CN112284963A - Full-automatic textile fiber dissolution tester - Google Patents
Full-automatic textile fiber dissolution tester Download PDFInfo
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- CN112284963A CN112284963A CN202011334072.1A CN202011334072A CN112284963A CN 112284963 A CN112284963 A CN 112284963A CN 202011334072 A CN202011334072 A CN 202011334072A CN 112284963 A CN112284963 A CN 112284963A
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- water bath
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- dissolving
- pump
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N5/00—Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid
- G01N5/04—Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by removing a component, e.g. by evaporation, and weighing the remainder
Abstract
The invention discloses a full-automatic textile fiber dissolution tester, which comprises: tester main part, dissolving device, stirring dewatering device, advance flowing back system and control system, dissolving device includes: water bath, dissolving tank, heating pipe, turning block and specimen jar are provided with a plurality of stirring pieces on the turning block, are provided with a plurality of meshes on the specimen jar, and stirring dewatering device includes: the water bath tank comprises a motor arranged below the water bath tank, a first magnetic block connected with an output shaft of the motor, and a second magnetic block arranged on the rotating block. According to the invention, through the action of the magnetic field between the first magnetic block and the second magnetic block of the stirring dehydration device, non-contact stirring is realized, and simultaneously, water bath heating can be carried out through the water bath tank to reach the dissolution temperature specified by the standard method.
Description
Technical Field
The invention relates to the technical field of detection equipment, in particular to a full-automatic textile fiber dissolution tester.
Background
The textile fiber components and content are important indexes related to the performance, cost and product care of textiles, clothes and home textiles. At present, the identification of the fiber content is incorporated into the mandatory standard in many countries, and becomes one of the contents that all the clothes and home textiles need to disclose the identification to consumers when being sold. The content authenticity of the fiber components and the content is also one of the items of various market supervision and inspection, and is the item with higher unqualified incidence in the supervision and spot inspection of various textiles.
The premise of accurately marking the fiber components and the content is the accurate measurement of the fiber components and the content, and therefore, production enterprises, detection mechanisms and national supervision centers in the textile industry need to consume a large amount of manpower and material resources to analyze the fiber components and the content. Among the most used methods, chemical dissolution quantitative analysis is used. The chemical dissolving quantitative analysis method is that a plurality of small samples are cut from the textile, the small samples are dried and weighed, then the small samples are put into different reagents, such as sulfuric acid, sodium hydroxide solution and the like, so that the small samples are dissolved, the small sample residues are filtered and dried, and the residual weight of the dissolved small samples is weighed. When the solution reagent is selected, the solution in which only one of the components is dissolved is selected as a detection reagent by contrasting the component table of the textile, and the proportion of the component can be obtained by comparing the original dry weight of the small sample with the dry weight of the residue after dissolution.
However, the operation of the conventional chemical dissolution quantitative analysis method requires manual work in the whole process, and the dissolution efficiency is low, so that the conical flask containing the reagent and the sample needs to be stirred or shaken manually and continuously. Since the reagent solution used in this manner is basically strong acid or strong base, if the operator makes a slight mistake, personal injury may occur. Moreover, each batch of textiles needs to be tested for many times, the workload is large, the fatigue of operators is easily caused, and the safety and the accuracy of detection results are not facilitated.
Accordingly, the prior art is deficient and needs improvement.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provides a full-automatic textile fiber dissolution tester.
The technical scheme of the invention is as follows: there is provided a full-automatic textile fiber dissolution tester, comprising: the tester main part, set up in dissolving device in the tester main part, set up in stirring dewatering device of dissolving device below, set up in advance flowing back system in the tester main part and set up in control system in the tester main part, dissolving device includes: set up in water bath in the tester main part, place in dissolving tank in the water bath, set up in heating pipe in the water bath, locate in the turning block in the dissolving tank and set up in sample jar on the turning block, be provided with a plurality of stirring pieces on the turning block, be provided with a plurality of meshes on the sample jar, stirring dewatering device includes: the water bath tank comprises a motor arranged below the water bath tank, a first magnetic block connected with an output shaft of the motor, and a second magnetic block arranged on the rotating block.
Further, the liquid inlet and outlet system comprises: set up in feed liquor pump package in the tester main part, set up in the flowing back pump of feed liquor pump package side, connect a plurality of feed liquor pipes of feed liquor pump package and connection the fluid-discharge tube of fluid-discharge pump, the feed liquor pump package includes a plurality of feed liquor pump, the feed liquor pump is connected to the one end of feed liquor pipe, the other end of feed liquor pipe set up in dissolving tank top, the fluid-discharge pump is connected to the one end of fluid-discharge tube, the other end of fluid-discharge tube extends to the inboard bottom of dissolving tank, the feed liquor pump adopts the peristaltic pump, the fluid-discharge pump adopts peristaltic pump or diaphragm pump.
