing functions required by the process are realized. The reaction kettle is widely used in petroleum, chemical, rubber and other industries. , pesticides, dyes, medicine, food and other industries.

现有的反应釜不能将液体试剂均匀的喷在反应釜内,从而导致各个试剂混合不均匀,从而使生产出来的药物达不到要求。The existing reaction kettle cannot evenly spray liquid reagents in the reaction kettle, resulting in uneven mixing of various reagents, so that the produced medicine cannot meet the requirements.

实用新型内容Utility model content

(一)要解决的技术问题(1) Technical problems to be solved

为了克服现有技术不足,现提出一种药物合成反应釜装置,本实用新型通过在反应室内设置套管和气管,且套管上设置多个出液口,气管上设置有多个出气口,这样可以将流入套管内部的液体试剂喷在反应室的不同深度,这样可以使各个试剂混合的比较均匀,因此本实用新型中的反应釜实用性较强。In order to overcome the deficiencies in the prior art, a drug synthesis reactor device is now proposed. The utility model is provided with a casing and a gas pipe in the reaction chamber, and a plurality of liquid outlets are arranged on the casing, and a plurality of gas outlets are arranged on the gas pipe. In this way, the liquid reagents flowing into the casing can be sprayed at different depths of the reaction chamber, so that the reagents can be mixed evenly, so the reaction kettle in the utility model has strong practicability.

(二)技术方案(2) Technical solutions

本实用新型通过如下技术方案实现:本实用新型提出了一种药物合成反应釜装置,包括底座,所述底座的上端面固定设置有反应箱,所述反应箱的内部下端安装有漏斗状的导料板,所述导料板以上为反应室,所述导料板以下为存储室,所述导料板的中部设置有出料口,且所述出料口内设置有电磁阀一,所述反应箱的顶端中部设置有驱动电机,且所述驱动电机上固接有伸到反应室底部的搅拌轴,所述搅拌轴上由上至下固接有多个搅拌叶,所述反应室内部的一侧顶端固接有伸向反应室底部的套管,所述套管的侧壁上由上至下设置有多个出液口,且所述套管的底端设置有通孔,所述反应箱的顶部设置有气泵,且所述气泵上连接有伸到套管内的气管,所述气管的侧壁上设置有多个与所述出液口一一对应的出气口,所述气泵的两侧均设置有装有液体试剂的试剂箱,所述试剂箱通过一输液管与所述套管连通,且所述输液管内设置有电磁阀二,所述反应箱的顶部还设置有装有固体试剂的储料罐,所述储料罐上连通有伸到反应室内的支管,且所述支管内设置有电磁阀三,所述反应室内设置有电加热丝,所述反应箱的外侧壁上还设置有电源以及与所述电源电性相连的控制器,所述控制器分别与所述电磁阀一、驱动电机、气泵、电磁阀二、电磁阀三以及电加热丝电性相连。The utility model is realized through the following technical solutions: the utility model proposes a drug synthesis reaction kettle device, including a base, a reaction box is fixedly arranged on the upper end surface of the base, and a funnel-shaped guide is installed at the inner lower end of the reaction box. A material plate, above the material guide plate is a reaction chamber, below the material guide plate is a storage room, the middle part of the material guide plate is provided with a discharge port, and the discharge port is provided with a solenoid valve one, the The middle part of the top of the reaction box is provided with a drive motor, and the drive motor is fixedly connected with a stirring shaft extending to the bottom of the reaction chamber, and the stirring shaft is fixedly connected with a plurality of stirring blades from top to bottom. A casing extending toward the bottom of the reaction chamber is fixedly connected to the top of one side of the casing, and a plurality of liquid outlets are arranged on the side wall of the casing from top to bottom, and a through hole is arranged at the bottom of the casing, so The top of the reaction box is provided with an air pump, and the air pump is connected with a gas pipe extending into the casing, and the side wall of the gas pipe is provided with a plurality of gas outlets corresponding to the liquid outlets one by one. Both sides of the reaction box are provided with reagent boxes containing liquid reagents, the reagent box communicates with the casing through an infusion tube, and a solenoid valve 2 is arranged in the infusion tube, and a device for installing There is a storage tank for solid reagents, the storage tank is connected with a branch pipe extending into the reaction chamber, and a solenoid valve 3 is arranged in the branch pipe, an electric heating wire is arranged in the reaction chamber, and the outside of the reaction box A power supply and a controller electrically connected to the power supply are also arranged on the wall, and the controller is electrically connected to the first solenoid valve, the driving motor, the air pump, the second solenoid valve, the third solenoid valve and the electric heating wire.

