CN212395945U - Extraction and separation device for biological pharmacy - Google Patents

Extraction and separation device for biological pharmacy Download PDF

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Publication number
CN212395945U
CN212395945U CN202020161829.0U CN202020161829U CN212395945U CN 212395945 U CN212395945 U CN 212395945U CN 202020161829 U CN202020161829 U CN 202020161829U CN 212395945 U CN212395945 U CN 212395945U
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China
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temperature steam
extraction
cavity
heat exchange
chamber
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Expired - Fee Related
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CN202020161829.0U
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Chinese (zh)
Inventor
张贤栋
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Sichuan Mass Spectrometry Biotechnology Co ltd
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Sichuan Mass Spectrometry Biotechnology Co ltd
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Abstract

The utility model discloses an extraction separation device for bio-pharmaceuticals, which belongs to the technical field of extraction separation devices, the solution to be extracted is put into a liquid inlet, the inner part of an extraction cavity is heated by starting an electric heating component, the generated high-temperature steam absorbs the high-temperature steam through a high-temperature steam absorption tube and is discharged through a high-temperature steam exhaust port, a high-temperature steam driving component is driven to rotate in the process that the high-temperature steam flows through a high-temperature steam flowing cavity, the stirring component is driven by the high-temperature steam driving component to stir the solution to be extracted, the extraction efficiency is further improved, the extraction solution is stirred by the high-temperature steam flowing without using a motor, thereby the energy is saved, the high-temperature steam is liquefied and radiated in a heat exchange cavity through a high-temperature steam cooling tube, and the heated heat exchange tube flows into an annular heat preservation tube to, and further recycles the heat energy of the high-temperature steam.

