CN214130379U - High-efficient organic compound extraction element - Google Patents
High-efficient organic compound extraction element Download PDFInfo
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- CN214130379U CN214130379U CN202022926057.8U CN202022926057U CN214130379U CN 214130379 U CN214130379 U CN 214130379U CN 202022926057 U CN202022926057 U CN 202022926057U CN 214130379 U CN214130379 U CN 214130379U
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Abstract
The utility model discloses a high-efficiency organic compound extraction device, which comprises a kettle body, wherein the top of the kettle body is provided with a kettle cover for sealing, the surface of the kettle cover is provided with a thermometer interface, a stirring device interface and a gas condensation pipe interface, an interlayer is arranged on the surface of the kettle body, an interlayer liquid outlet and an interlayer liquid inlet are arranged on the surface of the interlayer, the inner part of the kettle body is provided with a interlayer plate, the bottom of the kettle body is provided with a connecting pipe, the other end of the connecting pipe is connected with the receiving kettle body, the side surface of the kettle body is provided with an air duct, the other end of the air duct is connected with a connecting pipe, the bottom end of the kettle body is provided with a U-shaped liquid outlet pipe, and the highest height of the U-shaped liquid outlet pipe is lower than the height of a lower edge interface at the joint of the air guide pipe and the kettle body, the other end of the U-shaped liquid outlet pipe is connected with the receiving kettle body, and a heating bin is arranged on the outer surface of the receiving kettle body. The utility model provides the high efficiency and the purity of extracting.
Description
Technical Field
The utility model belongs to the technical field of the extraction element, concretely relates to high-efficient organic compound extraction element.
Background
In the preparation process of the existing medical intermediate, a great part of compounds are extracted from natural plants, some compounds are chemically synthesized organic matters, the solubility is poor, the purification is not facilitated, the organic solvent is required to be repeatedly used for extraction, the existing device is used for mixing the solvent and the material to be extracted, stirring is carried out for a certain time, the product is saturated in the solvent, filtering is carried out, the solvent is evaporated from filtrate, the solvent is heated and dissolved with a filter cake and then filtered, the solvent is repeatedly dissolved, filtered and extracted, a large amount of organic solvent is consumed in the process, and meanwhile, a large amount of manpower and production equipment are occupied. And because the extraction efficiency is low, the industrial production cost is high. Therefore, a high-efficiency organic compound extraction device is needed to solve the above problems and meet the needs of people.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a high-efficient organic compound extraction element to solve the problem that proposes among the above-mentioned background art.
In order to achieve the above object, the utility model provides a following technical scheme: the utility model provides a high-efficient organic compound extraction element, includes the cauldron body, the top of the cauldron body is provided with the kettle cover that is used for sealing, the surface of kettle cover is provided with thermometer interface, agitating unit interface, gas condenser pipe interface.
The surface of the kettle body is provided with an interlayer, and the surface of the interlayer is provided with an interlayer liquid outlet and an interlayer liquid inlet.
The inside of the cauldron body is provided with the interlayer board, the bottom of the cauldron body is provided with the connecting pipe, the other end of connecting pipe with receive the cauldron body coupling, the side of the cauldron body is provided with the air duct, the other end and the connecting pipe of air duct are connected, the bottom of the cauldron body is provided with U type drain pipe, and the highest height of U type drain pipe is less than the interface height along the lower of air duct and cauldron body coupling department, the other end of U type drain pipe with receive the cauldron body coupling.
The surface of the receiving kettle body is provided with a heating bin, and an outlet of the receiving kettle body is provided with a discharge valve.
Preferably, a condensing pipe is arranged in the gas condensing pipe interface, and a liquid inlet and a liquid outlet are arranged on the surface of the condensing pipe.
In any of the above schemes, preferably, the cross-sectional area of the gas-guide tube is 0.2-2.0 times of the cross-sectional area of the upper opening of the receiving kettle body.
