CN216366719U - Extraction element of little large-leaved gentian pharmacodynamic ingredient - Google Patents
Extraction element of little large-leaved gentian pharmacodynamic ingredient Download PDFInfo
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- CN216366719U CN216366719U CN202123119381.XU CN202123119381U CN216366719U CN 216366719 U CN216366719 U CN 216366719U CN 202123119381 U CN202123119381 U CN 202123119381U CN 216366719 U CN216366719 U CN 216366719U
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- tank
- extraction
- pipe
- gentiana
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- 238000000605 extraction Methods 0.000 title claims abstract description 52
- 230000003285 pharmacodynamic effect Effects 0.000 title claims abstract description 7
- 239000004615 ingredient Substances 0.000 title claims description 4
- 241001071795 Gentiana Species 0.000 title description 5
- 239000002904 solvent Substances 0.000 claims abstract description 32
- 241000501743 Gentiana macrophylla Species 0.000 claims abstract description 24
- 239000000463 material Substances 0.000 claims abstract description 23
- 238000010438 heat treatment Methods 0.000 claims abstract description 19
- 239000007788 liquid Substances 0.000 claims abstract description 14
- 238000011084 recovery Methods 0.000 claims abstract description 10
- 239000000523 sample Substances 0.000 claims abstract description 7
- 241000501719 Gentiana straminea Species 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 230000000857 drug effect Effects 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 5
- 238000007599 discharging Methods 0.000 abstract description 2
- 239000007921 spray Substances 0.000 description 7
- 239000004480 active ingredient Substances 0.000 description 5
- 239000003814 drug Substances 0.000 description 5
- 238000000034 method Methods 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 206010011224 Cough Diseases 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 230000003110 anti-inflammatory effect Effects 0.000 description 2
- 239000000498 cooling water Substances 0.000 description 2
- 230000002349 favourable effect Effects 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 208000000655 Distemper Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241001071804 Gentianaceae Species 0.000 description 1
- DUAGQYUORDTXOR-GPQRQXLASA-N Gentiopicrin Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@H]1[C@H](C=C)C2=CCOC(=O)C2=CO1 DUAGQYUORDTXOR-GPQRQXLASA-N 0.000 description 1
- DUAGQYUORDTXOR-WULZUDSJSA-N Gentiopicrin Natural products O([C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1)[C@H]1[C@@H](C=C)C=2C(C(=O)OCC=2)=CO1 DUAGQYUORDTXOR-WULZUDSJSA-N 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 206010068319 Oropharyngeal pain Diseases 0.000 description 1
- 201000007100 Pharyngitis Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000567 combustion gas Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000008236 heating water Substances 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
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Abstract
The utility model discloses an extraction device for medicinal components of gentiana macrophylla, which comprises an extraction tank and a concentration tank, wherein the upper part of the extraction tank is provided with a feed hopper and a liquid inlet pipe, the interior of the extraction tank is provided with an electric stirrer and a temperature control probe, the lower part of the extraction tank is provided with a discharge hole, and the discharge hole is provided with a filter; the outer wall of the extraction tank is provided with a mounting groove and a heating jacket, and an ultrasonic generator is arranged in the mounting groove; a material receiving port and a solvent outlet pipe are arranged at the upper part of the concentration tank, a heating jacket is arranged on the outer wall of the concentration tank, and a material discharging port is arranged at the bottom of the concentration tank; the material receiving port is connected with the filter, a condenser is arranged on the solvent outlet pipe, and the solvent outlet pipe is connected with a solvent recovery tank; this extraction element can effectively promote the extraction effect of little gentiana macrophylla pharmacodynamic component.
Description
Technical Field
The utility model relates to an extraction device for active ingredients of gentiana macrophylla pall, and belongs to the technical field of extraction devices.
Background
Gentiana macrophylla, a Mongolian medicine named as Huhe Zhuli root-its Juge, is a Dawuli gentian of Gentiana of Gentianaceae, widely distributed in inner Mongolia, Shaanxi, Gansu, Xinjiang and other places, and mostly grown in the fields of field, roadside, riverbank, ditch side, sunny mountain slope and the like, and is one of the commonly used medicinal materials of Mongolian medicine. The Gentiana microphylla, Gentiana macrophylla pall and Gentiana straminea Maxim are used as basic plants of Gentiana macrophylla in 2020 edition of Chinese pharmacopoeia.
Small gentiana macrophylla is recorded in the drug Standard of Ministry of health of the people's republic of China (Mongolian medicine booklet), is a Mongolian medicine commonly used in clinical practice, has the effects of clearing heat, detoxifying, relieving cough and eliminating phlegm, and is mainly used for treating cough due to lung heat, throat heat, sore throat, toxic heat, distemper and other symptoms. Iridoid compounds represented by gentiopicroside have certain anti-inflammatory effect, and can be regarded as main anti-inflammatory active ingredients of gentiana macrophylla medicinal materials.