进一步的,所述底座底部的四个拐角处均设置有万向滚轮,且所述万向滚轮中带有自锁装置。Further, universal rollers are provided at the four corners of the bottom of the base, and self-locking devices are provided in the universal rollers.

进一步的,所述驱动电机为伺服电机。Further, the drive motor is a servo motor.

进一步的,所述反应室的内侧顶部还设置有与所述控制器电性相连的温度传感器。Further, a temperature sensor electrically connected to the controller is also provided on the inner top of the reaction chamber.

进一步的,所述反应箱的下端设置有与所述存储室相配的抽屉。Further, the lower end of the reaction box is provided with a drawer matched with the storage chamber.

进一步的,所述抽屉上安装有把手。Further, a handle is installed on the drawer.

进一步的,所述控制器为PLC控制器。Further, the controller is a PLC controller.

(三)有益效果(3) Beneficial effects

本实用新型相对于现有技术,具有以下有益效果:本实用新型在反应室内设置套管和气管,且套管上设置多个出液口,气管上设置有多个出气口,可以将流入套管内部的液体试剂喷在反应室的不同深度,这样可以使各个试剂混合的比较均匀,同时各个试剂在搅拌叶的搅拌下,混合的更加均匀;同时,本实用新型还在反应室内设置电加热丝和温度传感器,这样可以准确的控制反应室内的温度,因此本实用新型中的反应釜实用性较强,适合在市场上推广和应用。Compared with the prior art, the utility model has the following beneficial effects: the utility model is provided with a casing and a gas pipe in the reaction chamber, and the casing is provided with a plurality of liquid outlets, and the gas pipe is provided with a plurality of gas outlets, which can flow into the sleeve The liquid reagents inside the tube are sprayed at different depths in the reaction chamber, so that each reagent can be mixed evenly, and at the same time, each reagent can be mixed more evenly under the stirring of the stirring blade; at the same time, the utility model is also provided with electric heating in the reaction chamber. wire and a temperature sensor, so that the temperature in the reaction chamber can be accurately controlled, so the reaction kettle in the utility model has strong practicability and is suitable for popularization and application in the market.

附图说明Description of drawings

图1为本实用新型中的整体结构示意图;Fig. 1 is the overall structure schematic diagram in the utility model;

图2为本实用新型中的内部结构示意图;Fig. 2 is the internal structure schematic diagram in the utility model;

图3为本实用新型中的结构框图。Fig. 3 is a structural block diagram in the utility model.

图中:1底座、2反应箱、3导料板、4反应室、5存储室、6出料口、7电磁阀一、8驱动电机、9搅拌轴、10搅拌叶、11套管、12 出液口、13通孔、14气泵、15气管、16出气口、17试剂箱、18输液管、19电磁阀二、20储料罐、21支管、22电磁阀三、23电加热丝、24控制器、25万向滚轮、26温度传感器、27抽屉、28把手。In the figure: 1 base, 2 reaction box, 3 material guide plate, 4 reaction chamber, 5 storage chamber, 6 discharge port, 7 solenoid valve 1, 8 drive motor, 9 stirring shaft, 10 stirring blade, 11 casing, 12 Liquid outlet, 13 through hole, 14 air pump, 15 air pipe, 16 air outlet, 17 reagent box, 18 infusion tube, 19 solenoid valve two, 20 storage tank, 21 branch pipe, 22 solenoid valve three, 23 electric heating wire, 24 Controller, 25 universal rollers, 26 temperature sensors, 27 drawers, 28 handles.

具体实施方式Detailed ways

为了使本实用新型的目的、技术方案及优点更加清楚明白,以下结合附图及实施例,对本实用新型进行进一步详细说明。应当理解,此处所描述的具体实施例仅仅用以解释本实用新型,并不用于限定本实用新型。In order to make the purpose, technical solution and advantages of the utility model clearer, the utility model will be further described in detail below in conjunction with the accompanying drawings and embodiments. It should be understood that the specific embodiments described here are only used to explain the utility model, and are not intended to limit the utility model.

