CN2160482Y - Quick freezing device for metals - Google Patents

Quick freezing device for metals Download PDF

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Publication number
CN2160482Y
CN2160482Y CN 93200732 CN93200732U CN2160482Y CN 2160482 Y CN2160482 Y CN 2160482Y CN 93200732 CN93200732 CN 93200732 CN 93200732 U CN93200732 U CN 93200732U CN 2160482 Y CN2160482 Y CN 2160482Y
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CN
China
Prior art keywords
metal
quick freezing
water
freezing device
cooling medium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN 93200732
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Chinese (zh)
Inventor
沈宁福
张东捷
徐长白
汤亚力
邵国胜
仝兴存
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ZHENGZHOU POLYTECHNICAL COLLEGE
Original Assignee
ZHENGZHOU POLYTECHNICAL COLLEGE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ZHENGZHOU POLYTECHNICAL COLLEGE filed Critical ZHENGZHOU POLYTECHNICAL COLLEGE
Priority to CN 93200732 priority Critical patent/CN2160482Y/en
Application granted granted Critical
Publication of CN2160482Y publication Critical patent/CN2160482Y/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)

Abstract

The utility model discloses a quick freezing device for metal, which can manufacture the microcrystal powder granules of the metal or flakes. The structure of the quick freezing device for metal is that the upper part of the quick freezing chamber is provided with a casting cup and a press head; the external side of the casting cup is provided with the external cover of the protective gas; the metal liquid can be ejected on an impeller disk which conducts the high-speed rotation through a nozzle; the metal liquid is excited to be the microcrystal powder granules or the flakes through the cold forming, and in addition, the quick freezing chamber is also provided with a spraying annular pipe and a metal pipe which are injected with the cooling medium. The quick freezing device for metal is suitable for producing all kinds of quick freezing alloys.

Description

Quick freezing device for metals
The utility model relates to a kind of equipment that obtains solidified metal microcrystalline powder or thin slice.
Announced a kind of preparation facilities of metal fine powder among the clear 63-221831 of day disclosure special permission communique (A); be characterized in that one horizontally rotates impeller; an and perpendicular nozzle; this patent does not relate to the cooling problem of rotating disk; there is not the protective gas cover in addition around the nozzle; metal liquid stream is gravity-assist pouring, and speed is not high, so metal dust cooling velocity not high (<10 5K/S), degree of oxidation is more serious.
The production metal powder device that the clear 59-159903 of day disclosure special permission communique (A) announces, its cooling substrate is tapered CD, its hitting power to metal liquid stream is little, so cooling velocity is not high yet.
The purpose of this utility model is to provide a kind of can improve the metal cooling velocity, reduces the preparation microcrystalline powder of degree of oxidation or the quick solidification apparatus of thin slice.
Thereby the utility model device is to realize rapid solidification by hitting metal liquid stream near cold metal blade in the high thermal conductivity of nozzle.
The utility model device is as shown in Figure 1: be placed with in rapid solidification chamber (9) top hold metal liquid (3) water cup (1), water the cup top one ventilation pressure head (11) is arranged, water the outer cover (2) that logical protective gas is equipped with in cup (1) outside, water the cup (a 1) bottom one nozzle (4) is arranged, there is a metallic impeller dish (5) below of nozzle (4); Inwall in rapid solidification chamber (9) has the spray ring pipe (6) of a logical cooling medium in addition, and the metal tube (7) of an injection cooling medium is arranged above the metallic impeller dish.
The utility model is to realize rapid solidification like this: water under the gas pressure effect of metal liquid (3) in pressure head (11) in the cup (1); form the liquid fluidization tower by nozzle (4); this liquid fluidization tower is passed into the protective gas protection in the protective gas cover (2); and the blade on the metallic impeller dish (5) that is rotated at a high speed soon hits; disperse; be frozen into powder or thin slice tangentially flies out along blade; these powders or thin slice flow under the cooling medium of ring pipe (6) ejection impacts and collect mouthful (10); at the same time; also cooling medium can be sprayed from the mouth of pipe (7), in order to cool metal blade and metal powder grain and thin slice.
This device characteristic is that the free travel of metal liquid stream is short, and cut apart, hit by the high interior cold blade of thermal conductivity, solidify with the solid dielectric heat-conducting mode, the rotating speed of impeller is 3000~7000 rev/mins, and impeller diameter is φ 180mm~280mm, thickness 10~20mm, make with fine copper or copper alloy, also other metal material of available other good heat conductivity is made, in addition blade surface also the method handled of usable surface increase the blade thermal conductivity, improve peptizaiton to metal fluid.The utility model device, cold blade has the hitting power of 4MPa in it to metal liquid stream, its cooling effect is higher than the ultrasonic atomizatio method fuel pulverizing plant that revolves casting device and fluid media (medium) heat conduction of solid dielectric heat conduction, and its oxidated layer thickness is equivalent to vacuum gas atomising device effect built in~5nm.This device hourly output is 30kg, and its granularity is adjustable.
Description of drawings
Fig. 1. the metal quick solidification apparatus
Fig. 2. the utility model impeller vertical view
Fig. 3. the utility model impeller side view
Embodiment
1. rapid solidification Al-Si-Ti, Al-Zn-Mg-Cu, Al-Fe alloy microcrystalline powder or web preparation.
With pressure head exit gas pressure 3.5kg/cm 2, protective gas pressure 2kg/cm 2, 6000 rev/mins of wheel speeds, impeller diameter 200mm, nozzle and impeller height 13mm, interior cold and spray medium is to obtain Al-Si-Ti, Al-Zn-Mg-Cu and Al-Fe microcrystalline powder and thin slice under the condition of water, particle mean size is~200um cooling velocity〉10 6K/s, powder surface oxidation layer thickness~5nm.Output 30kg/ hour.