In any of the above schemes, preferably, one of water bath heating and electric jacket heating is adopted in the heating chamber.
In any of the above schemes, preferably, the interlayer plate is one of a sand core plate, a metal mesh plate, a ceramic mesh plate and a mesh plate made of tetrafluoro material.
In any one of the above schemes, preferably, the connecting part of the kettle cover and the kettle body is provided with a rotating shaft, and the kettle cover is rotatably connected with the kettle body through the rotating shaft.
Preferably in any one of the above schemes, the kettle cover and the kettle body are integrally arranged, and the upper surface of the kettle cover is provided with a feed inlet.
In any of the above schemes, preferably, the surface of the kettle body is provided with a plurality of solid waste outlets, and the solid waste outlets are located above the interlayer plate.
The utility model discloses a technological effect and advantage: 1. the utility model adds the interlayer plate at the lower part of the material storage kettle body, which can effectively separate solid and liquid to avoid the problem of difficult filtration of the traditional equipment;
2. the extraction equipment in the utility model, the design of the heating bin arranged outside the air duct, the liquid outlet pipe, the condensing pipe and the receiving kettle body can lead the solvent for extraction to be recycled, compared with the traditional extraction filtration process, the utilization amount of the organic solvent is greatly reduced, and the operation workload of personnel is reduced;
3. the extraction equipment in the utility model, the design of the U-shaped liquid outlet pipe, can fully soak the solid materials by the organic solvent, improve the extraction effect of the target compounds and effectively save the extraction time;
4. the utility model provides an extract equipment heats cauldron body material through cauldron body intermediate layer, through improving the temperature in the cauldron for target substance's the speed of dissolving out improves extraction efficiency and purity.
Drawings
Fig. 1 is a schematic structural diagram of the present invention.
In the figure: 1. a kettle body; 2. an interlayer; 3. an interlayer liquid outlet; 4. a liquid inlet of the interlayer; 5. a thermometer interface; 6. a stirring device interface; 7. a gas condenser tube interface; 8. a interlayer plate; 9. an air duct; 10. a solid waste residue outlet; 11. a U-shaped liquid outlet pipe; 12. a connecting pipe; 13. a receiving kettle body; 14. a heating chamber; 15. a discharge valve; 16. and (5) a kettle cover.
Detailed Description
The following describes the present invention with reference to the accompanying drawings. It should be noted that the description of the embodiments is provided to help understanding of the present invention, but the present invention is not limited thereto. In addition, the technical features related to the embodiments of the present invention described below may be combined with each other as long as they do not conflict with each other.
The utility model provides a high-efficiency organic compound extraction device as shown in figure 1, which comprises a kettle body 1, wherein the surface of the kettle body 1 is provided with a plurality of solid waste residue outlets 10, the solid waste residue outlets 10 are positioned above a interlayer plate 8, when the number of the solid waste residue outlets 10 is selected according to the volume of the kettle body 1, the solid waste residue outlets 10 can be connected with the kettle body 1 by nuts or bayonets, gaskets are added in the middle to ensure the sealing performance of the kettle body, the top of the kettle body 1 is provided with a kettle cover 16 for sealing, the joint of the kettle cover 16 and the kettle body 1 is provided with a rotating shaft, the kettle cover 16 is rotatably connected with the kettle body 1 by the rotating shaft, when the kettle cover is rotatably connected, a gasket is added between the interface of the kettle cover 16 and the kettle body 1, then the metal bayonets or screws and nuts are connected to achieve the sealing effect, the kettle cover 16 and the kettle body 1 are integrally arranged, and the upper surface of the kettle cover 16 is provided with a charging hole, a thermometer interface 5, a stirring device interface 6 and a gas condensation pipe interface 7 are arranged on the surface of the kettle cover 16, the interfaces are standard interfaces to equip a condensation pipe, a stirring device and a thermometer, a condensation pipe is arranged in the gas condensation pipe interface 7, and a liquid inlet and a liquid outlet are arranged on the surface of the condensation pipe;