Description

Extraction and separation device for biological pharmacy
Technical Field
The utility model relates to an extraction separator especially relates to an extraction separator for bio-pharmaceuticals, belongs to extraction separator technical field.
Background
The principle of extractive separation (physical extraction) is to separate a liquid mixture by exploiting the difference in solubility of a solute in two immiscible liquid phases.
The principle of extractive separation (physical extraction) is to separate a liquid mixture by exploiting the difference in solubility of a solute in two immiscible liquid phases. However, for many physical extraction systems, particularly for some metals, the solvent extraction process is often accompanied by a chemical reaction, i.e., a chemical interaction between the solute and the extractant. This type of extractive mass transfer process with a chemical reaction is known as reactive extraction, also known as chemical extraction.
The extraction separator of bio-pharmaceuticals among the prior art often stirs the solution of improvement extraction efficiency in the reation kettle through driving motor drive stirring subassembly when separating the extraction, and consumes energy through driving motor comparison, and secondly the high temperature steam that produces need cool down the liquefaction, and its high temperature steam is but utilization that can not be fine, designs an extraction separator who is used for bio-pharmaceuticals for this and optimizes above-mentioned problem.
SUMMERY OF THE UTILITY MODEL
The main purpose of the utility model is to provide an extraction separation device for bio-pharmaceuticals, the solution to be extracted is put into the liquid inlet, the interior of the extraction cavity is heated by starting the electric heating component, the generated high-temperature steam absorbs the high-temperature steam through the high-temperature steam absorbing pipe and is discharged through the high-temperature steam exhaust port, the high-temperature steam driving component is driven to rotate in the process that the high-temperature steam flows through the high-temperature steam flowing cavity, the stirring component is driven by the high-temperature steam driving component to stir the solution to be extracted, the extraction efficiency is further improved, the stirring of the extraction solution is realized through the high-temperature steam flowing without using a motor, thereby the energy is saved, the high-temperature steam is liquefied and radiated in the heat exchange cavity through the high-temperature steam cooling pipe, the heated heat exchange pipe flows into the annular heat preservation pipe to preserve, and further recycles the heat energy of the high-temperature steam.
The purpose of the utility model can be achieved by adopting the following technical scheme:
an extraction and separation device for biological pharmacy comprises an extraction cavity and a heat insulation layer arranged outside the extraction cavity, the inner side of the heat-insulating layer is provided with an annular heat-insulating pipe, the inner side of the extraction cavity is provided with an electric heating assembly, the top of the extraction cavity is provided with a stirring assembly transmission cavity, and the inner side of the stirring component transmission cavity is provided with a high-temperature steam driving component, the high-temperature steam driving component is provided with a stirring component which penetrates to the inner side of the extraction cavity, the stirring component transmission cavity is connected with a heat exchange cavity, and the inner side of the heat exchange cavity is provided with a high-temperature steam cooling pipe, the inner wall of the heat exchange cavity is provided with a heat exchange pipe, and the heat exchange pipe is communicated with the annular heat preservation pipe through a second connecting hose, a drain valve is installed at the bottom outside the heat exchange cavity, and the drain valve is communicated with the bottom of the high-temperature steam cooling pipe.
Preferably, the electric heating assembly comprises an electric heater arranged on the outer side of the heat insulation layer, an electric heating plate is arranged on the inner wall of the extraction cavity, and the electric heater is electrically connected with the electric heating plate through a lead.
Preferably, the inner wall in extraction chamber the extraction intracavity wall is from top to bottom equidistantly installed the heat conduction pole, just the heat conduction pole is installed the one end of extraction intracavity wall with the electrical heating board towards one side intercommunication of extraction intracavity portion.
Preferably, the high-temperature steam driving assembly comprises a fan blade arranged on one side of the inner portion of the transmission cavity of the stirring assembly, a rotating rod is arranged at the middle position of one side of the fan blade, a second bevel gear is arranged at one end, far away from the fan blade, of the rotating rod, and a first bevel gear is meshed with the outer side of the second bevel gear.
Preferably, the stirring assembly comprises a stirring rod arranged at the bottom of the first bevel gear and penetrating through the inside of the extraction cavity, stirring blades are arranged on the outer side of the stirring rod along the axial direction of the stirring rod at equal intervals, and the stirring blades and the heat conducting rods are distributed in a staggered manner
Preferably, a high-temperature steam flowing cavity is formed in the outer side of the fan blade and located on one side of the inner portion of the stirring assembly transmission cavity, high-temperature steam exhaust ports are formed in the top and the bottom of the high-temperature steam flowing cavity, the high-temperature steam exhaust port located at the bottom of the high-temperature steam flowing cavity is communicated with the extraction cavity, and a first connecting hose is communicated with the top of the other high-temperature steam exhaust port.