Further, the other end of the liquid discharge pump is connected with a waste liquid collecting device.
Furthermore, the dissolving tank is made of corrosion-resistant materials
Further, the dissolving tank is a glass container.
Furthermore, a water injection port and a drain pipe are arranged in the water bath tank.
Further, the tester main part upper cover has closed the upper cover, the upper cover lid fits the dissolving device top, the upper cover is transparent material.
Further, a cover plate is arranged in the sample tank.
Further, the control system includes: the main control circuit is arranged in the tester main body, and the operation panel and the temperature control panel are arranged on the tester main body, and the dissolving device, the stirring and dewatering device and the liquid inlet and drainage system are connected with the main control circuit.
Furthermore, a thermocouple and a liquid level switch are arranged in the water bath tank and are connected with the main control circuit.
By adopting the scheme, the non-contact stirring is realized through the action of the magnetic field between the first magnetic block and the second magnetic block of the stirring dehydration device, and meanwhile, the water bath heating can be carried out through the water bath tank to reach the dissolving temperature specified by the standard method.
Drawings
FIG. 1 is a schematic structural diagram of the present invention.
Fig. 2 is a cross-sectional view of the present invention.
Fig. 3 is a schematic structural view of the dissolving apparatus.
FIG. 4 is a schematic view of the structure of the stirring dewatering device.
Detailed Description
The invention is described in detail below with reference to the figures and the specific embodiments.
Referring to fig. 1 to 4, the present invention provides a full-automatic textile fiber dissolution tester, including: the tester comprises a tester body 1, a dissolving device 2 arranged in the tester body 1, a stirring and dewatering device 3 arranged below the dissolving device 2, a liquid inlet and outlet system 4 arranged in the tester body 1, and a control system 5 arranged in the tester body 1. The dissolving device 2 includes: the tester comprises a water bath 21 arranged in the tester body 1, a dissolving tank 22 arranged in the water bath 21, a heating pipe 211 arranged in the water bath 21, a rotating block 23 arranged in the dissolving tank 22 and a sample tank 24 arranged on the rotating block 23, wherein the rotating block 23 is provided with a plurality of stirring blocks 231. The sample tank 24 is provided with a plurality of meshes 241. The agitation dehydration means 3 comprises: the water bath device comprises a motor 31 arranged below the water bath tank 21, a first magnetic block 32 connected with an output shaft of the motor 31, and a second magnetic block 33 arranged on the rotating block 23.
Before testing, a plurality of small samples are cut from a sample cloth, the component details of the samples are determined according to the qualitative result of the samples, one component is selected as the target of the dissolution test, and corresponding dissolution reagent and neutralization reagent are selected and introduced into the liquid inlet and discharge system 4. And drying and weighing the cut sample, recording the weight of the sample before dissolution, then filling the sample into a corrosion-resistant filter bag, and marking. Several filter bags requiring dissolution testing using the same dissolution reagent are placed in the sample tank 24 and the tester is turned on. After the tester is started, water is injected into the water bath 21, and if the temperature requirement of the dissolution standard method is met, the heating pipe 211 is started to heat. Meanwhile, the dissolving reagent is introduced into the dissolving tank 22 through the liquid inlet and outlet system 4, enters the sample tank 24 through the meshes 241 on the sample tank 24, and permeates into the filter bag to be contacted with the small sample. The motor 31 is started to drive the first magnetic block 32 to rotate, and the second magnetic block 33 is driven to rotate under the action of magnetic force. Because the rotating block 23 connects the second magnetic block 33 with the sample tank 24, when the second magnetic block 33 is driven by magnetic force to rotate, the rotating block 23 and the sample tank 24 rotate together with the second magnetic block 33, and at the same time, the stirring block 231 on the rotating block 23 stirs the dissolving reagent in the dissolving tank 22, thereby increasing the dissolving speed of the selected component in the small sample. The heating pipe 211 in the water bath 21 continuously works to provide water bath heating for the dissolving tank 22, so that heat is transferred to the dissolving reagent in the dissolving tank 22, the movement of molecules in the dissolving reagent is promoted, and the dissolving efficiency is improved.
After the dissolution is completed, the liquid inlet and outlet system 4 discharges the mixed solution of the dissolution reagent in the dissolution tank 22, then adds the neutralization reagent into the dissolution tank 22 again, and starts the stirring and dewatering device 3, so that the neutralization reagent is fully contacted with the dissolved small sample residues, and the dissolution reagent remained on the small sample residues is neutralized. Then the mixed solution of the neutralizing agent is discharged, clean water is injected into the dissolving tank 22 through the liquid inlet and discharge system 4, and the water is discharged after the small sample residues are washed clean. Finally, the motor 31 is started under the condition that no liquid exists in the dissolving tank 22, so that the filter bag filled with the small sample residues carries out centrifugal motion along with the rotation of the sample tank 24, the water is thrown out, and the dehydration is completed. And taking out the filter bag, drying and weighing the weight of the residual substance of the small sample in the filter bag, comparing the weight with the weight weighed before testing, and calculating the total weight of the dissolved components in the small sample so as to obtain the fiber content of the selected components in the sample cloth.