如图1-3,一种药物合成反应釜装置,包括底座1,所述底座1 的上端面固定设置有反应箱2,所述反应箱2的内部下端安装有漏斗状的导料板3,所述导料板3以上为反应室4,所述导料板3以下为存储室5,所述导料板3的中部设置有出料口6,且所述出料口6内设置有电磁阀一7,所述反应箱2的顶端中部设置有驱动电机8,且所述驱动电机8上固接有伸到反应室4底部的搅拌轴9,所述搅拌轴 9上由上至下固接有多个搅拌叶10,所述反应室4内部的一侧顶端固接有伸向反应室4底部的套管11,所述套管11的侧壁上由上至下设置有多个出液口12,且所述套管11的底端设置有通孔13,所述反应箱2的顶部设置有气泵14,且所述气泵14上连接有伸到套管11内的气管15,所述气管15的侧壁上设置有多个与所述出液口12一一对应的出气口16,所述气泵14的两侧均设置有装有液体试剂的试剂箱17,所述试剂箱17通过一输液管18与所述套管11连通,且所述输液管18内设置有电磁阀二19,所述反应箱2的顶部还设置有装有固体试剂的储料罐20,所述储料罐20上连通有伸到反应室4内的支管21,且所述支管21内设置有电磁阀三22,所述反应室4内设置有电加热丝23,所述反应箱2的外侧壁上还设置有电源以及与所述电源电性相连的控制器24,所述控制器24分别与所述电磁阀一7、驱动电机8、气泵14、电磁阀二19、电磁阀三22以及电加热丝23电性相连。As shown in Fig. 1-3, a drug synthesis reactor device includes a base 1, the upper end surface of the base 1 is fixed with a reaction box 2, and the inner lower end of the reaction box 2 is equipped with a funnel-shaped material guide plate 3, Above the material guide plate 3 is a reaction chamber 4, below the material guide plate 3 is a storage chamber 5, the middle part of the material guide plate 3 is provided with a discharge port 6, and an electromagnetic Valve one 7, the top middle part of the reaction box 2 is provided with a drive motor 8, and the drive motor 8 is fixedly connected with a stirring shaft 9 extending to the bottom of the reaction chamber 4, and the stirring shaft 9 is fixed from top to bottom. A plurality of stirring blades 10 are connected, and a sleeve 11 extending toward the bottom of the reaction chamber 4 is fixedly attached to the top of one side of the reaction chamber 4, and a plurality of outlets are arranged on the side wall of the sleeve 11 from top to bottom. liquid port 12, and the bottom end of the sleeve pipe 11 is provided with a through hole 13, the top of the reaction box 2 is provided with an air pump 14, and the air pump 14 is connected with a gas pipe 15 extending into the sleeve pipe 11, so The side wall of the gas pipe 15 is provided with a plurality of gas outlets 16 corresponding to the liquid outlets 12 one by one, and both sides of the air pump 14 are provided with a reagent box 17 containing a liquid reagent. It is communicated with the sleeve pipe 11 through a transfusion tube 18, and an electromagnetic valve 19 is arranged in the transfusion tube 18, and the top of the reaction box 2 is also provided with a storage tank 20 equipped with a solid reagent. The material tank 20 is communicated with a branch pipe 21 extending into the reaction chamber 4, and the branch pipe 21 is provided with a solenoid valve 3 22, the reaction chamber 4 is provided with an electric heating wire 23, and the outer wall of the reaction box 2 Also provided with a power supply and a controller 24 electrically connected to the power supply, the controller 24 is connected to the solenoid valve one 7, the driving motor 8, the air pump 14, the solenoid valve two 19, the solenoid valve three 22 and the electric valve respectively. The heating wire 23 is electrically connected.

进一步的,所述底座1底部的四个拐角处均设置有万向滚轮25,且所述万向滚轮25中带有自锁装置;便于移动整个反应釜装置。Further, the four corners of the bottom of the base 1 are provided with universal rollers 25, and the universal rollers 25 are equipped with self-locking devices; it is convenient to move the entire reactor device.

进一步的,所述驱动电机8为伺服电机;可以准确地控制电动机的转速。Further, the drive motor 8 is a servo motor; the rotation speed of the motor can be accurately controlled.

进一步的,所述反应室4的内侧顶部还设置有与所述控制器24 电性相连的温度传感器26;可以测量出反应釜内部的温度。Further, the inner top of the reaction chamber 4 is also provided with a temperature sensor 26 electrically connected to the controller 24; the temperature inside the reaction kettle can be measured.