However, the related research of the existing device for extracting the effective components of gentiana macrophylla pall is less, and the problems of inconvenient extraction and poor extraction effect exist.
SUMMERY OF THE UTILITY MODEL
The utility model overcomes the defects in the prior art, and aims to provide the device for extracting the active ingredients of the Gentiana macrophylla pall, which can effectively improve the extraction effect of the active ingredients of the Gentiana macrophylla pall.
In order to solve the technical problems, the technical scheme adopted by the utility model is as follows:
an extraction device for effective components of Gentiana macrophylla comprises an extraction tank and a concentration tank, wherein the upper part of the extraction tank is provided with a feed hopper and a liquid inlet pipe, the interior of the extraction tank is provided with an electric stirrer and a temperature control probe, the lower part of the extraction tank is provided with a discharge hole, and the discharge hole is provided with a filter; the outer wall of the extraction tank is provided with a mounting groove and a heating jacket, and an ultrasonic generator is arranged in the mounting groove; a material receiving port and a solvent outlet pipe are arranged at the upper part of the concentration tank, a heating jacket is arranged on the outer wall of the concentration tank, and a material discharging port is arranged at the bottom of the concentration tank; the material receiving port is connected with the filter, a condenser is arranged on the solvent outlet pipe, and the solvent outlet pipe is connected with a solvent recovery tank;
the heating jacket is a temperature-adjusting half pipe, and a first heat-conducting coil pipe and a second heat-conducting coil pipe are arranged in parallel inside the temperature-adjusting half pipe; the first heat conduction coil pipe and the second heat conduction coil pipe are respectively connected with heat conduction oil and heat conduction water.
Furthermore, the liquid inlet pipe is connected with a solvent tank, and a metering pump is arranged on the liquid inlet pipe.
Further, the top of the extraction tank is provided with an exhaust port, and the exhaust port is connected with a solvent recovery tank through a pipeline.
Furthermore, the extracting tank and the concentrating tank are both provided with pressure gauges.
Further, the filter both ends can be dismantled respectively and connect the discharge gate and connect the material mouth, the filter both ends all are provided with the ooff valve.
Further, a vacuum pump is arranged on the concentration tank.
Further, the bottom of the extraction tank is conical, and the discharge hole is positioned at the bottom of the conical shape.
Furthermore, a plurality of spray heads are arranged at the bottom of the liquid inlet pipe, and the spray heads are high-pressure spray heads.
Compared with the prior art, the utility model has the following beneficial effects:
(1) this device passes through the mode that ultrasonic wave and heating device combined together, handles behind the little gentiana macrophylla, can furthest draw little gentiana macrophylla pharmacodynamic component to reduce the loss of the pharmacodynamic component who extracts.
(2) The device has simple structure and convenient use, is favorable for improving the efficiency of equipment for extracting and concentrating the effective components of the gentiana macrophylla, and is suitable for extracting the effective components of the small-sized gentiana macrophylla.
(3) The oil bath coil pipe and the water bath coil pipe are arranged in the heating jacket, so that heating or cooling can be controlled by controlling the operation of an oil bath circulation system or a cooling water bath circulation system, the temperature in the tank can be controlled in real time, the heat transfer quantity is adjusted, the accurate control of the temperature is ensured, the extraction quality is improved, the operating environment is good, and the safety coefficient is high.
Drawings
FIG. 1 is a schematic structural view of the present invention;
in the figure: 1-an extraction tank, 2-a feed hopper, 3-a liquid inlet pipe, 4-an electric stirrer, 5-a temperature control probe, 6-a discharge port, 7-a filter, 8-a heating jacket, 9-an ultrasonic generator, 10-a concentration tank, 11-a material receiving port, 12-a solvent outlet pipe, 13-a condenser, 14-a solvent recovery tank, 15-a first heat conduction coil pipe, 16-a second heat conduction coil pipe, 17-a solvent tank, 18-a metering pump, 19-an exhaust port, 20-a pressure gauge, 21-a vacuum pump, 22-a spray head and 23-a discharge port.
Detailed Description
The utility model will be further explained with reference to the drawings.
Examples
An extraction device for effective components of Gentiana macrophylla comprises an extraction tank 1 and a concentration tank 10, wherein the upper part of the extraction tank 1 is provided with a feed hopper 2 and a liquid inlet pipe 3, the interior of the extraction tank is provided with an electric stirrer 4 and a temperature control probe 5, the lower part of the extraction tank is provided with a discharge hole 6, and the discharge hole 6 is provided with a filter 7; the outer wall of the extraction tank 1 is provided with a mounting groove and a heating jacket 8, and an ultrasonic generator 9 is arranged in the mounting groove; the upper part of the concentration tank 10 is provided with a material receiving port 11 and a solvent outlet pipe 12, the outer wall of the concentration tank is provided with a heating jacket 8, and the bottom of the concentration tank is provided with a material outlet 23; the material receiving port 11 is connected with the filter 7, a condenser 13 is arranged on the solvent outlet pipe 12, and the solvent outlet pipe 12 is connected with a solvent recovery tank 14;
the heating jacket 8 is a temperature-adjusting half pipe, and a first heat-conducting coil 15 and a second heat-conducting coil 16 are arranged in the temperature-adjusting half pipe in parallel; the first heat conducting coil 15 and the second heat conducting coil 16 are respectively connected with heat conducting oil and heat conducting water.
The liquid inlet pipe 3 is connected with a solvent tank 17, and a metering pump 18 is arranged on the liquid inlet pipe 3.
The top of the extraction tank 1 is provided with an exhaust port 19, and the exhaust port 19 is connected with a solvent recovery tank 14 through a pipeline.
The extraction tank 1 and the concentration tank 10 are both provided with a pressure gauge 20.
The filter 7 both ends can be dismantled respectively and connect discharge gate 6 and connect material mouth 11, filter 7 both ends all are provided with the ooff valve.
The concentration tank 10 is provided with a vacuum pump 21.
The bottom of the extraction tank 1 is conical, and the discharge port 6 is positioned at the bottom of the conical shape.
The bottom of the liquid inlet pipe 3 is provided with a plurality of spray heads 22, and the spray heads 22 are high-pressure spray heads.
The working principle of the utility model is as follows:
when using, smash little large-leaf gentian root raw materials, accurately weigh, add through feeder hopper 1 and draw jar 1 inside, with the solvent (for example water, ethanol or methyl alcohol) of appropriate concentration proportion through the measuring pump accurately add inside draw jar 1, according to temperature condition needs, open the heat conduction water or the heat conduction oil of appropriate temperature, draw jar interior material temperature control. The electric stirrer 4 is turned on so that the electric stirrer 4 is rotated at a high speed. Thus, the materials are stirred uniformly by the stirrer 4 rotating at high speed, and the materials are continuously stirred under the stirring action. The ultrasonic generator 9 is started, and the gentiana straminea maxim is extracted by ultrasonic waves, so that the extraction effect and efficiency of the effective components of the gentiana straminea maxim are improved.
Half pipe that adjusts temperature of heating jacket 8 sets up around extracting a jar outer wall spiral, half intraductal first heat conduction coil pipe 15 and the second heat conduction coil pipe 16 of setting up, connect the conduction oil and the heat conduction water of different temperatures respectively, accessible control conduction oil circulation, the operation of heat conduction hydrologic cycle or cooling water bath circulation system, control heats or cools off, with temperature in the real time control jar, adjust the heat transfer capacity, guarantee to extract the temperature accurate control of jar, improve the quality of little gentiana macrophylla pharmacodynamical composition, operation environment is good, high safety factor. When in use, only the first heat conducting coil 15 or the second heat conducting coil 16 may be used, or both coils may be used simultaneously.
After the extraction is completed, the discharge port 6 of the extraction tank 1 is opened, and the mixed material enters the concentration tank 10 from the material receiving port 11 after being filtered by the filter 7. During filtering, the vacuum pump 21 arranged on the concentration tank 10 can be opened to evacuate the air in the concentration tank 2, so as to provide a negative pressure environment, and improve the filtering efficiency.
During concentration, firstly, the extracting solution enters the concentration tank 10 through the material receiving port 11, the material receiving port switch is closed, the vacuum pump 21 is used for vacuumizing, the heating jacket 8 is started at the same time, and the temperature in the concentration tank 10 is raised by utilizing heating oil or heating water, so that the extracting solution in the tank body is heated and concentrated. The solvent in the extracting solution is discharged from a solvent outlet pipe 12, condensed by a condenser 13 and flows into a solvent recovery tank 14 to be collected, so that the solvent is recycled. Finally, the concentrated solution is discharged from the collecting tank through a discharge port 23 while the concentrated solution is hot. In the concentration process, once the temperature control probe 5 detects that the temperature in the concentration tank exceeds the preset value, the temperature of the heat conduction oil or the heat conduction water in the heating jacket 8 is adjusted, the temperature in the concentration tank is controlled, and the damage of the active ingredients of the gentiana macrophylla in the concentration process is avoided.
The device has simple structure and convenient use, is favorable for improving the efficiency of equipment for extracting and concentrating the effective components of the gentiana macrophylla, and is suitable for extracting the effective components of the small-sized gentiana macrophylla.