The liquid inlet and outlet system 4 comprises: the liquid inlet pump set 41, the liquid discharge pump 42, the connection of the liquid inlet pump set 41 a plurality of liquid inlet pipes and the connection of the liquid discharge pump 42 are arranged in the tester body 1, the liquid inlet pump set 41 comprises a plurality of liquid inlet pumps, one end of each liquid inlet pipe is connected with the corresponding liquid inlet pump, the other end of each liquid inlet pipe is arranged above the dissolving tank 22, one end of each liquid discharge pipe is connected with the corresponding liquid discharge pump 42, and the other end of each liquid discharge pipe extends to the bottom of the inner side of the dissolving tank 22. Among the liquid inlet pump 41 and the liquid outlet pump 42, the liquid inlet pump 41 is a peristaltic pump, and the liquid outlet pump 42 is a peristaltic pump or a diaphragm pump. The different liquid inlet pumps in the liquid inlet pump unit 41 respectively inject corresponding reagents or liquids into the dissolving tank 22 in different processes, so as to meet the working requirements of each process. The drain pump 42 drains the liquid in the dissolving tank 22 through a drain pipe extending to the bottom of the inside of the dissolving tank 22 for the next process. In the process, manual operation is not needed, meanwhile, operators are not needed to contact various reagents, the automation of the detection process is realized, errors of the detection data caused by errors of the operators are avoided, and the accuracy of the test data is improved. Meanwhile, the damage of strong acid or strong base used in the process of being detected by operators carelessly is avoided, and the safety of the tester is improved.
The other end of the liquid discharge pump 42 is connected with a waste liquid collecting device. Because the dissolving reagent adopted in the dissolving process is generally strong acid or strong base, if the dissolving reagent is directly discharged outside without being treated, the environment can be polluted, and meanwhile, potential safety hazards are formed. The mixed solution formed after each process is discharged into a waste liquid collecting device, so that the environmental pollution is avoided, and the safety is improved.
The dissolving tank 22 is made of corrosion-resistant materials, so that the dissolving tank 22 is prevented from being corroded by a dissolving reagent to influence the dissolving effect.
In this embodiment, the dissolving tank 22 is a glass container. In the laboratory, glass containers are one of the common devices, which are easy to access. Meanwhile, if the glass container is damaged carelessly, the glass container for replacement can be obtained quickly, the detection requirement is met, and the universality of the tester is enhanced.
A water injection pipe and a water discharge pipe are arranged in the water bath 21 so as to conveniently inject water into the water bath 21 and discharge water.
The tester main part 1 upper cover closes upper cover 11, upper cover 11 covers and closes the dissolving device 2 top, upper cover 11 is transparent material. The upper cover 11 is covered above the dissolving device 2 in the detection process, so as to prevent the reagent from splashing and injuring surrounding operators in the operation process of the stirring dehydration device 3. The upper cover 11 made of transparent material is convenient for operators to observe the internal working condition of the tester, so that the operators can timely handle various possible abnormal conditions.
A cover plate 242 is provided in the sample tank 24. After the small sample or the filter bag containing the small sample is placed in the sample tank 24, the cover plate 242 is placed in the sample tank 24 and compresses the small sample or the filter bag, and when the sample tank 24 rotates at a high speed along with the second magnetic block 33, the small sample or the filter bag is prevented from being thrown out of an opening above the sample tank 24 under the action of centrifugal force.
The control system 5 includes: the main control circuit is arranged in the tester body 1, and the operation panel 51 and the temperature control panel 52 are arranged on the tester body 1, and the dissolving device 2, the stirring and dehydrating device 3 and the liquid inlet and outlet system 4 are connected with the main control circuit. The temperature control panel 52 can set the temperature parameters in the water bath 21, and control the heating pipe 211 to heat and maintain the water temperature through the main control circuit, thereby improving the dissolving efficiency.
A thermocouple 213 and a liquid level switch 212 are arranged in the water bath 21, and the thermocouple 213 and the liquid level switch 212 are connected with a main control circuit. In the process of water injection in the water bath 21, the liquid level height is detected through the liquid level switch 212, when the liquid level height reaches a preset value, water injection is stopped, and the heating pipe 211 is controlled to heat and raise the temperature. The thermocouple 213 can detect the temperature of water in the water bath 21 in real time and display the temperature through the temperature control panel 52, so that an operator can know the specific working conditions in the water bath 21.