an interlayer 2 is arranged on the surface of the kettle body 1, an interlayer liquid outlet 3 and an interlayer liquid inlet 4 are arranged on the surface of the interlayer 2, and an external bath medium with a certain temperature is introduced into the interlayer 2 in the extraction process to control the temperature of the extracted materials in the kettle body 1, so that the extraction rate and the extraction purity are improved;
the inner part of the kettle body 1 is provided with a interlayer plate 8, the interlayer plate 8 is a detachable plate, the interlayer plate 8 is a mesh plate with a mesh number, the interlayer plate 8 can isolate solid particles, but liquid can pass through, the interlayer plate 8 is one of a sand core plate, a metal mesh plate, a ceramic mesh plate and a mesh plate made of PTFE material, or other plates with the function, the bottom of the kettle body 1 is provided with a connecting pipe 12, one end of the connecting pipe 12 is not communicated with the bottom of the kettle body 1 and is only fixedly connected on the surface of the kettle body 1, the other end of the connecting pipe 12 is connected with a receiving kettle body 13, the connection is communicated, the connecting pipe 12 can be a ground port, a flange interface and the like, so that the receiving kettle body 13 is connected with the kettle body 1 through a movable port capable of sealing, the side surface of the kettle body 1 is provided with an air duct 9, the air duct 9 is a circulating pipeline for communicating the kettle body 1 with the kettle body 13 and gasifying a solvent in the receiving kettle body 13, the sectional area of the air duct 9 is 0.2-2.0 times of the sectional area of the upper opening of the receiving kettle body 13, the other end of the air duct 9 is connected with a connecting pipe 12, the connection is a communication arrangement, a U-shaped liquid outlet pipe 11 is arranged at the bottom end of the kettle body 1, the U-shaped liquid outlet pipe 11 can effectively raise the height of a soaking solvent in the kettle body 1 so as to achieve the purpose of fully mixing extracted solids and the solvent and improve the extraction effect, one end of the U-shaped liquid outlet pipe 11 penetrates through the kettle body 1 for the liquid under the interlayer plate 8 to flow out, the highest height of the U-shaped liquid outlet pipe 11 is lower than the height of a lower edge interface at the connection part of the air duct 9 and the kettle body 1, the other end of the U-shaped liquid outlet pipe 11 is connected with the receiving kettle body 13, and the connection is a communication arrangement;
the outer surface of the receiving kettle body 13 is provided with a heating bin 14, the receiving kettle body 13 is placed in the heating bin 14 and can be taken out at any time, one of water bath heating and electric jacket heating is adopted in the heating bin 14 and the heating bin 14, and a discharge valve 15 is arranged at an outlet of the receiving kettle body 13.
In the using process of the high-efficiency organic compound extraction device, firstly, Chinese herbal medicines or organic mixtures to be extracted are put into a kettle body 1, an external bath medium with a certain temperature is introduced from an interlayer liquid inlet 4 and is discharged from an interlayer liquid outlet 3, so that the interior of the kettle body 1 is always kept at a proper temperature, the extraction rate is improved, then a thermometer, a stirring device and a condenser pipe are correspondingly arranged through an interface on a kettle cover 16, the thermometer constantly records the temperature of the interior of the kettle body 1, the stirring device stirs substances to be extracted in the kettle body 1 so as to fully extract, the extracted compounds and organic solvents pass through a partition plate 8 and enter a receiving kettle body 13 along a U-shaped liquid outlet pipe 11 for collection, then heating is carried out through a heating bin 14, the organic solvents in the receiving kettle body 13 are evaporated, and the gasified organic solvents enter the kettle body 1 from an air guide pipe 9, so that the organic solvent is recycled, and the extracted compound is enriched in the receiving kettle body 13 and then discharged and collected from the receiving kettle body 13 through the discharge valve 15.
