CN211741323U - Environment-friendly insoluble substance measuring device - Google Patents
Environment-friendly insoluble substance measuring device Download PDFInfo
- Publication number
- CN211741323U CN211741323U CN201922440159.6U CN201922440159U CN211741323U CN 211741323 U CN211741323 U CN 211741323U CN 201922440159 U CN201922440159 U CN 201922440159U CN 211741323 U CN211741323 U CN 211741323U
- Authority
- CN
- China
- Prior art keywords
- reagent
- extraction
- pipeline
- recovery
- condenser
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Landscapes
- Sampling And Sample Adjustment (AREA)
Abstract
The utility model discloses an environment-friendly insoluble substance measuring device, which comprises a reagent supply system, a reagent recovery system, an extraction system and an automatic monitoring system; the reagent supply system supplies a reagent to the extraction system through a pipeline; the extraction system is used for extracting the substance with the determination, and the reagent recovery system is connected with the extraction system and is used for recovering the reagent used by the extraction system; the control system of the automatic control system is in signal connection with the reagent supply system, the reagent recovery system and the extraction system. Finally, the environment and the health of operating personnel are protected, the reagent consumption and the waste liquid output are reduced, and the test precision is improved. Through a large amount of experimental contrasts, the reagent consumption of each test can be reduced by 90%, the detection cost of enterprises and the toxic reagent waste liquid treatment cost of test output are reduced, the automatic test mode ensures that the whole course of the test of the testing personnel is not directly contacted with the toxic reagent, and the occupational health hidden danger and the artificial detection error of the testing personnel are avoided.
Description
Technical Field
The utility model relates to a chemistry detects technical field, especially relates to an insoluble substance of environment-friendly survey device.
Background
In industries such as petroleum, asphalt, coal tar and the like, the content or components of a plurality of specific insoluble substances need to be repeatedly extracted and measured or obtained by using corresponding reagents. Part of test reagents are inhaled or contacted to cause great harm to human bodies, such as measurement of toluene insoluble substances; in particular, the binder pitch for carbon electrodes is important and must be measured in large quantities.
Toluene (easy to control poison-3), the precancerous substance list published by the international cancer research institution of the world health organization, and toluene is in the category 3 carcinogenic substance list. At the present stage, the traditional manual equipment is still used for measuring the toluene insoluble substance, the contact of operators with the reagent is frequent, and the physical damage is large; the reagent cannot be reused after being used once, so that a large amount of toxic waste liquid is formed, and the capital investment is increased; most laboratories have no relative quality and capability to treat waste liquid, so a large amount of non-tissue discharge is generated, and the environment is greatly damaged.
With the continuous increase of the use of asphalt, coal tar and the like in various industries, the materials are also required to be stricter, and the detection frequency is greatly increased. At present, no corresponding full-flow monitoring and measuring device exists in the industry, a using unit still uses traditional manual equipment, the health damage of operating personnel is large, the reagent consumption is large, the reagent management is disordered, and the environmental pollution is serious due to non-organized emission, so that an environment-friendly insoluble substance content measuring device is urgently needed.
SUMMERY OF THE UTILITY MODEL
The utility model discloses to the problem that prior art exists, provide an intelligent degree height, but insoluble substance survey device of recovered used reagent.
The utility model adopts the following technical proposal:
an environment-friendly insoluble substance measuring apparatus, characterized in that the insoluble substance measuring apparatus comprises: a reagent supply system, a reagent recovery system, an extraction system and an automatic monitoring system (21); the reagent supply system supplies a reagent to the extraction system through a pipeline; the extraction system is used for repeatedly siphoning, extracting and dissolving a sample and extracting insoluble substances, and the reagent recovery system is connected with the extraction system and is used for recovering a reagent used by the extraction system; the control system of the automatic control system is in signal connection with the reagent supply system, the reagent recovery system and the extraction system.
According to the above-mentioned environment-friendly insoluble matter measurement apparatus, the reagent supply system includes: a reagent bottle (20) and a liquid delivery pump (18); one side of the liquid delivery pump is connected with a reagent pumping and discharging pipeline (19), the reagent pumping and discharging pipeline (19) extends into the reagent bottle (20), the other side of the liquid delivery pump is connected with a reagent delivery pipeline, the reagent delivery pipeline enters the extraction system, and a first electromagnetic valve (17) is installed on the reagent delivery pipeline.
