CN2159819Y - Suspending cone centrifugal molecular distiller - Google Patents
Suspending cone centrifugal molecular distiller Download PDFInfo
- Publication number
- CN2159819Y CN2159819Y CN 93211495 CN93211495U CN2159819Y CN 2159819 Y CN2159819 Y CN 2159819Y CN 93211495 CN93211495 CN 93211495 CN 93211495 U CN93211495 U CN 93211495U CN 2159819 Y CN2159819 Y CN 2159819Y
- Authority
- CN
- China
- Prior art keywords
- cone
- rotary drum
- outlet
- distillation
- distillate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a suspending cone-shaped centrifugal molecular distiller which is composed of a suspending type cone-shaped rotary drum, a magnetic transmission device, a condenser for an electric heater.,a distillate receiver, a vacuum casing, etc. The utility model is suitable for high vacuum distillation and molecular distillation of thermosensitive materials. Compared with the prior art, the utility model has the advantages that the fabrication and the installation are convenient, the splash of entrainment can be prevented, the quality of products can be improved, etc. Because the relative evaporation area of the structure is large, the relative yield is large; the condensation are is large, and molecules can be close to the evaporation surface. The distillation of the molecules can be completed under the condition that the molecular free path is comparatively short, and the effect of the distillation is good.
Description
The utility model belongs to a kind of distillation equipment, is applicable to the high vacuum distillation and the molecular clock of higher boiling heat-sensitive materials.
The rotary drum of centrifugal molecular distillator system is installed on the base in the prior art, and condenser then is installed on the top cover, as the centrifugal molecular distillator of U.S. CVC company production.The processing and manufacturing of this kind structure is had relatively high expectations, owing to cause that very easily mist splashes during the less and misoperation of its relative disengagement area, affects the quality and yield of distillage.
The utility model purpose is to provide a kind of can preventing of being easy to make, and mist from splashing, and the relative all bigger outstanding taper centrifugal molecular distillator with condensation area of disengagement area.
According to the purpose of this utility model, designer's solution is that the taper centrifugal reel is hung vertically on the top cover, drives by magnetic drive device and makes its rotation, therefore is easy to make.After material enters rotary drum, upwards flow because the component of centrifugal force makes it become membranaceous, the molecule that evaporates after being heated condenses into distillate because the dirty distillate receiver that enters of gravity effect after running into condenser.Issuable mist also splashes away owing to action of centrifugal force is difficult to break away from rotary drum.
Accompanying drawing is the utility model structural representation
With reference to accompanying drawing, be vertically installed with the rotatable top board 3 that drives by magnetic drive device 2 for 1 time at top cover, rotary drum (cone-element) 4 is fixed on below the top board 3, rotary drum (cone-element) 4 outer electric heater 5 and the thermometer 6 of being with, heating and control temperature.Rotary drum (cone-element) 4 inner chambers have a grid formula condenser 7 that puts in from the bottom.Rotary drum 4 and electric heater 5 all are sealed in the vacuum casting 8.Condenser 7 is fixed on the base 9, is connected with distillate receiver 10 below the base 9, and there are a vacuum interface 11 that can be connected with the external vacuum system and distillate outlet 12 in its side.Cooling water inlet 13 also is housed, coolant outlet 14, material inlet 15 and vinasse outlet 16 on the base 9.
By above-mentioned formation, its operating process was as follows when present embodiment was used as the heat-sensitive materials molecular clock:
At first this equipment is vacuumized and reach desired degree (overbottom pressure 0.01-10Pa) and regulate electric heater 5 and make rotary drum 4 be warmed up to predetermined temperature with the external vacuum system, start magnetic drive device 2 and make rotary drum 4 rotations, feed cooling water by water inlet pipe and water outlet pipe 13,14 and can begin distillation procedure.
Material through degassing preheating enters the bottom of rotary drum (cone-element) 4 by feed pipe 15, because acting as of centrifugal force molecule membranaceously upwards flow, the molecule that volatilizes of the being heated device 7 that is condensed is condensed into that the liquid gravitate is dirty to be collected in the distillate receiver 10.Vinasse throws away by the slit between rotary drum (cone-element) 4 and the top board 3 owing to action of centrifugal force, and is dirty along vacuum casting, discharges from raffinate outlet 16.
The distiller that constitutes according to the utility model purpose has to be convenient to make and install, can prevent that mist from splashing, characteristics such as improve the quality of products, because relative disengagement area is big, so fractional yield is bigger, and condensation area is big and can more press close to evaporating surface, and making can be at molecular free path than finishing distillation under the billet spare, the distillation efficiency height.
Claims (1)
1, a kind of vacuum distillation of higher boiling heat-sensitive materials and outstanding taper centrifugal molecular distillator of molecular clock of being used for, comprise top cover (1), rotary drum (cone-element) (4), electric heater (5), thermometer (6), condenser (7), base (9), distillate receiver (10), vacuum interface (11), distillate outlet (12), cooling water inlet (13), coolant outlet (14), material inlet (15), vinasse outlet (16), shell (8), the top that it is characterized in that top cover (1) is provided with magnetic drive device (2) and a rotatable top board (3) that driven by magnetic drive device (2), rotary drum (cone-element) (4) is suspended on below the top board (3), electric heater (5) and thermometer (6) are located at the outside of rotary drum (cone-element) (4), condenser (7) inserts into the inner the chamber from rotary drum (cone-element) (4) bottom and is fixed on the base (9), rotary drum (cone-element) (4) and heater (5) all are sealed in the vacuum casting (8), distillate receiver (10) is located at below the base (9), distillate receiver (10) side is provided with a vacuum interface (11) that can be connected with vacuum system and distillate outlet (12), and cooling water inlet (13) and outlet (14) and material inlet (15) vinasse outlet (16) are all established and be contained on the base (9).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93211495 CN2159819Y (en) | 1993-04-30 | 1993-04-30 | Suspending cone centrifugal molecular distiller |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93211495 CN2159819Y (en) | 1993-04-30 | 1993-04-30 | Suspending cone centrifugal molecular distiller |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN2159819Y true CN2159819Y (en) | 1994-03-30 |
Family
ID=33793092
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 93211495 Expired - Fee Related CN2159819Y (en) | 1993-04-30 | 1993-04-30 | Suspending cone centrifugal molecular distiller |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN2159819Y (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102743891A (en) * | 2012-08-07 | 2012-10-24 | 饶攀 | Molecular distillation device |
| CN113426148A (en) * | 2021-07-12 | 2021-09-24 | 连云港市第一人民医院 | Molecular distiller for extracting and separating chemical components of traditional Chinese medicine |
-
1993
- 1993-04-30 CN CN 93211495 patent/CN2159819Y/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102743891A (en) * | 2012-08-07 | 2012-10-24 | 饶攀 | Molecular distillation device |
| CN102743891B (en) * | 2012-08-07 | 2014-04-30 | 饶攀 | Molecular distillation device |
| CN113426148A (en) * | 2021-07-12 | 2021-09-24 | 连云港市第一人民医院 | Molecular distiller for extracting and separating chemical components of traditional Chinese medicine |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |