CN209148617U - A kind of Solid Phase Extraction charger - Google Patents

A kind of Solid Phase Extraction charger Download PDF

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Publication number
CN209148617U
CN209148617U CN201821707354.XU CN201821707354U CN209148617U CN 209148617 U CN209148617 U CN 209148617U CN 201821707354 U CN201821707354 U CN 201821707354U CN 209148617 U CN209148617 U CN 209148617U
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China
Prior art keywords
branch
phase extraction
injection tube
pipe coupling
solid phase
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Active
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CN201821707354.XU
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Chinese (zh)
Inventor
李双
陈树兵
方科益
李露青
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NINGBO ENTRY-EXIT INSPECTION AND QUARANTINE BUREAU TECHNICAL CENTER OF PEOPLE'S REPUBLIC OF CHINA
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NINGBO ENTRY-EXIT INSPECTION AND QUARANTINE BUREAU TECHNICAL CENTER OF PEOPLE'S REPUBLIC OF CHINA
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Priority to CN201821707354.XU priority Critical patent/CN209148617U/en
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Abstract

The utility model discloses a kind of Solid Phase Extraction chargers, feature be include a sample liquid syringe, several are sequentially connected in series the tee pipe coupling of connection and several and the one-to-one branch's injection tube of tee pipe coupling, bolt is coaxially arranged on the syringe needle of sample liquid syringe, bolt is connect with the import of front end tee pipe coupling by thread seal, it closes the outlet of end tee pipe coupling, the liquid outlet of sample liquid syringe is connected to form infusion primary path with the supervisor of each tee pipe coupling, the branch pipe of each tee pipe coupling passes through pipeline and is connected to form infusion forehearth limb with branch injection tube, venthole is provided on branch's injection tube and at its inlet, the liquid outlet of branch's injection tube is provided with the column cap being used cooperatively with solid phase extraction column, the through-hole for connected component's injection tube and solid phase extraction column is provided in column cap, it is excellent Point be can batch complete activation, balance, elution and elution, and operate it is convenient.

Description

A kind of Solid Phase Extraction charger
Technical field
The utility model relates to chemical experiment fixture technology field, in particular to a kind of Solid Phase Extraction charger.
Background technique
In chemical analysis field, solid-phase extraction device is the important purification of one kind, concentration tool, is provided for solid-phase extraction column Carrier and hyperbaric environment enable substance to elute or retain using the difference of substance retention factor in solid-phase extraction column, into And complete the purification and concentration of determinand.
Solid-phase extraction device can generally place 20-30 solid-phase extraction column, and the sample institute of same batch processed simultaneously What is used is all the solid-phase extraction column of same specification, and step divides equally are as follows: activation, balance, loading, elution, elution, in above-mentioned 5 step, In addition to loading need individually one by one complete other than, other four steps can batch operation, be completed at the same time.It is above-mentioned however in traditional operation Five steps pass through manually liquid feeding one by one and complete, time-consuming and laborious.In commercialization analysis detection laboratory, detection portfolio increasingly increases Greatly, when encountering the detection process for needing solid-phase extraction column, such device seriously restricts detection cycle.Therefore, design one is needed Kind can batch complete activation, balance, elution, elution, operate convenient and fast Solid Phase Extraction charger.
Summary of the invention
The technical problem to be solved by the utility model is to provide one kind can batch complete activation, balance, elution, elution, Operate convenient and fast Solid Phase Extraction charger.
Technical solution adopted by the utility model to solve the above technical problems is as follows: a kind of Solid Phase Extraction charger, including One sample liquid syringe, several be sequentially connected in series connection tee pipe coupling and several with the tee pipe coupling one by one Corresponding branch's injection tube, is coaxially arranged with bolt on the syringe needle of the sample liquid syringe, described in the bolt and front end The import of tee pipe coupling connected by thread seal, the outlet closing of tee pipe coupling described in end, the sample liquid The liquid outlet of syringe is connected to form infusion primary path with the supervisor of each tee pipe coupling, each tee tube The branch pipe of connector passes through pipeline and is connected to form infusion forehearth limb with corresponding branch's injection tube, branch's injection It is provided with venthole on cylinder and at its inlet, the liquid outlet of branch's injection tube is provided with and solid phase extraction column The column cap being used cooperatively is provided in the column cap for being connected to branch's injection tube and the solid phase extraction column Through-hole.
The syringe needle end of the sample liquid syringe is provided with for preventing the bolt to be detached from the sample liquid injection The stopper of the syringe needle of device, the stopper are the diameter that truncated cone-shaped and its maximum gauge are less than the bolt.
The upper end outer wall of the pipeline is arranged with T-type upper cover, the T-type upper cover and the tee pipe coupling Branch outlet pass through thread seal connect;The lower end outer wall of the pipeline is arranged with T-type lower head, seals under the T-type Head is connect with the inlet of branch's injection tube by thread seal.
The column cap is the descending multilayer coaxial clyinder successively to successively decrease of diameter from top to bottom.It can be with different size The solid phase extraction column of type matches.
Compared with the prior art, the advantages of the utility model are: the utility model discloses a kind of Solid Phase Extraction liquid feedings Device unscrews bolt at syringe needle and removes syringe, be filled liquid back spin in use, column cap is connect with solid phase extraction column one by one Tight bolt injects liquid into branch's injection tube, since branch's injection tube is equipped with venthole, is left a blank to liquid by gravity Afterwards, next step operation is carried out, the activation of SPE column is sequentially completed, is balanced, elution and elution.By this charger, can single step it is complete At the activation of all SPE columns of same batch, balance, the operation of elution and elution is suitble to the batch operation of large size assay laboratory, fastly It is prompt efficient.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model Solid Phase Extraction charger.
Specific embodiment
The utility model is described in further detail below in conjunction with figure embodiment.
Specific embodiment
A kind of Solid Phase Extraction charger, as shown in Figure 1, include a sample liquid syringe 1, several be sequentially connected in series connection Tee pipe coupling 2 and several and the one-to-one branch's injection tube 3 of tee pipe coupling 2, it is same on the syringe needle of sample liquid syringe 1 Axis is provided with bolt 4, and bolt 4 is connect with the import of front end tee pipe coupling 2 by thread seal, end tee pipe coupling 2 Outlet closing, the liquid outlet of sample liquid syringe 1 are connected to form infusion primary path, Mei Gesan with the supervisor of each tee pipe coupling 2 The branch pipe of connection for bbreather pipe 2 passes through pipeline 5 and the connection of corresponding branch's injection tube 3 forms infusion forehearth limb, on branch's injection tube 3 And venthole 6 is provided at its inlet, the liquid outlet of branch's injection tube 3 is provided with to be made with the cooperation of solid phase extraction column 7 Column cap 8 is provided with the through-hole (not shown) for connected component's injection tube 3 and solid phase extraction column 7 in column cap 8.
In this particular embodiment, as shown in Figure 1, the syringe needle end of sample liquid syringe 1 is provided with for preventing bolt 4 de- Stopper 9 from 1 syringe needle of sample liquid syringe, stopper 9 are the diameter that truncated cone-shaped and its maximum gauge are less than bolt 4.The upper end of pipeline 5 Outer wall is arranged with T-type upper cover 10, and T-type upper cover 10 is connect with the branch outlet of tee pipe coupling 2 by thread seal;Pipeline 5 lower end outer wall is arranged with T-type lower head 11, and the inlet of T-type lower head 11 and branch's injection tube 3 passes through thread seal company It connects.Column cap 8 is the descending multilayer coaxial clyinder successively to successively decrease of diameter from top to bottom.
Above-described embodiment is the further explanation to the utility model, but the protection scope of the utility model is with claim Subject to book.