According to the above-mentioned environment-friendly insoluble substance measuring apparatus, the reagent recovery system comprises, in order from the top: a first lifting device (14), a first condenser (11), a recovery pot (12) and a first heater (13); the first lifting device (14) is used for lifting the first condenser (11); a circle of grooves are formed in the lower portion inside the first condenser (11), the reagent conveying pipeline is connected into the grooves through a reagent recovery pipeline, and a second electromagnetic valve (16) is installed on the reagent recovery pipeline; a vacuum pump (15) and a vent pipe are installed on the first condenser (11), and a third electromagnetic valve (10) is installed on the vent pipe.
According to above-mentioned environment-friendly insoluble substance survey device, characterized in that, extraction system includes from the top down in proper order: the device comprises a second lifting device (1), a rotary power device (2), a second condenser (3), an extraction cylinder (5), a heating pot (7) and a second heater (6); the second lifting device (1) is used for lifting the rotary power device (2) and the second condenser (3); a rotating rod is connected below the rotary power device (2); a filter cartridge (4) is placed in the extraction cartridge (5), a siphon pipe and a steam return pipe are arranged on the side wall of the extraction cartridge (5), one end of the siphon pipe is connected to the side wall of the extraction cartridge (5) and at the same height as the bottom of the filter cartridge (4), the other end of the siphon pipe extends into the upper part of the heating pot (7), and the steam return pipe is arranged on the side wall of the extraction cartridge (5) and is communicated with the upper part and the lower part of the extraction cartridge (5); the reagent conveying pipeline is connected into the extraction cylinder (5); the bottom of the heating pot (7) is connected to the interior of the recovery pot (12) through a reagent cooling recovery pipeline, and a fourth electromagnetic valve (8) and a third condenser (9) are installed on the reagent cooling recovery pipeline.
The apparatus for measuring an insoluble matter in an environment-friendly manner as described above is characterized in that the stirring blade is connected to the end of the rotating lever.
The utility model has the advantages that: the utility model relates to an environment-friendly insoluble substance measuring device. The device solves the defects of the traditional insoluble substance measuring device in the industry, finally realizes the protection of the environment and the health of operating personnel, reduces the reagent consumption and the waste liquid output, and improves the test precision. Through a large amount of experimental contrasts, the reagent consumption of each test can be reduced by 90%, the detection cost of enterprises and the toxic reagent waste liquid treatment cost of test output are greatly reduced, the automatic test mode ensures that the whole course of the test of the testing personnel is not directly contacted with the toxic reagent, and the occupational health hidden danger and the artificial detection error of the testing personnel are avoided.
Drawings
Fig. 1 is a schematic structural diagram of the present invention.
Detailed Description
Referring to fig. 1, the utility model discloses an insoluble material determination device of environment-friendly includes: the system comprises a reagent supply system, a reagent recovery system, an extraction system and an automatic control system; the reagent supply system supplies reagent to the extraction system through a pipeline; the extraction system is used for repeatedly siphoning, extracting and dissolving the sample and extracting insoluble substances, and the reagent recovery system is connected with the extraction system and is used for recovering the reagent used by the extraction system; the control system of the automatic control system is connected with the reagent supply system, the reagent recovery system and the extraction system through signals and controls the systems to work cooperatively.
In a preferred aspect, the reagent supply system comprises: a reagent bottle 20, a liquid transfer pump 18; one side of the liquid delivery pump is connected with a reagent pumping and discharging pipeline 19, the reagent pumping and discharging pipeline 19 extends into a reagent bottle 20, the other side of the liquid delivery pump 18 is connected with a reagent delivery pipeline, the reagent delivery pipeline enters the extraction system, and a first electromagnetic valve 17 is installed on the reagent delivery pipeline. Reagent recovery system includes from the top down in proper order: a first lifting device 14, a first condenser 11, a recovery boiler 12 and a first heater 13; the first lifting device 14 is used for lifting the first condenser 11; a circle of grooves are formed in the lower portion inside the first condenser 11, the reagent conveying pipeline is connected into the grooves through a reagent recovery pipeline, and a second electromagnetic valve 16 is installed on the reagent recovery pipeline; a vacuum pump 15 and a vent pipe are attached to the first condenser 11, and a third electromagnetic valve 10 is attached to the vent pipe. The extraction system includes from top to bottom in proper order: the device comprises a second lifting device 1, a rotary power device 2, a second condenser 3, an extraction cylinder 5, a heating pot 7 and a second heater 6; the second lifting device 1 is used for lifting the rotary power device 2 and the second condenser 3; a rotating rod is connected below the rotary power device 2; a filter cartridge 4 is placed in the extraction cylinder 5, a siphon pipe and a steam return pipe are arranged on the side wall of the extraction cylinder 5, one end of the siphon pipe is connected to the side wall of the extraction cylinder 5 at a position which is equal to the bottom of the filter cartridge 4 in height, the other end of the siphon pipe extends into the upper part of the heating pot 7, and the steam return pipe is arranged on the side wall of the extraction cylinder 5 and is communicated with the upper part and the lower part of the extraction; the reagent conveying pipeline is connected into the extraction cylinder 5; the bottom of the heating pan 7 is connected to the interior of a recovery pan 12 through a reagent cooling recovery line on which a fourth electromagnetic valve 8 and a third condenser 9 are installed. In the case of stirring, the stirring blade is connected to the end of the rotating rod.