Preferably, first coupling hose is kept away from the one end in high temperature steam flow chamber with heat exchange cavity intercommunication, heat exchange cavity is including installing the inside high temperature steam cooling pipe in heat exchange cavity, heat exchange cavity's inner wall is equipped with hot exchange pipe, first coupling hose with high temperature steam cooling pipe's top intercommunication, hot exchange pipe pass through second coupling hose with annular insulating tube intercommunication.
Preferably, the high-temperature steam cooling pipes are distributed in the heat exchange cavity in a spiral structure, and the heat exchange pipes are wound on the inner wall of the heat exchange cavity.
Preferably, the supporting legs are installed at four corners of the bottom of the extraction cavity, and the discharge port is installed at the middle position of the bottom of the supporting legs.
Preferably, the upper part of the interior of the extraction cavity is provided with a high-temperature steam absorption pipe, the high-temperature steam absorption pipe is communicated with the high-temperature steam exhaust port, and the top of the extraction cavity is communicated with a liquid inlet.
The utility model has the advantages of:
the utility model provides an extraction and separation device for biological pharmacy, which feeds solution to be extracted into a liquid inlet, the inside of the extraction cavity is heated by starting the electric heating component, the generated high-temperature steam absorbs the high-temperature steam through the high-temperature steam absorption pipe and is discharged through the high-temperature steam exhaust port, the high-temperature steam driving component is driven to rotate in the process that the high-temperature steam flows through the high-temperature steam flowing cavity, the high-temperature steam driving component drives the stirring component to stir the solution to be extracted, the extraction efficiency is further improved, the high-temperature steam flows to stir the extraction solution without using a motor, thereby it is more energy-conserving, high-temperature steam carries out the liquefaction heat dissipation in the heat exchange intracavity through high-temperature steam cooling pipe, and the hot exchange pipe that is heated flows into annular insulating tube and keeps warm to the extraction chamber, further recycles high-temperature steam's heat energy again.
Drawings
FIG. 1 is a side cross-sectional view of a preferred embodiment of an extraction separation apparatus for biopharmaceuticals in accordance with the present invention;
FIG. 2 is a schematic diagram of a steam drive and transmission assembly of a preferred embodiment of an extraction separation apparatus for biopharmaceuticals in accordance with the present invention;
FIG. 3 is an enlarged view of the structure at point A of a preferred embodiment of an extraction separation apparatus for biopharmaceuticals in accordance with the present invention;
fig. 4 is a schematic view of a heat exchange module according to a preferred embodiment of an extraction separation apparatus for biopharmaceuticals in accordance with the present invention.
In the figure: 1-a first connecting hose, 2-an extraction cavity, 3-a liquid inlet, 4-a heat preservation layer, 5-a ring-shaped heat preservation pipe, 6-an electric heating plate, 7-a heat conduction rod, 8-a stirring blade, 9-a stirring rod, 10-a supporting leg, 11-a heat exchange cavity, 12-an electric heater, 13-a stirring assembly transmission cavity, 14-a high-temperature steam flowing cavity, 15-a high-temperature steam cooling pipe, 16-a liquid discharge valve, 17-a heat exchange pipe, 18-a second connecting hose, 19-a fan blade, 20-a high-temperature steam exhaust port, 21-a high-temperature steam absorption pipe, 22-a rotating rod, 23-a first bevel gear and 24-a second bevel gear.
Detailed Description
In order to make the technical solutions of the present invention clearer and clearer for those skilled in the art, the present invention will be described in further detail with reference to the following embodiments and the accompanying drawings, but the embodiments of the present invention are not limited thereto.
As shown in fig. 1-4, the extraction and separation device for bio-pharmaceuticals provided in this embodiment includes an extraction cavity 2 and a heat insulation layer 4 installed outside the extraction cavity 2, an annular heat insulation pipe 5 is installed inside the heat insulation layer 4, an electric heating assembly is installed inside the extraction cavity 2, a stirring assembly transmission cavity 13 is installed at the top of the extraction cavity 2, and the inner side of the stirring component transmission cavity 13 is provided with a high-temperature steam driving component, the high-temperature steam driving component is provided with a stirring component which penetrates to the inner side of the extraction cavity 2, the stirring component transmission cavity 13 is connected with a heat exchange cavity 11, and the inner side of the heat exchange cavity 11 is provided with a high-temperature steam cooling pipe 15, the inner wall of the heat exchange cavity 11 is provided with a heat exchange pipe 17, and the heat exchange tube 17 is communicated with the annular heat preservation tube 5 through a second connecting hose 18, a liquid discharge valve 16 is installed at the bottom outside the heat exchange cavity 11, and the liquid discharge valve 16 is communicated with the bottom of the high-temperature steam cooling tube 15.