进一步的,所述反应箱2的下端设置有与所述存储室5相配的抽屉27;便于取出反应后的药物。Further, the lower end of the reaction box 2 is provided with a drawer 27 matched with the storage chamber 5; it is convenient to take out the reacted medicine.

进一步的,所述抽屉27上安装有把手28;便于打开抽屉27。进一步的,所述控制器24为PLC控制器。Further, a handle 28 is installed on the drawer 27 ; it is convenient to open the drawer 27 . Further, the controller 24 is a PLC controller.

工作原理:使用时,首先将固体试剂放在储料罐20内,将液体试剂放在试剂箱17内,可以通过控制器24打开电磁阀二19和电磁阀三22,这样液体试剂就会流入套管11内,此时,通过控制器24 启动气泵14,气管15喷出来的气体可以将套管11内的液体试剂通过出液口12冲到反应室4内,这样液体试剂就就均匀的喷在反应室 4的不同深度,从而使得各个原料混合的比较均匀;同时,本实用新型还在反应室4内设置电加热丝23和温度传感器26,这样可以准确的控制反应室4内的温度,从而制造出达标的药物,因此本实用新型中的反应釜实用性极强,非常适合在市场上推广和应用。Working principle: when in use, first put the solid reagent in the storage tank 20, put the liquid reagent in the reagent box 17, and open the solenoid valve 2 19 and solenoid valve 3 22 through the controller 24, so that the liquid reagent will flow into the In the sleeve pipe 11, at this time, the air pump 14 is started by the controller 24, and the gas ejected from the air pipe 15 can rush the liquid reagent in the sleeve pipe 11 into the reaction chamber 4 through the liquid outlet 12, so that the liquid reagent is just uniform Spray at different depths of the reaction chamber 4, so that the mixing of each raw material is relatively uniform; at the same time, the utility model also sets an electric heating wire 23 and a temperature sensor 26 in the reaction chamber 4, so that the temperature in the reaction chamber 4 can be accurately controlled , so as to produce up-to-standard medicines, so the reactor in the utility model has strong practicability and is very suitable for popularization and application in the market.

以上所述,仅为本实用新型较佳的具体实施方式,但本实用新型的保护范围并不局限于此,任何熟悉本技术领域的技术人员在本实用新型揭露的技术范围内,根据本实用新型的技术方案及其实用新型构思加以等同替换或改变,都应涵盖在本实用新型的保护范围之内。The above is only a preferred embodiment of the utility model, but the scope of protection of the utility model is not limited thereto. The equivalent replacement or change of the new technical solution and the concept of the utility model shall be covered by the protection scope of the utility model.

Claims (7)

