CN217127445U - Device for extracting perilla polysaccharide - Google Patents
Device for extracting perilla polysaccharide Download PDFInfo
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- CN217127445U CN217127445U CN202220771283.XU CN202220771283U CN217127445U CN 217127445 U CN217127445 U CN 217127445U CN 202220771283 U CN202220771283 U CN 202220771283U CN 217127445 U CN217127445 U CN 217127445U
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Abstract
The utility model discloses a device for extracting perilla polysaccharide, which relates to the technical field of polysaccharide extraction, and comprises a raw material crushing box, a drying box, a degreasing box, an ultrasonic crushing box and a dialysis bag, wherein the raw material crushing box is used for crushing perilla seeds, the raw material crushing box is connected with the drying box, the drying box is used for drying crushed perilla seed powder, the drying box is connected with the degreasing box, the degreasing box is connected with the ultrasonic crushing box through a mud pump, a water system precipitate obtained by standing after degreasing operation in the degreasing box is pumped to the ultrasonic crushing box through the mud pump, and the ultrasonic crushing box is connected with the dialysis bag through a solution pump; the utility model discloses can accomplish the systematic extraction of perilla polysaccharide in the perilla seed, device simple structure, the enzyme process combines the ultrasonic wave breakage, can improve perilla polysaccharide's extraction rate greatly.
Description
Technical Field
The utility model relates to a polysaccharide draws technical field, especially relates to a draw device of purple perilla polysaccharide.
Background
The perilla is a common Chinese herbal medicine and an important economic crop, and flowers, leaves, stems and fruit materials of the perilla have high development and utilization values. Perilla seed is dry mature particle of perilla, rich in grease, oil yield is 36-50%, higher than cottonseed, rapeseed and castor seed, etc., perilla oil is rich in alpha-linolenic acid, and is a good health oil, so far, perilla seed is mostly used for extracting grease in domestic and foreign fields, and other researches are few. The added value of the perilla can be greatly improved by extracting the polysaccharide from the perilla seeds, the research report about the perilla polysaccharide is more rarely reported, and only Liu Da Chuan and the like adopt hot water to extract the polysaccharide from the perilla cake.
Therefore, it is an urgent problem to provide a device for extracting perilla polysaccharide.
SUMMERY OF THE UTILITY MODEL
The utility model aims at providing an extract perillaseed polysaccharide's device to solve the problem that above-mentioned prior art exists, can accomplish the systematization of perillaseed polysaccharide in the perillaseed and draw, device simple structure, the extraction rate is high.
In order to achieve the above object, the utility model provides a following scheme:
the utility model provides an extract perillapolysaccharide's device, smash case, stoving case, degreasing box, the broken case of ultrasonic wave and dialysis bag including the raw materials, the raw materials is smashed the case and is used for smashing the perilla seed, the raw materials is smashed the case and is connected the stoving case, the stoving case is used for the stoving of the perilla seed powder after smashing, the stoving case is connected the degreasing box, the degreasing box is connected through the dredge pump the broken case of ultrasonic wave, the aqueous system precipitate that stews after the degreasing operation in the degreasing box and obtain by the dredge pump extremely the broken case of ultrasonic wave, the broken case of ultrasonic wave passes through the solution pump and connects the dialysis bag.
Preferably, the top of the raw material crushing box is provided with a feeding port.
Preferably, the bottom of the raw material crushing box is provided with a funnel-shaped first discharging channel, the raw material crushing box is connected with a feeding port at the top of the drying box through the first discharging channel, and a first discharging valve is arranged on the first discharging channel.
Preferably, the raw material crushing box is internally provided with a crushing rod driven by a motor, and the crushing rod is provided with a crushing blade.
Preferably, the bottom of stoving case is provided with hopper-shaped unloading passageway two, the stoving case passes through unloading passageway two is connected the pan feeding mouth at degrease roof portion, be provided with the unloading valve on the unloading passageway two.
Preferably, the bottom of the degreasing tank is connected with the ultrasonic crushing tank through a pipeline, and the sludge pump is arranged on the pipeline.
Preferably, the bottom of the degreasing box is also provided with a liquid outlet.
Preferably, the ultrasonic crushing box is connected with the dialysis bag through a pipeline, and the solution pump is arranged on the pipeline.
The utility model discloses following beneficial technological effect has been gained for prior art:
the utility model provides an extract perillapolyose's device can accomplish the systematic extraction of perillapolyose in the perilla seed, device simple structure, and the enzyme process combines the ultrasonic wave breakage, can improve perillapolyose's extraction rate greatly.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings required to be used in the embodiments will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to these drawings without creative efforts.
FIG. 1 is a schematic structural view of the apparatus for extracting perilla polysaccharide of the present invention;
in the figure: 1-raw material crushing box, 2-drying box, 3-degreasing box, 4-ultrasonic crushing box, 5-dialysis bag, 6-feeding port, 7-feeding channel I, 8-motor, 9-crushing rod, 10-crushing blade, 11-feeding channel II, 12-mud pump, 13-liquid discharge port and 14-solution pump.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
The utility model aims at providing an extract perilla polysaccharide's device to solve the problem that prior art exists.
In order to make the above objects, features and advantages of the present invention more comprehensible, the present invention is described in detail with reference to the accompanying drawings and the detailed description.
The device of drawing perillapolysaccharide in this embodiment, as shown in fig. 1, including raw materials crushing case 1, stoving case 2, degreasing box 3, ultrasonic wave broken case 4 and dialysis bag 5, raw materials crushing case 1 is used for smashing the perilla seed, raw materials crushing case 1 connects stoving case 2, stoving case 2 is used for the stoving of the perilla seed powder after smashing, degreasing box 3 is connected to stoving case 2, degreasing box 3 passes through dredge pump 12 and connects ultrasonic wave broken case 4, the aqueous system precipitate that the interior degreasing operation of degreasing box 3 was later stood and is obtained is taken out to ultrasonic wave broken case 4 by dredge pump 12, ultrasonic wave broken case 4 passes through solution pump 14 and connects dialysis bag 5.