Although embodiments of the present invention have been shown and described, it is understood that the above embodiments are exemplary and should not be construed as limiting the present invention, and that variations, modifications, substitutions and alterations can be made to the above embodiments by those of ordinary skill in the art without departing from the scope of the present invention.
Claims (8)
1. An efficient organic compound extraction device, characterized in that: the device comprises a kettle body (1), wherein a kettle cover (16) used for sealing is arranged at the top of the kettle body (1), and a thermometer interface (5), a stirring device interface (6) and a gas condensation pipe interface (7) are arranged on the surface of the kettle cover (16);
an interlayer (2) is arranged on the surface of the kettle body (1), and an interlayer liquid outlet (3) and an interlayer liquid inlet (4) are arranged on the surface of the interlayer (2);
the kettle is characterized in that a interlayer plate (8) is arranged inside the kettle body (1), a connecting pipe (12) is arranged at the bottom of the kettle body (1), the other end of the connecting pipe (12) is connected with a receiving kettle body (13), an air duct (9) is arranged on the side surface of the kettle body (1), the other end of the air duct (9) is connected with the connecting pipe (12), a U-shaped liquid outlet pipe (11) is arranged at the bottom end of the kettle body (1), the highest height of the U-shaped liquid outlet pipe (11) is lower than the height of a lower edge interface at the joint of the air duct (9) and the kettle body (1), and the other end of the U-shaped liquid outlet pipe (11) is connected with the receiving kettle body (13);
the outer surface of the receiving kettle body (13) is provided with a heating bin (14), and an outlet of the receiving kettle body (13) is provided with a discharge valve (15).
2. A high efficiency organic compound extraction apparatus as defined in claim 1, wherein: and a condensing pipe is arranged in the gas condensing pipe interface (7), and a liquid inlet and a liquid outlet are arranged on the surface of the condensing pipe.
3. A high efficiency organic compound extraction apparatus as defined in claim 1, wherein: the sectional area of the gas guide pipe (9) is 0.2-2.0 times of the sectional area of the upper opening of the receiving kettle body (13).
4. A high efficiency organic compound extraction apparatus as defined in claim 1, wherein: one of water bath heating and electric heating jacket heating is adopted in the heating bin (14).
5. A high efficiency organic compound extraction apparatus as defined in claim 1, wherein: the interlayer plate (8) is one of a sand core plate, a metal screen plate, a ceramic screen plate and a screen plate made of PTFE materials.
6. A high efficiency organic compound extracting apparatus as set forth in any one of claims 1 to 5, wherein: the kettle cover (16) is provided with a rotating shaft at the joint of the kettle body (1), and the kettle cover (16) is rotatably connected with the kettle body (1) through the rotating shaft.
7. A high efficiency organic compound extraction apparatus as defined in claim 1, wherein: the kettle cover (16) and the kettle body (1) are arranged integrally, and a feed inlet is formed in the upper surface of the kettle cover (16).
8. A high efficiency organic compound extraction apparatus as defined in claim 1, wherein: the surface of the kettle body (1) is provided with a plurality of solid waste residue outlets (10), and the solid waste residue outlets (10) are positioned above the interlayer plate (8).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022926057.8U CN214130379U (en) | 2020-12-07 | 2020-12-07 | High-efficient organic compound extraction element |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202022926057.8U CN214130379U (en) | 2020-12-07 | 2020-12-07 | High-efficient organic compound extraction element |
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| CN214130379U true CN214130379U (en) | 2021-09-07 |
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| CN202022926057.8U Active CN214130379U (en) | 2020-12-07 | 2020-12-07 | High-efficient organic compound extraction element |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115487536A (en) * | 2022-10-25 | 2022-12-20 | 湖南农业大学 | Large Soxhlet extraction equipment and method for extracting materials |
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2020
- 2020-12-07 CN CN202022926057.8U patent/CN214130379U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115487536A (en) * | 2022-10-25 | 2022-12-20 | 湖南农业大学 | Large Soxhlet extraction equipment and method for extracting materials |
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