After the device is powered on, all the mechanisms start to work in coordination. The automatic measurement and control system detects the station state and confirms that each system is in a normal standby station; starting; the automatic measurement and control system detects the station state and confirms that each system is in a normal standby station; starting; the automatic measurement and control system outputs a command according to the selected test type; the second lifting device 1 acts to drive the rotary power device 2 and the second condenser 3 to ascend in a combined manner; an operator manually puts the filter cartridge 4 containing the sample into the extraction cartridge 5; the second lifting device 1 acts to drive the rotary power device 2 and the second condenser 3 to descend in a combined manner; the liquid delivery pump 18 and the first electromagnetic valve 17 act to deliver the reagent in the reagent bottle 20 into the extraction cylinder 5; the rotary power device 2 works according to a set program to stir the materials in the filter cylinder 4; the second heater 6 works to heat the reagent; the reagent steam rises; the second condenser 3 works, the liquid flows into the filter cylinder 4 after being condensed, and when the liquid reaches the siphon height, the extraction cylinder 5 forms siphon; carrying out reciprocating circulation, and dissolving by equipment according to set time or extraction times; the fourth electromagnetic valve 8 and the vacuum pump 15 work to pump the used reagent in the extraction cylinder 5 and the heating pot 7 into the recovery pot 12, and the fourth electromagnetic valve 8 and the vacuum pump 15 are closed; the third electromagnetic valve 10 works; the second heater 6 stops working, the program gives an alarm, and the equipment prompts sampling; taking out the filter cartridge 4, putting the filter cartridge into an oven, drying and cooling the filter cartridge to room temperature, weighing the mass and inputting the mass into an automatic measurement and control system; meanwhile, the first heater 13 works to heat the used reagent in the evaporation recovery pot 12, steam enters the first condenser 11, and the steam is condensed and flows into a groove below; the second electromagnetic valve 16 and the liquid delivery pump 18 work in reverse, and deliver the recovered reagent in the groove back to the reagent bottle 20; and the automatic measurement and control system calculates, counts and analyzes the acquired data and outputs a result.
The above only is the embodiment of the present invention, not limiting the scope of the present invention, all the equivalent structure changes made in the specification and the attached drawings or directly or indirectly applied to other related technical fields are all included in the patent protection scope of the present invention.
Claims (5)
1. An environment-friendly insoluble substance measuring apparatus, characterized in that the insoluble substance measuring apparatus comprises: the system comprises a reagent supply system, a reagent recovery system, an extraction system and an automatic control system; the reagent supply system supplies a reagent to the extraction system through a pipeline; the extraction system is used for repeatedly siphoning, extracting and dissolving a sample and extracting insoluble substances, and the reagent recovery system is connected with the extraction system and is used for recovering a reagent used by the extraction system; the control system of the automatic control system is in signal connection with the reagent supply system, the reagent recovery system and the extraction system.
2. The environmentally friendly insolubles determination apparatus of claim 1, wherein the reagent supply system comprises: a reagent bottle (20) and a liquid delivery pump (18); one side of the liquid delivery pump is connected with a reagent pumping and discharging pipeline (19), the reagent pumping and discharging pipeline (19) extends into the reagent bottle (20), the other side of the liquid delivery pump is connected with a reagent delivery pipeline, the reagent delivery pipeline enters the extraction system, and a first electromagnetic valve (17) is installed on the reagent delivery pipeline.