In the embodiment, the top of the raw material crushing box 1 is provided with a feeding port 6; the bottom of the raw material crushing box 1 is provided with a funnel-shaped blanking channel I7, the raw material crushing box 1 is connected with a feeding port 6 at the top of the drying box 2 through the blanking channel I7, and a blanking valve is arranged on the blanking channel I7. The raw material crushing box 1 is internally provided with a crushing rod 9 driven by a motor 8, and the crushing rod 9 is provided with a crushing blade 10.
In this embodiment, the bottom of the drying box 2 is provided with a funnel-shaped discharging channel two 11, the drying box 2 is connected with the feeding port 6 at the top of the degreasing box 3 through the discharging channel two 11, and the discharging channel two 11 is provided with a discharging valve.
In this embodiment, the bottom of the degreasing tank 3 is connected to the ultrasonic crushing tank 4 through a pipeline, and the sludge pump 12 is disposed on the pipeline.
In this embodiment, a liquid outlet 13 is further disposed at the bottom of the degreasing tank 3.
In this embodiment, the ultrasonication tank 4 is connected to the dialysis bag 5 through a pipe, and the solution pump 14 is disposed on the pipe.
The utility model provides an extract perillapolysaccharide's device carries out the step that perillapolysaccharide drawed as follows:
firstly, crushing perilla seeds in a raw material crushing box 1, and opening a blanking valve to enable perilla seed powder to enter a drying box 2 for drying;
secondly, putting the dried perilla seed powder into a degreasing box 3, adding degreasing liquid with the volume being 3 times that of the powder, standing for 4 hours, and separating an organic phase from a water system precipitate;
thirdly, pumping the water system sediment into the ultrasonic crushing box 4 by a mud pump 12, discharging an organic phase from a liquid outlet 13, adding 25 times of distilled water by volume into the water system sediment in the ultrasonic crushing box 4, firstly performing ultrasonic crushing, and then adding papain for auxiliary extraction to obtain a crude polysaccharide solution;
removing free foreign protein in the crude polysaccharide solution by adopting a sevag method, adding ammonia water, adjusting the pH value to 8-9, dropwise adding hydrogen peroxide with the mass concentration of 15%, and decoloring for 2d at normal temperature;
fifthly, opening a solution pump 14 to pump the decolorized solution in the fourth step into a dialysis bag 5, dialyzing with distilled water for 48 hours, and repeatedly dialyzing for 2 times to obtain a perilla polysaccharide extracting solution;
sixthly, performing fractional purification on the perilla polysaccharide extracting solution by adopting a DEAE column chromatography, namely completing the extraction and purification of the perilla polysaccharide from the perilla seeds.
The utility model discloses the principle and the implementation mode of the utility model are explained by applying the concrete examples, and the explanation of the above examples is only used for helping to understand the method and the core idea of the utility model; meanwhile, for the general technical personnel in the field, according to the idea of the present invention, there are changes in the concrete implementation and the application scope. In summary, the content of the present description should not be construed as a limitation of the present invention.
Claims (8)
1. The utility model provides an extract perilla polysaccharide's device which characterized in that: including raw materials crushing case, stoving case, degreasing box, the broken case of ultrasonic wave and dialysis bag, the raw materials crushing case is used for smashing the perilla seed, the raw materials crushing case is connected the stoving case, the stoving case is used for the stoving of the perilla seed powder after smashing, the stoving case is connected the degreasing box, the degreasing box is connected through the mud pump the broken case of ultrasonic wave, the system precipitate that obtains of stewing behind the degreasing operation in the degreasing box is by the mud pump is pumped extremely the broken case of ultrasonic wave, the broken case of ultrasonic wave passes through the solution pump and connects the dialysis bag.
2. The apparatus for extracting perilla polysaccharide according to claim 1, wherein: the top of the raw material crushing box is provided with a feeding port.
3. The apparatus for extracting perilla polysaccharide according to claim 1, wherein: the bottom of the raw material crushing box is provided with a funnel-shaped first discharging channel, the raw material crushing box is connected with a feeding port at the top of the drying box through the first discharging channel, and a first discharging valve is arranged on the first discharging channel.
4. The apparatus for extracting perilla polysaccharide according to claim 1, wherein: the inside crushing pole that is provided with by the motor drive of raw materials crushing incasement portion, be provided with crushing blade on the crushing pole.
5. The apparatus for extracting perilla polysaccharide according to claim 1, wherein: the bottom of stoving case is provided with hopper-shaped unloading passageway two, the stoving case passes through unloading passageway two is connected the pan feeding mouth at degrease roof portion, be provided with the unloading valve on the unloading passageway two.
6. The apparatus for extracting perilla polysaccharide according to claim 1, wherein: the bottom of the degreasing tank is connected with the ultrasonic crushing tank through a pipeline, and the mud pump is arranged on the pipeline.
7. The apparatus for extracting perilla polysaccharide according to claim 1, wherein: and a liquid outlet is also formed in the bottom of the degreasing box.
8. The apparatus for extracting perilla polysaccharide according to claim 1, wherein: the ultrasonic crushing box is connected with the dialysis bag through a pipeline, and the solution pump is arranged on the pipeline.
Priority Applications (1)
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CN202220771283.XU CN217127445U (en) | 2022-04-02 | 2022-04-02 | Device for extracting perilla polysaccharide |
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CN202220771283.XU CN217127445U (en) | 2022-04-02 | 2022-04-02 | Device for extracting perilla polysaccharide |
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