Claims (2)

1, a kind of metal quick solidification apparatus that relates to rapid solidification field manufacturing microcrystallizing alloy; it is characterized in that: rapid solidification chamber (9) top is placed with water glass (1) that holds metal liquid (3); water the cup top one pressure head (11) is arranged; water the outer cover (2) that logical protective gas is equipped with in cup (1) outside; one metallic impeller dish (5) is arranged in the below of nozzle (4), and the inwall in rapid solidification chamber (9) has the spray ring pipe (6) of a logical cooling medium in addition.The metal tube (7) that one injection cooling medium is arranged above the metallic impeller dish.
2, metal quick solidification apparatus according to claim 1 is characterized in that an inner cold water road is arranged on the said metallic impeller dish (5), and water channel extends to the metal blade of high thermal conductivity.
CN 93200732 1993-01-05 1993-01-05 Quick freezing device for metals Expired - Fee Related CN2160482Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 93200732 CN2160482Y (en) 1993-01-05 1993-01-05 Quick freezing device for metals

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 93200732 CN2160482Y (en) 1993-01-05 1993-01-05 Quick freezing device for metals

Publications (1)

Publication Number Publication Date
CN2160482Y true CN2160482Y (en) 1994-04-06

Family

ID=33785416

Family Applications (1)

Application Number Title Priority Date Filing Date
CN 93200732 Expired - Fee Related CN2160482Y (en) 1993-01-05 1993-01-05 Quick freezing device for metals

Country Status (1)

Country Link
CN (1) CN2160482Y (en)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100569415C (en) * 2003-03-28 2009-12-16 独立行政法人科学技术振兴机构 The metal jet device
CN102233431A (en) * 2010-05-07 2011-11-09 乐普(北京)医疗器械股份有限公司 Method for preparing magnesium alloy material
CN103212717A (en) * 2013-02-26 2013-07-24 连云港倍特超微粉有限公司 Rotary tube type device and method for preparing zinc alloy blasting shots
CN111558723A (en) * 2020-06-24 2020-08-21 湖南天际智慧材料科技有限公司 Device and method for rapidly producing amorphous powder by water atomization method
CN113618074A (en) * 2021-08-16 2021-11-09 辽宁科技大学 Device and method for preparing iron alloy particles
CN113828783A (en) * 2020-06-24 2021-12-24 湖南天际智慧材料科技有限公司 Rapid cooling production equipment and method for amorphous powder
CN113828780A (en) * 2020-06-24 2021-12-24 湖南天际智慧材料科技有限公司 Secondary quenching type amorphous powder production equipment and method thereof
CN113828782A (en) * 2020-06-24 2021-12-24 湖南天际智慧材料科技有限公司 Production method and equipment of amorphous material
CN113828781A (en) * 2020-06-24 2021-12-24 湖南天际智慧材料科技有限公司 Device and method for producing amorphous powder by water atomization method

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100569415C (en) * 2003-03-28 2009-12-16 独立行政法人科学技术振兴机构 The metal jet device
CN102233431A (en) * 2010-05-07 2011-11-09 乐普(北京)医疗器械股份有限公司 Method for preparing magnesium alloy material
CN103212717A (en) * 2013-02-26 2013-07-24 连云港倍特超微粉有限公司 Rotary tube type device and method for preparing zinc alloy blasting shots
CN111558723A (en) * 2020-06-24 2020-08-21 湖南天际智慧材料科技有限公司 Device and method for rapidly producing amorphous powder by water atomization method
CN113828783A (en) * 2020-06-24 2021-12-24 湖南天际智慧材料科技有限公司 Rapid cooling production equipment and method for amorphous powder
CN113828780A (en) * 2020-06-24 2021-12-24 湖南天际智慧材料科技有限公司 Secondary quenching type amorphous powder production equipment and method thereof
CN113828782A (en) * 2020-06-24 2021-12-24 湖南天际智慧材料科技有限公司 Production method and equipment of amorphous material
CN113828781A (en) * 2020-06-24 2021-12-24 湖南天际智慧材料科技有限公司 Device and method for producing amorphous powder by water atomization method
CN113618074A (en) * 2021-08-16 2021-11-09 辽宁科技大学 Device and method for preparing iron alloy particles

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GR01 Patent grant
C19 Lapse of patent right due to non-payment of the annual fee
CF01 Termination of patent right due to non-payment of annual fee