3. The apparatus for measuring insolubles in an environment-friendly manner according to claim 2, wherein the reagent recovery system comprises, in order from top to bottom: a first lifting device (14), a first condenser (11), a recovery pot (12) and a first heater (13); the first lifting device (14) is used for lifting the first condenser (11); a circle of grooves are formed in the lower portion inside the first condenser (11), the reagent conveying pipeline is connected into the grooves through a reagent recovery pipeline, and a second electromagnetic valve (16) is installed on the reagent recovery pipeline; a vacuum pump (15) and a vent pipe are installed on the first condenser (11), and a third electromagnetic valve (10) is installed on the vent pipe.
4. The apparatus for determining insolubles in an environmentally friendly manner as set forth in claim 3, wherein the extraction system comprises, in order from top to bottom: the device comprises a second lifting device (1), a rotary power device (2), a second condenser (3), an extraction cylinder (5), a heating pot (7) and a second heater (6); the second lifting device (1) is used for lifting the rotary power device (2) and the second condenser (3); a rotating rod is connected below the rotary power device (2); a filter cartridge (4) is placed in the extraction cartridge (5), a siphon pipe and a steam return pipe are arranged on the side wall of the extraction cartridge (5), one end of the siphon pipe is connected to the side wall of the extraction cartridge (5) and at the same height as the bottom of the filter cartridge (4), the other end of the siphon pipe extends into the upper part of the heating pot (7), and the steam return pipe is arranged on the side wall of the extraction cartridge (5) and is communicated with the upper part and the lower part of the extraction cartridge (5); the reagent conveying pipeline is connected into the extraction cylinder (5); the bottom of the heating pot (7) is connected to the interior of the recovery pot (12) through a reagent cooling recovery pipeline, and a fourth electromagnetic valve (8) and a third condenser (9) are installed on the reagent cooling recovery pipeline.
5. The apparatus for measuring insolubles in accordance with claim 4, wherein the rotating rod has a distal end connected to a stirring blade.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201922440159.6U CN211741323U (en) | 2019-12-30 | 2019-12-30 | Environment-friendly insoluble substance measuring device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201922440159.6U CN211741323U (en) | 2019-12-30 | 2019-12-30 | Environment-friendly insoluble substance measuring device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN211741323U true CN211741323U (en) | 2020-10-23 |
Family
ID=72871978
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201922440159.6U Active CN211741323U (en) | 2019-12-30 | 2019-12-30 | Environment-friendly insoluble substance measuring device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN211741323U (en) |
-
2019
- 2019-12-30 CN CN201922440159.6U patent/CN211741323U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN205270331U (en) | But real -time detection soil prosthetic devices | |
| CN202305455U (en) | Automatic acid rain monitor | |
| CN206847994U (en) | A kind of sampler suitable for analysis meter | |
| CN106872232A (en) | Full-automatic microwave device | |
| CN211741323U (en) | Environment-friendly insoluble substance measuring device | |
| CN211905273U (en) | Insoluble substance measuring device | |
| CN209640139U (en) | A kind of unattended environment-friendly type insolubles content measurement device | |
| CN112284963A (en) | Full-automatic textile fiber dissolution tester | |
| CN111272532B (en) | Full-automatic digestion acid-removing instrument | |
| CN109540730A (en) | A kind of unattended environment-friendly type insolubles content measurement device and method | |
| CN206584241U (en) | Strength of fluid On-line Control device | |
| CN202305305U (en) | Timely chlorine ion concentration dilution preprocessing device | |
| CN206463849U (en) | A kind of vacuum stirring equipment of remote monitoring | |
| CN107777765A (en) | In nuclear power station acidic and alkaline waste water and discharge method and system | |
| CN211602909U (en) | Online analyzer capable of measuring chemical oxygen demand in water | |
| CN104007279B (en) | The pressure-off formula charging of automatic sampler moves material discharge system | |
| CN207779753U (en) | Petroleum liquid sample Autosampler | |
| CN206638549U (en) | One kind automatically determines coal density system | |
| CN112557627B (en) | Rapid sampling and detecting system and method for soil barrier factors of urban relocation land | |
| CN206906403U (en) | A kind of reagent switching device for biology sensor | |
| CN114858881B (en) | Water-soluble acid-base test system | |
| CN209117425U (en) | A kind of sampler of barreled industrial chemicals | |
| CN112305153B (en) | Automatic analysis detector for bentonite content and detection method thereof | |
| CN211988701U (en) | Intelligent liquid adding robot for inspection and detection | |
| CN109856365A (en) | A kind of portable residual detection device of multifunctional agriculture planting soil agriculture |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant |