CN212594118U - Multifunctional tank capable of extracting, separating, concentrating, crystallizing and filtering - Google Patents
Multifunctional tank capable of extracting, separating, concentrating, crystallizing and filtering Download PDFInfo
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- CN212594118U CN212594118U CN202020869178.0U CN202020869178U CN212594118U CN 212594118 U CN212594118 U CN 212594118U CN 202020869178 U CN202020869178 U CN 202020869178U CN 212594118 U CN212594118 U CN 212594118U
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/10—Greenhouse gas [GHG] capture, material saving, heat recovery or other energy efficient measures, e.g. motor control, characterised by manufacturing processes, e.g. for rolling metal or metal working
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Abstract
The utility model discloses a can extract, divide liquid, concentrate, crystallization, filterable multi-functional jar, including multi-functional jar, press from both sides cover, bottom valve, glass pipe, filter, storage tank, sight glass, eyepiece, advance pipe, heat exchanger, recovery jar and dropwise add device, the utility model discloses a one set of system has gathered a plurality of operation technology such as extraction, branch liquid, concentrate, crystallization, filtration in a multi-functional jar, has reduced the equipment input, does not occupy more production places, increases the security and the convenience of production operation simultaneously, changes into new multi-functional jar operation, and production operating time is less than half the time at ordinary times, and solvent recovery has compared and has improved 30%, and cleaning device's waste water only has original one fifth, and the production operation workshop has also not had the irritability smell of solvent, and is littleer to the injury of operation staff.
Description
The technical field is as follows:
the utility model belongs to the technical field of the bio-pharmaceuticals, especially, relate to a can extract, divide liquid, concentrate, crystallization, filterable multi-functional jar.
Background art:
in the process of extracting a product from microbial cells with an organic solvent, metabolites of the microorganism and other impurities are generally dissolved in the solvent. And then, the physicochemical properties of the product are utilized to perform back and forth extraction by using different solvents, so that the product is separated from impurities, and a refined product is obtained.
In industrial production, different professional equipment is used for independent operation. The extraction is carried out by adding organic solvent into an extraction tank; after extraction is finished, transferring the feed liquid into a liquid separating tank, standing for 1h, and carrying out liquid separating operation after the feed liquid is separated; after the separation is finished, transferring the upper layer material solution to a concentration kettle for concentration; after the concentration is finished, the concentrated solution is transferred to a crystallization kettle for the last step of crystallization, and the filtration is finished. In the process, the materials are transferred in four sets of equipment and single operation is completed, so that the use efficiency of the equipment is reduced, and the loss in the material transfer process is increased; the solvent is easy to volatilize, inflammable and explosive, and the potential safety hazard is increased. Therefore, a multifunctional tank capable of performing extraction, liquid separation, concentration, crystallization and filtration is necessary.
The utility model has the following contents:
in order to solve the problems, the utility model provides a multifunctional tank capable of extracting, separating, concentrating, crystallizing and filtering, which is characterized in that the multifunctional tank comprises a multifunctional tank, a jacket, a bottom valve, a glass tube, a filter, a storage tank, a sight glass, an ocular lens, an inlet tube, a heat exchanger, a recovery tank and a dripping device, the jacket is lined in the multifunctional tank, the jacket is respectively connected with a steam inlet and outlet pipeline and a cooling water inlet and outlet pipeline through valves, the bottom of the multifunctional tank is connected with the bottom valve, the bottom valve is connected with the glass tube through a jacket connecting piece, the bottom of the glass tube is connected with a valve, the bottom of the valve is connected with a tee joint of a three-way pipeline, the two-way of the three-way pipeline is connected with the filter through a pipeline, the filter is connected with a first storage tank, the three-way joint is connected with, inside is equipped with the stirring rake that is connected with agitator motor, agitator motor has frequency conversion device, multi-functional jar top is equipped with eyepiece and two and advances the pipe, and one advances the pipe and be the liquid inlet pipe, and another advances union coupling has the heat exchanger, the liquid inlet pipe is connected with feed liquid import and nitrogen gas respectively, heat exchanger below exit linkage has the recovery jar, the recovery jar is connected with vacuum unit, dropwise add device is installed to multi-functional jar top, dropwise add device is including the flowmeter, valve and the second storage tank that connect gradually.
Preferably, a valve is arranged on a pipeline between the two-way of the three-way pipeline and the filter.
Preferably, a valve is arranged between the filter and the first storage tank.
Preferably, a valve is arranged between the inlet pipe and the heat exchanger.
Preferably, a valve is arranged between the liquid feeding pipe and the feed liquid inlet.
Preferably, a valve is arranged between the recovery tank and the vacuum unit.
The utility model discloses beneficial effect: the utility model discloses a multi-functional jar lies in having assembleed a plurality of operation technology such as extraction, liquid separation, concentration, crystallization, filtration in a multi-functional jar through one set of system, has reduced the equipment input, does not occupy more production places of production, increases the security and the convenience of production operation simultaneously. The operation of the new multifunctional tank is changed, the production operation time is half less than that in ordinary times, the solvent recovery ratio is improved by 30 percent, the waste water for cleaning equipment is only one fifth of that in the prior art, and the production operation workshop has no pungent smell of the solvent and has less harm to operators.
Description of the drawings:
for ease of illustration, the invention is described in detail by the following detailed description and accompanying drawings.
Fig. 1 is a schematic view of the overall structure of the present invention.
In the figure: 1-a jacket; 2-a bottom valve; 3-a ferrule connector; 4-a glass tube; 5-a filter; 6-a first storage tank; 7-sight glass; 8-a stirring motor; 9-stirring paddle; 10-ocular lens; 11-a heat exchanger; 12-a recovery tank; 13-a vacuum unit; 14-a flow meter; 15-second reservoir.
The specific implementation mode is as follows:
in order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention will be described below with reference to specific embodiments shown in the accompanying drawings. It should be understood that the description is intended to be illustrative only and is not intended to limit the scope of the present invention. Moreover, in the following description, descriptions of well-known structures and techniques are omitted so as to not unnecessarily obscure the concepts of the present invention.
As shown in figure 1, the utility model discloses a can extract, divide liquid, concentrate, crystallization, filterable multi-functional jar, its characterized in that includes multi-functional jar, presss from both sides cover 1, bottom valve 2, glass pipe 4, filter 5, storage tank, sight glass 7, eyepiece 10, advances pipe, heat exchanger 11, recovery tank 12 and dropwise add device, multi-functional jar inside lining has press from both sides cover 1, it is connected with steam business turn over pipeline and cooling water business turn over pipeline respectively through the valve to press from both sides cover 1, multi-functional jar bottom is connected with bottom valve 2, bottom valve 2 is connected with glass pipe 4 through cutting ferrule connecting piece 3, glass pipe 4 bottom is connected with the valve, the valve bottom is connected with one of three-way pipe way, the two-way of three-way pipe has filter 5 through the pipe connection, filter 5 is connected with first storage tank 6, the three-way connection has the pipeline that is equipped with the valve, multi-functional, inside is equipped with the stirring rake 9 that is connected with agitator motor 8, agitator motor 8 has frequency conversion device, multi-functional jar top is equipped with eyepiece 10 and two and advances the pipe, and one advances to manage for the liquid inlet pipe, and another advances union coupling has heat exchanger 11, the liquid inlet pipe is connected with feed liquid import and nitrogen gas respectively, 11 below exit linkage of heat exchanger have recovery tank 12, recovery tank 12 is connected with vacuum unit 13, the dropwise add device is installed to multi-functional jar top, the dropwise add device is including flowmeter 14, valve and the second storage tank 15 that connects gradually.
Specifically, a valve is arranged on a pipeline between the two-way of the three-way pipeline and the filter 5, a valve is arranged between the filter 5 and the first storage tank 6, a valve is arranged between the inlet pipe and the heat exchanger 11, a valve is arranged between the liquid feed pipe and the feed liquid inlet, and a valve is arranged between the recovery tank 12 and the vacuum unit 13.
The working principle is as follows: the utility model discloses a multi-functional jar has increased one set of liquid and concentrated system on the basis of extraction jar, has mainly increased one in the multi-functional jar and has pressed from both sides cover 1, connects steam and frozen water for concentrated extract. A cutting sleeve connecting piece 3 is used for connecting a glass tube 4 below the bottom valve 2, and a valve is arranged below the glass tube 4 and used for controlling the flow rate of liquid separation; and a tee joint below the valve is connected with the filter 5 and the first storage tank 6 and is used for collecting the crystallized product. The upper inlet pipe is connected with a plate heat exchanger 11 to recover the solvent.