Claims (4)

1. a kind of Solid Phase Extraction charger, it is characterised in that: including a sample liquid syringe, several be sequentially connected in series the three of connection Connection for bbreather pipe and several and the one-to-one branch's injection tube of the tee pipe coupling, the needle of the sample liquid syringe Bolt is coaxially arranged on head, the import of tee pipe coupling described in the bolt and front end is connected by thread seal, end The outlet closing of the end tee pipe coupling, the liquid outlet of the sample liquid syringe and each tee pipe coupling Supervisor's connection forms infusion primary path, and the branch pipe of each tee pipe coupling passes through pipeline and the corresponding branch Injection tube is connected to form infusion forehearth limb, is provided with venthole on branch's injection tube and at its inlet, described The liquid outlet of branch's injection tube be provided with the column cap being used cooperatively with solid phase extraction column, be provided with and be used in the column cap The through-hole of connection branch's injection tube and the solid phase extraction column.
2. a kind of Solid Phase Extraction charger according to claim 1, it is characterised in that: the syringe needle of the sample liquid syringe End is provided with the stopper of the syringe needle for preventing the bolt to be detached from the sample liquid syringe, and the stopper is rotary table Shape and its maximum gauge are less than the diameter of the bolt.
3. a kind of Solid Phase Extraction charger according to claim 1, it is characterised in that: the upper end outer wall set of the pipeline Equipped with T-type upper cover, the T-type upper cover is connect with the branch outlet of the tee pipe coupling by thread seal;Institute The lower end outer wall for the pipeline stated is arranged with T-type lower head, and the inlet of the T-type lower head and branch's injection tube is logical Cross thread seal connection.
4. a kind of Solid Phase Extraction charger according to claim 1, it is characterised in that: the column cap is straight from top to bottom The descending multilayer coaxial clyinder successively to successively decrease of diameter.
CN201821707354.XU 2018-10-22 2018-10-22 A kind of Solid Phase Extraction charger Active CN209148617U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821707354.XU CN209148617U (en) 2018-10-22 2018-10-22 A kind of Solid Phase Extraction charger

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821707354.XU CN209148617U (en) 2018-10-22 2018-10-22 A kind of Solid Phase Extraction charger

Publications (1)

Publication Number Publication Date
CN209148617U true CN209148617U (en) 2019-07-23

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201821707354.XU Active CN209148617U (en) 2018-10-22 2018-10-22 A kind of Solid Phase Extraction charger

Country Status (1)

Country Link
CN (1) CN209148617U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110604947A (en) * 2019-09-04 2019-12-24 天津渤海水产研究所 Organic matter solid phase extraction composite set

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110604947A (en) * 2019-09-04 2019-12-24 天津渤海水产研究所 Organic matter solid phase extraction composite set
CN110604947B (en) * 2019-09-04 2024-05-31 天津市水产研究所 Organic matter solid phase extraction composite set

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