In conclusion, the non-contact type stirring is realized through the action of the magnetic field between the first magnetic block and the second magnetic block of the stirring dehydration device, meanwhile, water bath heating can be carried out through the water bath tank, the dissolving temperature specified by the standard method is reached, the instrument can meet the requirement of simultaneously dissolving a large number of small samples, the detection efficiency is improved, the manual operation is reduced, the automation degree is improved, and the safety of operators is guaranteed.
The present invention is not limited to the above preferred embodiments, and any modifications, equivalent substitutions and improvements made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (10)
1. The utility model provides a full-automatic textile fiber dissolves tester which characterized in that includes: the tester main part, set up in dissolving device in the tester main part, set up in stirring dewatering device of dissolving device below, set up in advance flowing back system in the tester main part and set up in control system in the tester main part, dissolving device includes: set up in water bath in the tester main part, place in dissolving tank in the water bath, set up in heating pipe in the water bath, locate in the turning block in the dissolving tank and set up in sample jar on the turning block, be provided with a plurality of stirring pieces on the turning block, be provided with a plurality of meshes on the sample jar, stirring dewatering device includes: the water bath tank comprises a motor arranged below the water bath tank, a first magnetic block connected with an output shaft of the motor, and a second magnetic block arranged on the rotating block.
2. The fully automatic textile fiber dissolution tester according to claim 1, wherein the liquid inlet and outlet system comprises: set up in feed liquor pump package in the tester main part, set up in the flowing back pump of feed liquor pump package side, connect a plurality of feed liquor pipes of feed liquor pump package and connection the fluid-discharge tube of fluid-discharge pump, the feed liquor pump package includes a plurality of feed liquor pump, the feed liquor pump is connected to the one end of feed liquor pipe, the other end of feed liquor pipe set up in dissolving tank top, the fluid-discharge pump is connected to the one end of fluid-discharge tube, the other end of fluid-discharge tube extends to the inboard bottom of dissolving tank, the feed liquor pump adopts the peristaltic pump, and the fluid-discharge pump adopts peristaltic pump or diaphragm pump.
3. The fully automatic textile fiber dissolution tester according to claim 2, wherein a waste liquid collection device is connected to the other end of the liquid discharge pump.
4. The fully automatic textile fiber dissolution tester according to claim 1, wherein the dissolution tank is made of a corrosion resistant material.
5. The fully automatic textile fiber dissolution tester according to claim 1, wherein the dissolution tank is a glass container.
6. The fully automatic textile fiber dissolution tester as recited in claim 1, wherein a water inlet and a drain are disposed within the water bath.
7. The full-automatic textile fiber dissolution tester according to claim 1, wherein an upper cover covers the tester main body, the upper cover covers the dissolution device, and the upper cover is made of a transparent material.
8. The fully automatic textile fiber dissolution tester according to claim 1, wherein a cover plate is provided inside the sample tank.
9. The fully automatic textile fiber dissolution tester according to claim 1, wherein the control system comprises: the main control circuit is arranged in the tester main body, and the operation panel and the temperature control panel are arranged on the tester main body, and the dissolving device, the stirring and dewatering device and the liquid inlet and drainage system are connected with the main control circuit.
10. The full-automatic textile fiber dissolution tester according to claim 9, wherein a thermocouple and a level switch are disposed in the water bath, and the thermocouple and the level switch are connected to a main control circuit.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011334072.1A CN112284963A (en) | 2020-11-24 | 2020-11-24 | Full-automatic textile fiber dissolution tester |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011334072.1A CN112284963A (en) | 2020-11-24 | 2020-11-24 | Full-automatic textile fiber dissolution tester |
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| Publication Number | Publication Date |
|---|---|
| CN112284963A true CN112284963A (en) | 2021-01-29 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202011334072.1A Pending CN112284963A (en) | 2020-11-24 | 2020-11-24 | Full-automatic textile fiber dissolution tester |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113484184A (en) * | 2021-09-07 | 2021-10-08 | 南通春潮纺织品有限公司 | Digital image-based automatic detection method and device for fiber content in textile |
| CN113834751A (en) * | 2021-09-30 | 2021-12-24 | 常熟中纺联检测中心有限公司 | Quantitative and intelligent dissolving equipment for fibers |
-
2020
- 2020-11-24 CN CN202011334072.1A patent/CN112284963A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113484184A (en) * | 2021-09-07 | 2021-10-08 | 南通春潮纺织品有限公司 | Digital image-based automatic detection method and device for fiber content in textile |
| CN113834751A (en) * | 2021-09-30 | 2021-12-24 | 常熟中纺联检测中心有限公司 | Quantitative and intelligent dissolving equipment for fibers |
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