Drop into the solution that needs the extraction to inlet 3, heat extraction chamber 2 inside through starting electrical heating element, the high-temperature steam that produces absorbs high-temperature steam through high-temperature steam absorption tube 21, discharge through high-temperature steam gas vent 20, in-process that high-temperature steam flows chamber 14 through high-temperature steam drives the rotation of high-temperature steam drive assembly, it stirs the solution that needs the extraction to drive the stirring subassembly through high-temperature steam drive assembly, further improve extraction efficiency, and it need not to use the motor to stir extraction solution through high-temperature steam flow realization, thereby it is more energy-conserving, high-temperature steam carries out liquefaction heat dissipation in heat exchange chamber 11 through high-temperature steam cooling tube 15, the hot heat exchange pipe 17 that is heated flows into annular insulating tube 5 and keeps warm extraction chamber 2, further recycle high-temperature steam's heat energy again.
In this embodiment, the electric heating assembly comprises an electric heater 12 installed outside the heat insulating layer 4, the electric heating plate 6 is installed on the inner wall of the extraction chamber 2, and the electric heater 12 is electrically connected with the electric heating plate 6 through a conducting wire.
Heating of the extraction chamber 2 is achieved by activating the electric heater 12 and activating the electric heating plate 6 by means of the electric heater 12.
In this embodiment, the inner wall of the extraction chamber 2 of the inner wall of the extraction chamber 2 is provided with the heat conducting rods 7 at equal intervals from top to bottom, and the heat conducting rods 7 are arranged at one end of the inner wall of the extraction chamber 2 and communicated with one side of the electric heating plate 6 facing the inside of the extraction chamber 2.
Through the further realization heat-conduction of heat-conducting rod 7, improve heat-conduction efficiency, make the solution heating in its extraction chamber 2 more swift.
In the embodiment, the high-temperature steam driving assembly comprises a fan blade 19 installed on one side inside the transmission cavity 13 of the stirring assembly, a rotating rod 22 is installed at the middle position of one side of the fan blade 19, a second bevel gear 24 is installed at one end of the rotating rod 22 far away from the fan blade 19, and a first bevel gear 23 is meshed with the outer side of the second bevel gear 24.
The high-temperature steam drives the fan blades 19 to rotate, the rotating rods 22 are driven to rotate through the fan blades 19, the rotating rods 22 drive the second bevel gears 24 to rotate, the first bevel gears 23 are driven to rotate through the second bevel gears 24, and the stirring assemblies are driven to rotate through the first bevel gears 23.
In this embodiment, the stirring assembly includes the stirring rod 9 installed at the bottom of the first bevel gear 23 and penetrating through the inside of the extraction chamber 2, the stirring blades 8 are installed at equal intervals on the outer side of the stirring rod 9 along the axial direction of the stirring rod 9, and the stirring blades 8 and the heat conducting rods 7 are distributed in a staggered manner.
Drive puddler 9 through first bevel gear 23 and rotate, drive stirring leaf 8 through puddler 9 and rotate to solution that needs the extraction in the extraction chamber 2 stirs, stirring leaf 8 further improves stirring and heating efficiency with heat conduction pole 7 crisscross distribution simultaneously.
In this embodiment, the outside of the fan blade 19 and the inside one side of the stirring assembly transmission cavity 13 are provided with a high temperature steam flowing cavity 14, the top and the bottom of the high temperature steam flowing cavity 14 are both provided with high temperature steam exhaust ports 20, the high temperature steam exhaust ports 20 at the bottom of the high temperature steam flowing cavity 14 are communicated with the extraction cavity 2, and the top of the other group of high temperature steam exhaust ports 20 is communicated with the first connecting hose 1.
In the embodiment, one end of the first connecting hose 1, which is far away from the high-temperature steam flowing cavity 14, is communicated with the heat exchange cavity 11, the heat exchange cavity 11 comprises a high-temperature steam cooling pipe 15 which is installed inside the heat exchange cavity 11, a heat exchange pipe 17 is arranged on the inner wall of the heat exchange cavity 11, the first connecting hose 1 is communicated with the top of the high-temperature steam cooling pipe 15, and the heat exchange pipe 17 is communicated with the annular heat preservation pipe 5 through a second connecting hose 18.
In the present embodiment, the high temperature desuperheating pipes 15 are distributed in a spiral structure inside the heat exchange chamber 11, and the heat exchange pipes 17 are wound around the inner wall of the heat exchange chamber 11.
In this embodiment, the supporting legs 10 are installed at the four corners of the bottom of the extraction chamber 2, and the discharge port is installed at the middle position of the bottom of the supporting legs 10.
In this embodiment, the high temperature steam absorption pipe 21 is disposed above the interior of the extraction chamber 2, the high temperature steam absorption pipe 21 is communicated with the high temperature steam exhaust port 20, and the top of the extraction chamber 2 is communicated with the liquid inlet 3.
The above description is only a further embodiment of the present invention, but the scope of protection of the present invention is not limited thereto, and any person skilled in the art can replace or change the technical solution and the concept of the present invention within the scope of the present invention.

Claims (10)

1. An extraction and separation device for biological pharmacy is characterized in that: comprises an extraction cavity (2) and a heat preservation layer (4) arranged outside the extraction cavity (2), wherein the inner side of the heat preservation layer (4) is provided with an annular heat preservation pipe (5), the inner side of the extraction cavity (2) is provided with an electric heating component, a stirring component transmission cavity (13) is arranged at the top of the extraction cavity (2), the inner side of the stirring component transmission cavity (13) is provided with a high-temperature steam driving component, the high-temperature steam driving component is provided with a stirring component which runs through the inner side of the extraction cavity (2), the stirring component transmission cavity (13) is connected with a heat exchange cavity (11), the inner side of the heat exchange cavity (11) is provided with a high-temperature steam cooling pipe (15), the inner wall of the heat exchange cavity (11) is provided with a heat exchange pipe (17), and the heat exchange pipe (17) is communicated with the annular heat preservation pipe (5) through a second connecting, and a liquid discharge valve (16) is installed at the bottom outside the heat exchange cavity (11), and the liquid discharge valve (16) is communicated with the bottom of the high-temperature steam cooling pipe (15).
2. The extractive separation apparatus for biopharmaceuticals of claim 1, wherein: the electric heating assembly comprises an electric heater (12) arranged on the outer side of the heat preservation layer (4), an electric heating plate (6) is arranged on the inner wall of the extraction cavity (2), and the electric heater (12) is electrically connected with the electric heating plate (6) through a wire.
3. The extractive separation apparatus for biopharmaceuticals of claim 2, wherein: the inner wall of extraction chamber (2) inner wall from top to bottom is equidistant installs heat conduction rod (7), just heat conduction rod (7) are installed the one end of extraction chamber (2) inner wall with electric heating plate (6) towards extract the inside one side intercommunication in chamber (2).
4. An extractive separation apparatus for biopharmaceuticals as claimed in claim 3, wherein: high temperature steam drive assembly is including installing fan leaf (19) of stirring subassembly transmission chamber (13) inside one side, just intermediate position department on one side of fan leaf (19) installs bull stick (22), bull stick (22) are kept away from the one end of fan leaf (19) is installed second bevel gear (24), the outside meshing of second bevel gear (24) has first bevel gear (23).
5. The extraction separation apparatus for biopharmaceuticals of claim 4, wherein said extraction separation apparatus comprises: the stirring assembly comprises a stirring rod (9) which is arranged at the bottom of the first bevel gear (23) and penetrates through the interior of the extraction cavity (2), stirring blades (8) are arranged on the outer side of the stirring rod (9) along the axial direction of the stirring rod (9) at equal intervals, and the stirring blades (8) and the heat conducting rods (7) are distributed in a staggered mode.
6. The extraction separation apparatus for biopharmaceuticals of claim 4, wherein said extraction separation apparatus comprises: the outside of fan leaf (19) just is located the inside one side of stirring subassembly transmission chamber (13) is equipped with high temperature steam and flows chamber (14), high temperature steam gas vent (20) have all been seted up to the top and the bottom in high temperature steam flow chamber (14), and are located high temperature steam gas vent (20) of high temperature steam flow chamber (14) bottom department with extract chamber (2) intercommunication, another group the top intercommunication of high temperature steam gas vent (20) has first connecting hose (1).
7. The extractive separation apparatus for biopharmaceuticals of claim 6, wherein: keep away from first coupling hose (1) the one end of high temperature steam flow chamber (14) with heat exchange chamber (11) intercommunication, heat exchange chamber (11) are including installing inside high temperature steam cooling pipe (15) of heat exchange chamber (11), first coupling hose (1) with the top intercommunication of high temperature steam cooling pipe (15), hot exchange pipe (17) through second coupling hose (18) with annular insulating tube (5) intercommunication.
8. The extractive separation apparatus for biopharmaceuticals of claim 7, wherein: the high-temperature steam cooling pipe (15) is distributed in the heat exchange cavity (11) in a spiral structure, and the heat exchange pipe (17) is wound on the inner wall of the heat exchange cavity (11).
9. The extractive separation apparatus for biopharmaceuticals of claim 1, wherein: the four corners department of extraction chamber (2) bottom installs supporting leg (10), just the intermediate position department of supporting leg (10) bottom installs the discharge gate.
10. The extractive separation apparatus for biopharmaceuticals of claim 6, wherein: the inside top in extraction chamber (2) is equipped with high temperature steam absorption pipe (21), just high temperature steam absorption pipe (21) with high temperature steam gas vent (20) intercommunication, the top intercommunication in extraction chamber (2) has liquid inlet (3).
CN202020161829.0U 2020-02-11 2020-02-11 Extraction and separation device for biological pharmacy Expired - Fee Related CN212395945U (en)

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Application Number Priority Date Filing Date Title
CN202020161829.0U CN212395945U (en) 2020-02-11 2020-02-11 Extraction and separation device for biological pharmacy

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Application Number Priority Date Filing Date Title
CN202020161829.0U CN212395945U (en) 2020-02-11 2020-02-11 Extraction and separation device for biological pharmacy

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CN212395945U true CN212395945U (en) 2021-01-26

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114570052A (en) * 2022-03-04 2022-06-03 德州绿霸精细化工有限公司 Method and device for continuously producing diethyl maleate
CN114632491A (en) * 2022-02-18 2022-06-17 江苏恒德力化工设备制造有限公司 Enamel reaction kettle convenient to use

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114632491A (en) * 2022-02-18 2022-06-17 江苏恒德力化工设备制造有限公司 Enamel reaction kettle convenient to use
CN114570052A (en) * 2022-03-04 2022-06-03 德州绿霸精细化工有限公司 Method and device for continuously producing diethyl maleate

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Granted publication date: 20210126

Termination date: 20220211