1.一种药物合成反应釜装置,其特征在于,包括底座(1),所述底座(1)的上端面固定设置有反应箱(2),所述反应箱(2)的内部下端安装有漏斗状的导料板(3),所述导料板(3)以上为反应室(4),所述导料板(3)以下为存储室(5),所述导料板(3)的中部设置有出料口(6),且所述出料口(6)内设置有电磁阀一(7),所述反应箱(2)的顶端中部设置有驱动电机(8),且所述驱动电机(8)上固接有伸到反应室(4)底部的搅拌轴(9),所述搅拌轴(9)上由上至下固接有多个搅拌叶(10),所述反应室(4)内部的一侧顶端固接有伸向反应室(4)底部的套管(11),所述套管(11)的侧壁上由上至下设置有多个出液口(12),且所述套管(11)的底端设置有通孔(13),所述反应箱(2)的顶部设置有气泵(14),且所述气泵(14)上连接有伸到套管(11)内的气管(15),所述气管(15)的侧壁上设置有多个与所述出液口(12)一一对应的出气口(16),所述气泵(14)的两侧均设置有装有液体试剂的试剂箱(17),所述试剂箱(17)通过一输液管(18)与所述套管(11)连通,且所述输液管(18)内设置有电磁阀二(19),所述反应箱(2)的顶部还设置有装有固体试剂的储料罐(20),所述储料罐(20)上连通有伸到反应室(4)内的支管(21),且所述支管(21)内设置有电磁阀三(22),所述反应室(4)内设置有电加热丝(23),所述反应箱(2)的外侧壁上还设置有电源以及与所述电源电性相连的控制器(24),所述控制器(24)分别与所述电磁阀一(7)、驱动电机(8)、气泵(14)、电磁阀二(19)、电磁阀三(22)以及电加热丝(23)电性相连。1. A drug synthesis reactor device, characterized in that it comprises a base (1), the upper end surface of the base (1) is fixedly provided with a reaction box (2), and the inner lower end of the reaction box (2) is equipped with A funnel-shaped material guide plate (3), above the described material guide plate (3) is a reaction chamber (4), below the described material guide plate (3) is a storage chamber (5), the described material guide plate (3) The middle part of the reaction box (2) is provided with a discharge port (6), and a solenoid valve one (7) is provided in the discharge port (6), and a drive motor (8) is provided at the top middle part of the reaction box (2), and the The drive motor (8) is fixedly connected with a stirring shaft (9) extending to the bottom of the reaction chamber (4), and the stirring shaft (9) is fixedly connected with a plurality of stirring blades (10) from top to bottom. A sleeve (11) extending toward the bottom of the reaction chamber (4) is fixedly attached to the top of one side of the reaction chamber (4), and a plurality of liquid outlets are arranged on the side wall of the sleeve (11) from top to bottom. (12), and the bottom end of the casing (11) is provided with a through hole (13), the top of the reaction box (2) is provided with an air pump (14), and the air pump (14) is connected with an extension To the air pipe (15) in the casing (11), the side wall of the air pipe (15) is provided with a plurality of air outlets (16) corresponding to the liquid outlets (12), and the air pump ( Both sides of 14) are provided with a reagent case (17) that liquid reagent is housed, and the reagent case (17) communicates with the sleeve pipe (11) through a transfusion tube (18), and the transfusion tube (18) ) is provided with electromagnetic valve two (19), and the top of the reaction box (2) is also provided with a storage tank (20) equipped with solid reagents, and the storage tank (20) is connected with a Branch pipe (21) in (4), and electromagnetic valve three (22) is arranged in described branch pipe (21), electric heating wire (23) is provided with in described reaction chamber (4), described reaction box (2 ) is also provided with a power supply and a controller (24) electrically connected to the power supply on the outer wall, and the controller (24) is respectively connected to the electromagnetic valve one (7), the driving motor (8), the air pump ( 14), solenoid valve two (19), solenoid valve three (22) and electric heating wire (23) are electrically connected. 2.根据权利要求1所述的一种药物合成反应釜装置,其特征在于,所述底座(1)底部的四个拐角处均设置有万向滚轮(25),且所述万向滚轮(25)中带有自锁装置。2. A kind of drug synthesis reactor device according to claim 1, characterized in that, four corners of the bottom of the base (1) are provided with universal rollers (25), and the universal rollers ( 25) with self-locking device. 3.根据权利要求1所述的一种药物合成反应釜装置,其特征在于,所述驱动电机(8)为伺服电机。3. A drug synthesis reactor device according to claim 1, characterized in that the drive motor (8) is a servo motor. 4.根据权利要求1所述的一种药物合成反应釜装置,其特征在于,所述反应室(4)的内侧顶部还设置有与所述控制器(24)电性相连的温度传感器(26)。4. A kind of drug synthesis reactor device according to claim 1, characterized in that, the inner top of the reaction chamber (4) is also provided with a temperature sensor (26) electrically connected to the controller (24). ). 5.根据权利要求1所述的一种药物合成反应釜装置,其特征在于,所述反应箱(2)的下端设置有与所述存储室(5)相配的抽屉(27)。5. A drug synthesis reactor device according to claim 1, characterized in that a drawer (27) matching the storage chamber (5) is provided at the lower end of the reaction box (2). 6.根据权利要求5所述的一种药物合成反应釜装置,其特征在于,所述抽屉(27)上安装有把手(28)。6. A medicine synthesis reactor device according to claim 5, characterized in that, a handle (28) is installed on the drawer (27). 7.根据权利要求1所述的一种药物合成反应釜装置,其特征在于,所述控制器(24)为PLC控制器。7. A kind of drug synthesis reactor device according to claim 1, characterized in that, the controller (24) is a PLC controller.
CN201822133458.0U 2018-12-19 2018-12-19 A kind of drug synthetic reaction kettle device Active CN209576659U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112774604A (en) * 2020-12-16 2021-05-11 九江绿为沃特环保科技有限公司 Reaction unit for producing and processing synthetic materials

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112774604A (en) * 2020-12-16 2021-05-11 九江绿为沃特环保科技有限公司 Reaction unit for producing and processing synthetic materials

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