It should be noted that in the description of the present invention, the terms "center", "upper", "lower", "left", "right", "vertical", "horizontal", "inner", "outer", etc. indicating the directions or positional relationships are based on the directions or positional relationships shown in the drawings, which are only for convenience of description, and do not indicate or imply that the device or element must have a specific orientation, be constructed and operated in a specific orientation, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first," "second," and "third" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.
Furthermore, it should be noted that, in the description of the present invention, unless otherwise explicitly specified or limited, the terms "mounted," "connected," and "connected" are to be construed broadly, and may be, for example, fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood by those skilled in the art according to specific situations.
The terms "comprises," "comprising," or any other similar term are intended to cover a non-exclusive inclusion, such that a process, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, article, or apparatus.
The embodiments of the present invention have been described in detail with reference to the accompanying drawings, but the present invention is not limited to the above embodiments, and various changes can be made within the knowledge of those skilled in the art without departing from the gist of the present invention.
Claims (8)
1. The device for extracting the effective components of gentiana macrophylla is characterized by comprising an extraction tank (1) and a concentration tank (10), wherein the upper part of the extraction tank (1) is provided with a feed hopper (2) and a liquid inlet pipe (3), the interior of the extraction tank is provided with an electric stirrer (4) and a temperature control probe (5), the lower part of the extraction tank is provided with a discharge hole (6), and the discharge hole (6) is provided with a filter (7); the outer wall of the extraction tank (1) is provided with a mounting groove and a heating jacket (8), and an ultrasonic generator (9) is arranged in the mounting groove; a material receiving port (11) and a solvent outlet pipe (12) are arranged at the upper part of the concentration tank (10), a heating jacket (8) is arranged on the outer wall, and a discharge port (23) is arranged at the bottom; the material receiving port (11) is connected with the filter (7), a condenser (13) is arranged on the solvent outlet pipe (12), and the solvent outlet pipe (12) is connected with a solvent recovery tank (14);
the heating jacket (8) is a temperature-adjusting half pipe, and a first heat-conducting coil pipe (15) and a second heat-conducting coil pipe (16) are arranged in the temperature-adjusting half pipe in parallel; the first heat conduction coil pipe (15) and the second heat conduction coil pipe (16) are respectively connected with heat conduction oil and heat conduction water.
2. The extraction device of gentiana straminea maxim pharmacodynamic ingredients according to claim 1, wherein the liquid inlet pipe (3) is connected with a solvent tank (17), and a metering pump (18) is arranged on the liquid inlet pipe (3).
3. The extraction device of gentiana straminea maxim drug effect components as claimed in claim 1, wherein an exhaust port (19) is arranged at the top of the extraction tank (1), and the exhaust port (19) is connected with a solvent recovery tank (14) through a pipeline.
4. The extraction device of gentiana straminea maxim medicinal components as claimed in claim 1, wherein the pressure gauge (20) is installed on each of the extraction tank (1) and the concentration tank (10).
5. The device for extracting effective components from gentiana macrophylla according to claim 1, wherein the two ends of the filter (7) are detachably connected with the discharge port (6) and the receiving port (11), and the two ends of the filter (7) are provided with switch valves.
6. The extraction device of gentiana straminea maxim medicinal components as claimed in claim 1, wherein the vacuum pump (21) is disposed on the concentration tank (10).
7. The extraction device of gentiana straminea maxim medicinal components as claimed in claim 1, wherein the bottom of the extraction tank (1) is conical, and the discharge port (6) is located at the conical bottom.
8. The extraction device of gentiana straminea maxim pharmacodynamic ingredients according to claim 1, wherein a plurality of nozzles (22) are arranged at the bottom of the liquid inlet pipe (3), and the nozzles (22) are high pressure nozzles.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202123119381.XU CN216366719U (en) | 2021-12-09 | 2021-12-09 | Extraction element of little large-leaved gentian pharmacodynamic ingredient |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202123119381.XU CN216366719U (en) | 2021-12-09 | 2021-12-09 | Extraction element of little large-leaved gentian pharmacodynamic ingredient |
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| Publication Number | Publication Date |
|---|---|
| CN216366719U true CN216366719U (en) | 2022-04-26 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202123119381.XU Expired - Fee Related CN216366719U (en) | 2021-12-09 | 2021-12-09 | Extraction element of little large-leaved gentian pharmacodynamic ingredient |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115300935A (en) * | 2022-08-05 | 2022-11-08 | 重庆市药研院制药有限公司 | Concentration device and concentration method for extract of root pieces of herba pyrrosiae |
-
2021
- 2021-12-09 CN CN202123119381.XU patent/CN216366719U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115300935A (en) * | 2022-08-05 | 2022-11-08 | 重庆市药研院制药有限公司 | Concentration device and concentration method for extract of root pieces of herba pyrrosiae |
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| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20220426 |