The bottom valve 2 is closed before extraction, and the bottom valve 2 is opened after extraction is finished. After the material liquid is observed to be layered through the two side sight glasses 7, a valve below the glass tube 4 is controlled, and the lower-layer material is discharged. And after the material liquid separation operation is finished, opening a steam valve for concentration, and recovering the solvent by using the first storage tank 6. After the solution is concentrated, acid, alkali or other substances are dropped through a dropping device to crystallize, and finally, the crystallized product is collected through a filter 5 below.
The basic principles and the main features of the invention and the advantages of the invention have been shown and described above. It will be understood by those skilled in the art that the present invention is not limited to the above embodiments, and that the foregoing embodiments and descriptions are provided only to illustrate the principles of the present invention without departing from the spirit and scope of the present invention. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (6)
1. A multifunctional tank capable of performing extraction, liquid separation, concentration, crystallization and filtration is characterized by comprising a multifunctional tank, a jacket, a bottom valve, a glass tube, a filter, a storage tank, a sight glass, an ocular, a feed tube, a heat exchanger, a recovery tank and a dripping device, wherein the jacket is lined in the multifunctional tank, the jacket is respectively connected with a steam inlet and outlet pipeline and a cooling water inlet and outlet pipeline through valves, the bottom of the multifunctional tank is connected with the bottom valve, the bottom valve is connected with the glass tube through a sleeve connecting piece, the bottom of the glass tube is connected with the valve, the bottom of the valve is connected with a through of a three-way pipeline, the through of the three-way pipeline is connected with the filter through a pipeline, the filter is connected with a first storage tank, the three-way pipeline is connected with a pipeline provided with a valve, both side walls of the multifunctional, stirring motor has frequency conversion device, multi-functional jar top is equipped with eyepiece and two and advances the pipe, advances to manage for liquid inlet pipe, and another advances union coupling has the heat exchanger, the liquid inlet pipe is connected with feed liquid import and nitrogen gas respectively, heat exchanger below exit linkage has the recovery jar, the recovery jar is connected with the vacuum unit, dropwise add device is installed to multi-functional jar top, dropwise add device is including the flowmeter, valve and the second storage tank that connect gradually.
2. The multifunctional tank capable of performing extraction, liquid separation, concentration, crystallization and filtration according to claim 1, is characterized in that: and a valve is arranged on the pipeline between the two-way of the three-way pipeline and the filter.
3. The multifunctional tank capable of performing extraction, liquid separation, concentration, crystallization and filtration according to claim 1, is characterized in that: and a valve is arranged between the filter and the first storage tank.
4. The multifunctional tank capable of performing extraction, liquid separation, concentration, crystallization and filtration according to claim 1, is characterized in that: and a valve is arranged between the inlet pipe and the heat exchanger.
5. The multifunctional tank capable of performing extraction, liquid separation, concentration, crystallization and filtration according to claim 1, is characterized in that: and a valve is arranged between the liquid feeding pipe and the feed liquid inlet.
6. The multifunctional tank capable of performing extraction, liquid separation, concentration, crystallization and filtration according to claim 1, is characterized in that: and a valve is arranged between the recovery tank and the vacuum unit.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020869178.0U CN212594118U (en) | 2020-05-22 | 2020-05-22 | Multifunctional tank capable of extracting, separating, concentrating, crystallizing and filtering |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202020869178.0U CN212594118U (en) | 2020-05-22 | 2020-05-22 | Multifunctional tank capable of extracting, separating, concentrating, crystallizing and filtering |
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| Publication Number | Publication Date |
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| CN212594118U true CN212594118U (en) | 2021-02-26 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202020869178.0U Active CN212594118U (en) | 2020-05-22 | 2020-05-22 | Multifunctional tank capable of extracting, separating, concentrating, crystallizing and filtering |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113877242A (en) * | 2021-09-30 | 2022-01-04 | 河北化工医药职业技术学院 | Purification system for producing chiral drugs |
| CN114669093A (en) * | 2022-02-25 | 2022-06-28 | 安徽东至广信农化有限公司 | Material separation device for reduction synthesis of o-phenylenediamine |
-
2020
- 2020-05-22 CN CN202020869178.0U patent/CN212594118U/en active Active
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113877242A (en) * | 2021-09-30 | 2022-01-04 | 河北化工医药职业技术学院 | Purification system for producing chiral drugs |
| CN114669093A (en) * | 2022-02-25 | 2022-06-28 | 安徽东至广信农化有限公司 | Material separation device for reduction synthesis of o-phenylenediamine |
| CN114669093B (en) * | 2022-02-25 | 2023-11-07 | 安徽东至广信农化有限公司 | Material separation device for reduction synthesis of o-phenylenediamine |
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